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- PDB-151d: DIVERSITY OF WATER RING SIZE AT DNA INTERFACES: HYDRATION AND DYN... -
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Open data
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Basic information
Entry | Database: PDB / ID: 151d | ||||||||||||||||||
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Title | DIVERSITY OF WATER RING SIZE AT DNA INTERFACES: HYDRATION AND DYNAMICS OF DNA-ANTHRACYCLINE COMPLEXES | ||||||||||||||||||
![]() | DNA (5'-D(*![]() DNA / RIGHT HANDED DNA / DOUBLE HELIX / COMPLEXED WITH DRUG | Function / homology | DOXORUBICIN / DNA | ![]() Method | ![]() ![]() Lipscomb, L.A. / Peek, M.E. / Zhou, F.X. / Bertrand, J.A. / VanDerveer, D. / Williams, L.D. | ![]() ![]() Title: Water ring structure at DNA interfaces: hydration and dynamics of DNA-anthracycline complexes. Authors: Lipscomb, L.A. / Peek, M.E. / Zhou, F.X. / Bertrand, J.A. / VanDerveer, D. / Williams, L.D. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 15.6 KB | Display | ![]() |
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PDB format | ![]() | 8.9 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 414.9 KB | Display | ![]() |
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Full document | ![]() | 422.3 KB | Display | |
Data in XML | ![]() | 2.5 KB | Display | |
Data in CIF | ![]() | 3.3 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
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Links
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Assembly
Deposited unit | ![]()
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1 | ![]()
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Unit cell |
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Components
#1: DNA chain | Mass: 1809.217 Da / Num. of mol.: 1 / Source method: obtained synthetically |
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#2: Chemical | ChemComp-DM2 / |
#3: Water | ChemComp-HOH / |
-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 2.82 Å3/Da / Density % sol: 56.41 % | ||||||||||||||||||||||||||||||||
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Crystal grow | Method: vapor diffusion, sitting drop / pH: 6.5 / Details: pH 6.50, VAPOR DIFFUSION, SITTING DROP | ||||||||||||||||||||||||||||||||
Components of the solutions |
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-Data collection
Diffraction | Mean temperature: 113 K |
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Diffraction source | Source: ![]() |
Detector | Type: SDMS / Detector: AREA DETECTOR |
Radiation | Scattering type: x-ray |
Radiation wavelength | Relative weight: 1 |
Reflection | Highest resolution: 1.4 Å / Num. all: 17251 / Num. obs: 3402 / Observed criterion σ(F): 1 |
Reflection | *PLUS Highest resolution: 1.4 Å / Observed criterion σ(F): 1 / Num. measured all: 17251 / Rmerge F obs: 0.057 |
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Processing
Software | Name: NUCLSQ / Classification: refinement | ||||||||||||
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Refinement | Highest resolution: 1.4 Å / σ(F): 1 /
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Refine Biso |
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Refinement step | Cycle: LAST / Highest resolution: 1.4 Å
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Software | *PLUS Name: NUCLSQ / Classification: refinement | ||||||||||||
Refinement | *PLUS Highest resolution: 1.4 Å / σ(F): 1 / Rfactor obs: 0.2 | ||||||||||||
Solvent computation | *PLUS | ||||||||||||
Displacement parameters | *PLUS | ||||||||||||
Refine LS restraints | *PLUS
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