+Open data
-Basic information
Entry | Database: PDB / ID: 28dn | ||||||||||||||||||
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Title | CRYSTAL STRUCTURE ANALYSIS OF AN A(DNA) OCTAMER D(GTACGTAC) | ||||||||||||||||||
Components | DNA (5'-D(*Keywords | DNA / A-DNA / DOUBLE HELIX | Function / homology | DNA | Function and homology information Method | X-RAY DIFFRACTION / Resolution: 2.4 Å | Authors | Courseille, C. / Dautant, A. / Hospital, M. / Langlois D'Estaintot, B. / Precigoux, G. / Molko, D. / Teoule, R. | Citation | Journal: Acta Crystallogr.,Sect.A / Year: 1990 | Title: Crystal Structure Analysis of an A(DNA) Octamer d(GTACGTAC) Authors: Courseille, C. / Dautant, A. / Hospital, M. / Langlois D'Estaintot, B. / Precigoux, G. / Molko, D. / Teoule, R. History |
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-Structure visualization
Structure viewer | Molecule: MolmilJmol/JSmol |
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-Downloads & links
-Download
PDBx/mmCIF format | 28dn.cif.gz | 14.1 KB | Display | PDBx/mmCIF format |
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PDB format | pdb28dn.ent.gz | 8.3 KB | Display | PDB format |
PDBx/mmJSON format | 28dn.json.gz | Tree view | PDBx/mmJSON format | |
Others | Other downloads |
-Validation report
Summary document | 28dn_validation.pdf.gz | 364 KB | Display | wwPDB validaton report |
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Full document | 28dn_full_validation.pdf.gz | 366.8 KB | Display | |
Data in XML | 28dn_validation.xml.gz | 3.6 KB | Display | |
Data in CIF | 28dn_validation.cif.gz | 4.4 KB | Display | |
Arichive directory | https://data.pdbj.org/pub/pdb/validation_reports/8d/28dn ftp://data.pdbj.org/pub/pdb/validation_reports/8d/28dn | HTTPS FTP |
-Related structure data
Similar structure data |
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-Links
-Assembly
Deposited unit |
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1 |
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Unit cell |
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Components on special symmetry positions |
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-Components
#1: DNA chain | Mass: 2426.617 Da / Num. of mol.: 1 / Source method: obtained synthetically |
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#2: Water | ChemComp-HOH / |
-Experimental details
-Experiment
Experiment | Method: X-RAY DIFFRACTION |
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-Sample preparation
Crystal | Density Matthews: 2.31 Å3/Da / Density % sol: 46.67 % | ||||||||||||||||||||||||||||||||||||||||||||||||
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Crystal grow | Temperature: 293 K / Method: vapor diffusion, sitting drop / pH: 6 Details: pH 6.00, VAPOR DIFFUSION, SITTING DROP, temperature 293.00K | ||||||||||||||||||||||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS Temperature: 293 K / pH: 6 | ||||||||||||||||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 279 K |
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Detector | Type: NICOLET / Detector: DIFFRACTOMETER |
Radiation | Scattering type: x-ray |
Radiation wavelength | Relative weight: 1 |
Reflection | Highest resolution: 2.4 Å / Num. all: 2682 / Num. obs: 894 / Observed criterion σ(I): 1 |
Reflection | *PLUS Highest resolution: 2.4 Å / Observed criterion σ(I): 1 / Num. measured all: 2682 / Rmerge(I) obs: 0.055 |
-Processing
Software | Name: X-PLOR / Classification: refinement | ||||||||||||
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Refinement | Highest resolution: 2.4 Å / σ(I): 1 /
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Refine Biso |
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Refinement step | Cycle: LAST / Highest resolution: 2.4 Å
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Refinement | *PLUS Highest resolution: 2.4 Å | ||||||||||||
Solvent computation | *PLUS | ||||||||||||
Displacement parameters | *PLUS |