分子量: 8634.127 Da / 分子数: 1 / 断片: P4 STEM / 変異: C70U / 由来タイプ: 合成 詳細: synthesized from DNA oligonucleotide template by T7 RNA polymerase
-
実験情報
-
実験
実験
手法: 溶液NMR
NMR実験
Conditions-ID
Experiment-ID
Solution-ID
タイプ
1
1
1
2D NOESY
2
2
2
2D NOESY
3
3
3
2D NOESY
4
4
4
2D NOESY
2
5
2
DQF-COSY
2
6
2
31P-1H-COSY
2
7
2
13C-1H-HMQC
NMR実験の詳細
Text: This structure was determined using standard 2D homonuclear techniques as well as 13C and 31P heteronuclear experiments at natural isotope abundance
手法: restrained molecular dynamics, simulated annealing / ソフトェア番号: 1 詳細: The average structure is based on superposition of 17 converged structures after refinement. The average RMS deviation between the ensemble and the average structure is 1.9 Angstrom. A total ...詳細: The average structure is based on superposition of 17 converged structures after refinement. The average RMS deviation between the ensemble and the average structure is 1.9 Angstrom. A total of 268 NOE derived distance constraints, 171 dihedral restraints and 49 distance restraints from hydrogen bonds were used for refinement