Text: REPRESENTATIVE MODEL NUMBER: 1 THE STRUCTURE WAS DETERMINED USING A 3D N15-EDITED NOESY-HSQC AND HOMONUCLEAR 2D NOESY EXPERIMENTS.
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試料調製
詳細
内容: 10 MM ACETATE BUFFER
試料状態
イオン強度: 50 mM NACL / pH: 5.6 / 温度: 310 K
結晶化
*PLUS
手法: other / 詳細: NMR
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NMR測定
NMRスペクトロメーター
タイプ: Bruker AMX600 / 製造業者: Bruker / モデル: AMX600 / 磁場強度: 600 MHz
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解析
ソフトウェア
名称
分類
X-PLOR
モデル構築
X-PLOR
精密化
X-PLOR
位相決定
NMR software
名称
バージョン
開発者
分類
XPLOR 3.851 (EXTENDED VERSION)
VERSION)
BRUNGER, NILGES
精密化
XPLOR (EXTENDED VERSION)
VERSION)
構造決定
精密化
手法: simulated annealing / ソフトェア番号: 1 詳細: STRUCTURE CALCULATIONS WERE PERFORMED WITH THE SUPPORT OF THE ARIA (AMBIGUOUS RESTRAINTS FOR ITERATIVE ASSIGNMENT) PROTOCOL (NILGES ET AL., J. MOL. BIOL. 269, 408-422). 100 STRUCTURES WERE ...詳細: STRUCTURE CALCULATIONS WERE PERFORMED WITH THE SUPPORT OF THE ARIA (AMBIGUOUS RESTRAINTS FOR ITERATIVE ASSIGNMENT) PROTOCOL (NILGES ET AL., J. MOL. BIOL. 269, 408-422). 100 STRUCTURES WERE CALCULATED OF WHICH THE BEST 50 STRUCTURES WERE SELECTED.
NMRアンサンブル
コンフォーマー選択の基準: LEAST RESTRAINT VIOLATION 計算したコンフォーマーの数: 1 / 登録したコンフォーマーの数: 50