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- PDB-1h6l: beta-propeller phytase in complex with phosphate and calcium ions -
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Open data
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Basic information
Entry | Database: PDB / ID: 1h6l | ||||||
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Title | beta-propeller phytase in complex with phosphate and calcium ions | ||||||
![]() | 3-PHYTASE | ||||||
![]() | HYDROLASE / PHOSPHATASE / PHYTASE / PROPELLER / PHOSPHATE | ||||||
Function / homology | ![]() | ||||||
Biological species | ![]() ![]() | ||||||
Method | ![]() ![]() | ||||||
![]() | Shin, S. / Ha, N.C. / Oh, B.H. | ||||||
![]() | ![]() Title: Enzyme Mechanism and Catalytic Property of Beta Propeller Phytase Authors: Shin, S. / Ha, N.C. / Oh, B.H. / Oh, T. / Oh, B.H. | ||||||
History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 87.8 KB | Display | ![]() |
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PDB format | ![]() | 63.7 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 371.6 KB | Display | ![]() |
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Full document | ![]() | 372.2 KB | Display | |
Data in XML | ![]() | 8.2 KB | Display | |
Data in CIF | ![]() | 12.8 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
Related structure data | ![]() 2pooS S: Starting model for refinement |
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Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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Unit cell |
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Components
#1: Protein | Mass: 38821.566 Da / Num. of mol.: 1 / Source method: isolated from a natural source / Source: (natural) ![]() ![]() | ||||
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#2: Chemical | ChemComp-CA / #3: Chemical | #4: Water | ChemComp-HOH / | |
-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 2.23 Å3/Da / Density % sol: 44.87 % | ||||||||||||||||||||
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Crystal grow | pH: 6.5 / Details: pH 6.50 | ||||||||||||||||||||
Crystal grow | *PLUS Temperature: 277 K / Method: vapor diffusion, hanging drop / Details: Ha, N.C., (1999) Acta Crystallogr, D55, 691. | ||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 297 K |
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Diffraction source | Source: ![]() |
Radiation | Monochromator: GRAPHITE / Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength: 1.5418 Å / Relative weight: 1 |
Reflection | Resolution: 1.8→20 Å / Num. obs: 32362 / % possible obs: 94.7 % / Observed criterion σ(I): 1 / Redundancy: 7.73 % / Rmerge(I) obs: 0.059 / Net I/σ(I): 12 |
Reflection shell | Resolution: 1.8→1.86 Å / Redundancy: 2.5 % / Rmerge(I) obs: 0.271 / Mean I/σ(I) obs: 3 / % possible all: 80.2 |
Reflection | *PLUS Lowest resolution: 20 Å / Num. measured all: 250463 |
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Processing
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Refinement | Method to determine structure: ![]() Starting model: 2POO Resolution: 1.8→20 Å / σ(F): 1
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Refinement step | Cycle: LAST / Resolution: 1.8→20 Å
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Refine LS restraints |
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Software | *PLUS Name: CNS / Classification: refinement | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refinement | *PLUS Lowest resolution: 20 Å | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Solvent computation | *PLUS | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | *PLUS |