分子量: 2235.421 Da / 分子数: 1 / 由来タイプ: 合成 詳細: The peptide was chemically synthesized. The sequence of the peptide occurs naturally in the fungus neurospora crassa. 参照: UniProt: P02807
-
実験情報
-
実験
実験
手法: 溶液NMR
NMR実験
Conditions-ID
Experiment-ID
Solution-ID
タイプ
1
1
1
2D TOCSY
1
2
1
2D NOESY
1
3
1
DQF-COSY
NMR実験の詳細
Text: This structure was determined using standard 2D homonuclear techniques
-
試料調製
詳細
内容: 0.5 mM Neurospora crassa MT, 20 mM phosphate buffer, 0.1 mM 2,2-dimethyl-2-silapentane-5-sulfonate, 0.02% NaN3, 90% H2O, 10% D2O 溶媒系: 90% H2O/10% D2O
試料状態
イオン強度: 20 mM KPi / pH: 6.5 / 圧: ambient / 温度: 283 K
手法: the hybrid distance geometry-dynamical simulated annealing protocol ソフトェア番号: 1 詳細: the structure was calculated with 152 NOEs and 13 dihedral angle restraints