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- PDB-7qza: Crystal structure of a DyP-type peroxidase 29E4 variant from Pseu... -

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Open data

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Basic information

Entry

Database: PDB / ID: 7qza

Title

Crystal structure of a DyP-type peroxidase 29E4 variant from Pseudomonas putida

Components

Dyp-type peroxidase family protein

Keywords

OXIDOREDUCTASE / DyP / heme / directed evolution / Pseudomonas putida

Function / homology

Function and homology information

peroxidase activity / heme binding / metal ion binding
Similarity search - Function

Biological species

Pseudomonas putida (bacteria)

Method

X-RAY DIFFRACTION /

SYNCHROTRON /

MOLECULAR REPLACEMENT / Resolution: 2.698 Å

Authors

Borges, P.T. / Silva, D. / Frazao, C. / Martins, L.O.

Funding support

European Union,

United Kingdom, 2items

Organization	Grant number	Country
H2020 Marie Curie Actions of the European Commission	B-LigZymes H2020-MSCA-RISE 2018	European Union
Foundation for Science and Technology (FCT)	PTDC/BII-BBF/29564/2017	United Kingdom

Citation

Journal: Comput Struct Biotechnol J / Year: 2022
Title: Unveiling molecular details behind improved activity at neutral to alkaline pH of an engineered DyP-type peroxidase.
Authors: Borges, P.T. / Silva, D. / Silva, T.F.D. / Brissos, V. / Canellas, M. / Lucas, M.F. / Masgrau, L. / Melo, E.P. / Machuqueiro, M. / Frazao, C. / Martins, L.O.

History

Deposition	Jan 30, 2022	Deposition site: PDBE / Processing site: PDBE
Revision 1.0	Aug 3, 2022	Provider: repository / Type: Initial release
Revision 1.1	Aug 24, 2022	Group: Database references / Category: citation / citation_author Item: _citation.journal_volume / _citation.page_first ..._citation.journal_volume / _citation.page_first / _citation.page_last / _citation.pdbx_database_id_PubMed / _citation.title / _citation_author.name
Revision 1.2	May 1, 2024	Group: Data collection / Refinement description Category: chem_comp_atom / chem_comp_bond / pdbx_initial_refinement_model

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Structure visualization

Structure viewer	Molecule: MolmilJmol/JSmol

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Downloads & links

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Download

PDBx/mmCIF format	7qza.cif.gz	890.4 KB	Display	PDBx/mmCIF format
PDB format	pdb7qza.ent.gz	755.4 KB	Display	PDB format
PDBx/mmJSON format	7qza.json.gz		Tree view	PDBx/mmJSON format
Others	Other downloads

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Validation report

Summary document	7qza_validation.pdf.gz	3.2 MB	Display	wwPDB validaton report
Full document	7qza_full_validation.pdf.gz	3.2 MB	Display
Data in XML	7qza_validation.xml.gz	81.4 KB	Display
Data in CIF	7qza_validation.cif.gz	104.1 KB	Display
Arichive directory	https://data.pdbj.org/pub/pdb/validation_reports/qz/7qza ftp://data.pdbj.org/pub/pdb/validation_reports/qz/7qza	HTTPS FTP

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Related structure data

Related structure data	7qyqC 7qyzC C: citing same article (ref.)
Similar structure data	Similarity search - Function & homologyF&H Search Similarity search - FunctionF&H Search Similarity search - HomologyF&H Search

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Links

PDB pages	PDBj / wwPDB / NCBI

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Assembly

Deposited unit

A: Dyp-type peroxidase family protein

B: Dyp-type peroxidase family protein

C: Dyp-type peroxidase family protein

D: Dyp-type peroxidase family protein

E: Dyp-type peroxidase family protein

F: Dyp-type peroxidase family protein

G: Dyp-type peroxidase family protein

H: Dyp-type peroxidase family protein

hetero molecules

256 kDa, 8 polymers
Search similar-shape structures of this assembly by Omokage search (details)

A: Dyp-type peroxidase family protein

B: Dyp-type peroxidase family protein

C: Dyp-type peroxidase family protein

G: Dyp-type peroxidase family protein

hetero molecules

defined by author&software
Evidence: gel filtration
128 kDa, 4 polymers
Search similar-shape structures of this assembly by Omokage search (details)

D: Dyp-type peroxidase family protein

F: Dyp-type peroxidase family protein

hetero molecules

E: Dyp-type peroxidase family protein

H: Dyp-type peroxidase family protein

hetero molecules

defined by author&software
128 kDa, 4 polymers
Search similar-shape structures of this assembly by Omokage search (details)

Unit cell

Length a, b, c (Å)	72.957, 78.813, 98.931
Angle α, β, γ (deg.)	91.020, 92.930, 94.000
Int Tables number	1
Space group name H-M	P1

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Components

#1: Protein	Dyp-type peroxidase family protein Mass: 31351.293 Da / Num. of mol.: 8 Source method: isolated from a genetically manipulated source Source: (gene. exp.) Pseudomonas putida (bacteria) Strain: ATCC 47054 / DSM 6125 / CFBP 8728 / NCIMB 11950 / KT2440 Gene: PP_3248 / Production host: Escherichia coli BL21(DE3) (bacteria) / References: UniProt: Q88HV5
#2: Chemical	ChemComp-HEM / PROTOPORPHYRIN IX CONTAINING FE / HEME Mass: 616.487 Da / Num. of mol.: 8 / Source method: obtained synthetically / Formula: C₃₄H₃₂FeN₄O₄ / Feature type: SUBJECT OF INVESTIGATION
#3: Water	ChemComp-HOH / water Mass: 18.015 Da / Num. of mol.: 11 / Source method: isolated from a natural source / Formula: H₂O
Has ligand of interest	Y

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Experimental details

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Experiment

Experiment	Method: X-RAY DIFFRACTION / Number of used crystals: 1

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Sample preparation

Crystal	Density Matthews: 2.26 Å³/Da / Density % sol: 45.55 %
Crystal grow	Temperature: 293.15 K / Method: vapor diffusion, hanging drop / pH: 8.5 Details: 0.02 M magnesium chloride hexahydrate, 0.02 M calcium chloride dehydrate, 0.1 M Tris-BICINE pH 8.5, 37.5 % v/v of a precipitant mixture composed of 12.5 % v/v MPD, 12.5 % w/v PEG 1000, 12.5% w/v PEG 3350

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Data collection

Diffraction	Mean temperature: 100 K / Serial crystal experiment: N
Diffraction source	Source: SYNCHROTRON / Site: ALBA / Beamline: XALOC / Wavelength: 0.9792 Å
Detector	Type: DECTRIS PILATUS 6M / Detector: PIXEL / Date: Mar 9, 2019
Radiation	Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength	Wavelength: 0.9792 Å / Relative weight: 1
Reflection	Resolution: 2.698→98.78 Å / Num. obs: 54918 / % possible obs: 90.9 % / Redundancy: 2 % / B_iso Wilson estimate: 71.22 Å² / CC_1/2: 0.998 / R_pim(I) all: 0.04 / Net I/σ(I): 11.55
Reflection shell	Resolution: 2.7→2.8 Å / Num. unique obs: 7338 / CC_1/2: 0.497

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Processing

Software

Name	Version	Classification
PHENIX	1.13_2998	refinement
XSCALE		data scaling
PDB_EXTRACT	3.27	data extraction
XDS		data reduction
PHASER		phasing

Refinement

Method to determine structure:

MOLECULAR REPLACEMENT
Starting model: PpDyP WT

Resolution: 2.698→78.602 Å / SU ML: 0.38 / Cross valid method: FREE R-VALUE / σ(F): 1.97 / Phase error: 23.49 / Stereochemistry target values: LS_WUNIT_K1

	R_factor	Num. reflection	% reflection
R_free	0.1892	54892	100 %
R_work	0.1892	54892	-
obs	0.1892	54892	90.82 %

Solvent computation

Shrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å / Solvent model: FLAT BULK SOLVENT MODEL

Displacement parameters

B_iso max: 220.74 Å² / B_iso mean: 81.0125 Å² / B_iso min: 20 Å²

Refinement step

Cycle: final / Resolution: 2.698→78.602 Å

	Protein	Nucleic acid	Ligand	Solvent	Total
Num. atoms	17455	0	344	11	17810
B_iso mean	-	-	73.95	45.69	-
Num. residues	-	-	-	-	2264

LS refinement shell

Refine-ID: X-RAY DIFFRACTION / R_factor R_free error: 0

Resolution (Å)	R_factor R_free	Num. reflection R_free	R_factor R_work	Num. reflection R_work	% reflection obs (%)
2.698-2.7285	0.4278	1209	0.4278	1209	59
2.7285-2.7606	0.3925	1317	0.3925	1317	67
2.7606-2.7942	0.3716	1513	0.3716	1513	73
2.7942-2.8296	0.3657	1718	0.3657	1718	86
2.8296-2.8668	0.3692	1843	0.3692	1843	93
2.8668-2.9061	0.3547	1938	0.3547	1938	94
2.9061-2.9476	0.3342	1888	0.3342	1888	95
2.9476-2.9916	0.3081	1923	0.3081	1923	95
2.9916-3.0384	0.2854	1973	0.2854	1973	96
3.0384-3.0882	0.292	1878	0.292	1878	95
3.0882-3.1414	0.2846	1940	0.2846	1940	95
3.1414-3.1986	0.2751	1886	0.2751	1886	95
3.1986-3.2601	0.2678	1905	0.2678	1905	94
3.2601-3.3266	0.2608	1844	0.2608	1844	91
3.3266-3.399	0.2399	1931	0.2399	1931	95
3.399-3.478	0.2281	1885	0.2281	1885	93
3.478-3.565	0.2107	1930	0.2107	1930	96
3.565-3.6614	0.202	1893	0.202	1893	94
3.6614-3.7691	0.1923	1889	0.1923	1889	93
3.7691-3.8908	0.1716	1845	0.1716	1845	94
3.8908-4.0298	0.1631	1854	0.1631	1854	91
4.0298-4.1912	0.1617	1851	0.1617	1851	92
4.1912-4.3819	0.1501	1913	0.1501	1913	95
4.3819-4.6129	0.1355	1928	0.1355	1928	95
4.6129-4.9019	0.1362	1880	0.1362	1880	94
4.9019-5.2803	0.1496	1844	0.1496	1844	92
5.2803-5.8115	0.1522	1880	0.1522	1880	93
5.8115-6.6521	0.1686	1919	0.1686	1919	94
6.6521-8.3794	0.1404	1782	0.1404	1782	89
8.3794-78.602	0.1295	1893	0.1295	1893	94

Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°²)	L12 (°²)	L13 (°²)	L22 (°²)	L23 (°²)	L33 (°²)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å²)	T12 (Å²)	T13 (Å²)	T22 (Å²)	T23 (Å²)	T33 (Å²)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	-0.0037	-0.0096	0.0035	0.0104	0.0283	0.0595	0.0983	0.2816	-0.0951	-0.5017	0.3093	0.7142	0.4542	-0.0303	-0.0002	0.6273	0.114	-0.0213	0.572	0.0401	0.7186	-9.6378	6.7594	10.3769
2	0.0473	-0.2243	0.0375	1.1688	-0.24	0.0512	0.0174	0.0906	0.086	-0.5506	0.5417	0.061	-0.1388	0.4762	0.2198	0.5509	-0.1235	0.0596	0.8018	-0.0744	0.4433	11.3297	6.1328	3.8554
3	0.3344	-0.2152	-0.0087	0.3988	-0.0979	0.1016	-0.0235	0.7886	0.4775	-0.7953	-0.1463	0.0224	0.4895	0.0048	0.0366	0.6705	-0.058	-0.0851	0.7239	0.0846	0.5524	4.9725	12.7155	4.5594
4	0.0996	-0.0606	0.0209	0.551	0.4638	0.6314	0.2075	0.2131	0.1915	0.462	0.0618	0.3293	0.4092	0.336	-0.002	0.5009	0.0271	-0.0397	0.5277	-0.0102	0.514	4.5995	7.8528	16.7874
5	0.0027	0.0218	-0.0066	0.0484	-0.0045	0.0154	-0.1004	0.2308	-0.067	0.2888	-0.0904	0.2846	0.2756	0.6408	0.0001	0.7654	0.1346	-0.0097	0.7419	-0.0204	0.7041	8.2152	-2.6717	3.3717
6	0.0311	-0.0042	-0.0078	0.009	-0.0122	0.041	0.1047	0.1221	-0.2243	0.1315	0.7212	-0.2281	-0.0771	0.2782	-0.0009	0.5764	-0.026	0.0193	0.6875	-0.0517	0.6007	13.0081	2.325	9.1884
7	0.026	0.0086	0.026	0.0174	0.0218	0.0389	0.1898	-0.0538	-0.0994	-0.0755	0.1493	0.2967	0.6061	0.2886	-0	0.5669	0.0287	-0.08	0.6736	-0.0594	0.6382	-7.264	-2.5278	22.9314
8	0.0127	-0.0257	0.0023	0.0208	0.0226	0.0254	-0.0972	-0.1639	0.0263	-0.0918	-0.206	0.0028	-0.1861	-0.4093	-0.0001	0.7193	0.0248	0.0885	0.7695	-0.0622	0.7397	-11.813	3.8273	29.4326
9	0.0023	-0.0178	-0.0054	0.0385	0.0168	0.0188	-0.0007	-0.0836	0.3271	-0.4722	0.4921	0.0451	-0.0647	-0.2648	0.0001	0.7868	0.0737	0.0401	0.7863	0.172	0.76	-13.1606	18.1071	15.2114
10	0.1398	0.1356	-0.0712	0.1189	0.019	0.0822	-0.0903	0.0807	0.1189	0.3792	0.0391	0.1213	-0.1899	-0.0212	-0.0001	0.4764	0.0369	0.0469	0.4211	0.04	0.4999	-1.7561	3.9301	31.2898
11	0.2009	-0.0743	0.1291	0.0746	-0.0135	0.072	-0.0181	-0.2672	0.2216	0.1596	-0.0109	0.4043	-0.4898	-0.2616	-0.0001	0.8347	0.0603	0.2129	0.6419	-0.0213	0.7529	-11.8582	10.9368	37.1018
12	0.0187	-0.0045	-0.0145	0.0081	0.0057	0.0024	0.2664	-0.2604	0.1446	-0.0506	-0.2612	0.1171	-0.1482	-0.1049	-0.0002	1.2243	0.2225	0.272	0.7506	0.0479	0.8063	-8.83	25.0313	28.1667
13	0.0417	0.0433	-0.0614	0.0476	-0.0402	0.2284	-0.0384	0.0603	0.0399	0.0845	0.0396	0.1929	0.4025	-0.0271	-0.0005	0.4696	0.0327	0.0179	0.5197	-0.0395	0.5686	-2.0934	5.1807	21.9815
14	0.2354	0.2055	-0.2217	0.2169	-0.2399	0.2642	-0.3226	-0.09	-0.174	0.138	-0.6139	-0.0894	-0.5359	-0.0883	-0.0281	0.5349	0.1313	-0.0035	0.4697	0.0126	0.6847	-0.3415	20.6576	24.2823
15	0.07	0.0693	0.0867	0.031	0.0692	0.0737	0.1379	-0.1628	-0.0043	0.4776	0.3624	-0.1664	-0.1547	0.5199	-0.0003	0.7735	0.0614	0.0965	0.4538	-0.0439	0.5922	1.7961	12.9249	36.0583
16	0.134	0.1943	0.0357	0.1258	0.0678	0.041	-0.2632	-0.067	0.3079	-0.1708	-0.251	-0.1537	0.1783	-0.0361	-0.0064	0.4928	-0.0002	-0.038	0.533	0.1062	0.4815	2.1734	14.5701	6.5331
17	0.42	-0.2797	-0.1339	0.4808	-0.3325	0.1774	0.0877	-0.0897	-0.2575	0.4899	-0.0706	0.0128	-0.0021	0.0614	-0.0347	0.6689	-0.1047	-0.0958	0.7008	0.0373	0.4393	26.8485	4.0082	37.1662
18	0.0956	0.2007	0.0324	0.4416	0.0481	0.0124	-0.2653	-0.1146	0.308	0.2177	-0.0627	0.3103	-0.0569	-0.0144	0.0024	1.2564	-0.0537	-0.0409	0.8659	-0.0124	0.5666	17.2904	4.9807	49.5442
19	0.3789	0.2679	0.0384	0.1763	0.0962	0.1524	0.262	-0.5342	0.1672	0.4899	-0.3112	-0.1499	-0.0937	0.1574	0.0139	0.6476	0.0102	-0.1324	0.6389	-0.0074	0.5386	23.1108	10.4261	42.5276
20	0.2875	0.0682	-0.3624	0.0861	-0.0236	0.3265	0.1603	0.0722	0.2819	0.0951	-0.0606	-0.1531	0.4381	-0.3212	0.0001	0.5841	0.0092	-0.104	0.6011	-0.0133	0.4861	22.4992	10.0676	28.6758
21	0.0038	0.0207	-0.0087	0.0975	-0.0153	0.0246	0.4367	0.1135	0.2421	-0.0572	0.091	0.2109	-0.009	-0.3143	0.0001	0.8244	-0.0534	-0.0679	0.634	0.0898	0.6891	23.188	-7.5339	39.7129
22	0.0322	-0.0408	0.0082	0.0653	-0.0556	0.0271	-0.5931	0.5449	0.1335	0.4051	0.02	0.0756	-0.4689	0.4158	0.0001	0.7955	-0.0967	-0.0006	0.7178	-0.044	0.5789	17.1497	-0.327	36.1425
23	0.0362	0.0424	0.0333	0.0264	0.0276	0.0317	-0.0582	-0.1858	0.039	-0.3314	-0.2978	-0.5074	-0.0157	-0.2127	-0.0006	0.4321	0.0001	-0.1408	0.5733	0.0626	0.6061	37.4476	-1.4848	19.2927
24	0.2184	0.064	-0.2862	0.1558	-0.1286	0.3788	-0.1831	0.1512	0.3011	0.0651	0.0179	-0.1842	0.276	-0.03	-0.0669	0.4281	-0.0067	-0.1259	0.521	-0.0404	0.589	34.7457	11.2379	27.9829
25	0.0208	0.0205	-0.0054	0.0074	-0.0071	-0.0029	0.0435	0.2468	-0.0631	0.3795	-0.1035	-0.0012	-0.3536	-0.0882	-0	0.5795	-0.0155	-0.0203	0.7472	-0.0093	0.5624	32.4124	-0.2546	4.3376
26	0.0234	0.041	-0.0577	0.071	-0.1437	0.2203	-0.0343	0.5256	0.1636	0.1547	0.1883	-0.1829	-0.4239	0.26	0.0019	0.4693	-0.0959	0.0241	0.6783	-0.0309	0.702	39.8216	10.4109	9.2639
27	0.0411	-0.0008	-0.0235	0.0031	-0.0004	0.003	0.0051	-0.4135	-0.2555	-0.0897	-0.3173	-0.2582	-0.6187	0.1345	-0.0004	0.6871	-0.1813	-0.0978	0.6172	-0.0119	0.6914	37.8882	19.7644	22.2888
28	0.0699	-0.0151	-0.0269	0.0294	0.138	0.0825	-0.1166	-0.211	-0.0842	-0.0503	0.1539	-0.3261	0.1068	-0.1589	0.0001	0.3973	-0.0692	-0.0921	0.4563	-0.0277	0.4688	28.2501	4.3706	25.3625
29	0.362	-0.1444	-0.074	0.2818	0.2295	0.1888	-0.4411	0.569	0.2632	0.3393	-0.7996	0.1439	-0.2801	-0.2019	-0.0428	0.46	-0.1166	-0.0941	0.3915	-0.0266	0.7424	28.3785	19.9081	20.9626
30	0.0453	-0.0314	0.0258	0.0099	-0.0062	0.0141	0.1189	-0.2169	0.1081	-0.1096	0.3742	-0.396	-0.3059	-0.0121	0.001	0.4394	-0.0655	-0.0221	0.5599	-0.0066	0.6029	26.9157	16.7963	11.2959
31	0.0222	0.0513	-0.0225	0.1258	-0.027	0.0176	-0.0898	-0.012	0.1257	-0.1676	0.0788	-0.1273	-0.2708	-0.2497	0.0001	0.5428	-0.0631	-0.0438	0.5164	-0.0266	0.4751	23.6067	8.9947	23.5102
32	-0.004	0.0016	-0.0082	-0.0031	-0.017	0.0292	-0.288	-0.3408	0.0937	-0.1034	-0.1821	-0.0218	-0.0963	0.306	0.0001	0.9675	-0.0622	-0.164	0.8755	-0.005	0.7782	28.3098	13.2062	48.4344
33	0.0043	-0.0009	0.006	0.0087	0.0016	0.0085	-0.1578	0.3046	0.0209	0.1255	-0.2217	0.1561	-0.2185	-0.1303	-0.0001	1.0103	-0.0907	0.2377	0.4678	-0.1302	0.8303	-15.157	-30.9618	22.9134
34	0.0136	0.0105	0.0079	0.0213	0.0034	0.0156	-0.0878	-0.5731	0.0449	-0.5366	-0.1689	0.4569	-0.2147	-0.0403	-0.0002	0.8277	-0.064	0.1057	0.727	-0.0393	0.7705	-10.8808	-19.5228	17.1397
35	0.052	0.0632	0.0221	0.0653	-0.0388	0.0238	0.0074	0.1724	0.0612	0.7097	0.095	0.1034	0.3975	0.0806	0.0002	0.9568	-0.0406	0.0616	0.4472	0.0412	0.5411	1.5623	-26.4636	36.9861
36	0.0235	0.0023	0.0183	0.0385	-0.0004	0.0127	-0.2959	-0.2096	0.2402	0.3797	-0.1063	0.6028	-0.0924	0.0473	-0.0006	0.8526	-0.0193	0.3584	0.6075	0.0261	0.8469	-11.7449	-23.7645	32.3718
37	0.08	0.0735	0.0918	0.0847	0.0585	0.0624	0.0749	-0.186	-0.1476	0.1124	0.0657	0.1457	0.0199	0.3795	0	0.7991	0.0216	0.0459	0.5543	0.0275	0.6337	5.1244	-36.593	25.354
38	0.3307	-0.0449	0.3914	0.0146	0.0557	0.3845	-0.04	-0.737	0.0779	-0.3041	0.4978	0.1748	0.0823	-0.2787	0.0379	0.7459	-0.0549	0.1325	0.4904	-0.0212	0.6873	-6.5617	-18.3679	24.2089
39	0.0753	-0.0065	0.0532	0.0565	0.0065	0.0506	-0.1937	0.3682	0.3223	0.6921	-0.2098	0.0527	-0.0073	0.2855	0.0002	0.8738	-0.0379	0.064	0.5987	-0.0649	0.6232	-0.2462	-17.6784	34.1564
40	0.0787	0.1121	0.0172	0.1004	-0.0041	0.0194	0.335	-0.0898	0.0645	-0.0731	-0.0977	0.5233	-0.4011	-0.4356	-0.0001	0.7501	0.0556	-0.0904	0.6566	-0.013	0.8264	-2.5184	-16.4518	10.2804
41	0.0102	-0.009	0.0091	0.0454	-0.0359	0.0214	0.2127	-0.1534	-0.2756	-0.3798	-0.3986	0.6551	-0.0648	-0.6374	-0.0002	0.9157	-0.2651	-0.0359	0.9167	-0.1204	0.8271	-11.0057	-29.6026	6.2771
42	0.4163	-0.0025	0.4327	0.0145	-0.1722	0.5496	-0.1844	0.3415	-0.4167	0.2157	0.1475	0.0977	0.2944	0.1223	0.0013	0.7094	-0.0831	0.0639	0.4549	-0.0951	0.7559	-5.9356	-34.2871	18.4732
43	0.0085	0.0069	0.014	0.0186	0.0149	0.0186	0.1863	0.152	0.0596	0.0879	-0.0521	0.1408	-0.2969	0.2257	0	0.7308	-0.0894	0.0506	0.6371	-0.0292	0.683	9.6144	-18.353	-0.0107
44	0.0468	-0.0619	-0.0488	0.0761	0.0297	0.0927	-0.0593	0.3602	-0.2107	-0.3907	0.0682	0.0553	0.1788	0.201	0.0018	0.758	-0.0718	-0.0696	0.551	-0.0662	0.6013	0.2257	-30.6787	-3.3849
45	0.0668	0.0936	-0.086	0.0191	0.005	0.221	0.1801	-0.1231	-0.0312	0.1587	-0.0507	0.1143	-0.1088	-0.025	0.0001	0.5144	-0.0799	-0.0591	0.4567	-0.0761	0.5397	-1.5506	-28.1829	13.319
46	0.1773	-0.1113	-0.0279	0.1206	-0.1235	0.2916	0.1712	0.2188	-1.0865	-0.1677	0.2701	0.1885	-0.3705	0.2399	0.0135	0.6894	-0.1725	-0.0445	0.4593	-0.0628	0.7367	2.6259	-39.604	12.1564
47	0.1882	-0.0154	-0.0548	0.0409	-0.001	0.0295	0.0471	-0.2255	0.1017	-0.1708	0.1809	0.2365	0.1703	0.5837	-0.0002	0.6299	0.0031	0.0251	0.5003	-0.0648	0.5834	10.5294	-32.6155	5.4716
48	0.6758	-0.075	0.3988	0.0235	-0.1098	0.2683	-0.0152	0.0787	-0.185	0.4463	0.026	-0.0766	0.4046	-0.0415	0.0433	0.8276	-0.1519	0.1635	0.3652	-0.0535	0.6428	-7.4866	-33.6251	29.5773
49	0.0422	-0.0129	-0.0059	0.0034	0.0256	0.03	-0.575	0.1011	0.0739	0.1699	-0.1652	0.4864	-0.1585	0.1534	-0.0007	0.7044	0.0248	-0.1421	0.7908	0.1154	0.9777	32.5558	-9.8536	-5.8739
50	0.4557	0.4344	0.0396	1.1111	0.0614	0.0046	-0.004	-0.3268	0.1884	0.6482	-0.0513	0.0202	0.1614	0.228	0.0282	0.5288	0.0213	-0.06	0.7494	-0.0003	0.3714	50.562	-3.8936	-10.4027
51	0.0159	0.0348	-0.0154	0.0423	-0.0702	0.0524	-0.301	-0.5298	-0.1863	0.4122	-0.0548	-0.0917	-0.0798	-0.0377	-0.0001	0.7099	0.1578	-0.0497	0.8049	-0.0263	0.4869	45.472	-5.1105	-1.6285
52	0.0524	0.0247	0.0402	0.0065	0.0211	0.0069	0.3411	0.0624	-0.3188	0.2374	-0.5157	-0.2056	0.1954	0.1167	0.0001	0.669	0.0739	0.0577	0.6786	0.1061	0.6218	52.1071	-19.5608	-10.5365
53	0.3131	0.0184	0.1961	0.1261	0.0542	0.1043	-0.2614	0.1247	0.0141	-0.3176	0.2695	0.0667	-0.2766	0.0707	-0	0.5778	-0.038	0.0829	0.6571	-0.0107	0.5492	45.0865	-9.4979	-20.5395
54	0.0038	-0.0517	-0.001	0.0475	0.0662	0.0506	0.2416	0.1067	0.2804	0.3886	0.0733	0.0556	-0.2757	0.3818	0.0001	0.7123	-0.1592	-0.05	0.6814	-0.0347	0.5923	47.4841	6.2671	-7.6441
55	0.0141	-0.0518	0.0136	0.2339	0.2507	0.1297	-0.1775	-0.1848	0.8012	0.3158	-0.0744	0.0075	-0.1645	-0.0747	0	0.5862	-0.0327	-0.0339	0.8234	0.0956	0.6771	44.1984	1.053	-15.5928
56	0.0012	-0.0041	0.0026	0.0085	-0.0017	0.0046	-0.4767	0.0115	-0.1317	0.143	-0.143	0.3179	-0.0715	0.0394	-0.0005	0.5232	-0.1917	-0.0137	1.0741	0.0513	0.8341	27.6405	0.5037	-27.208
57	0.0129	-0.0162	0.0301	0.06	0.0151	0.0274	0.0989	-0.1812	0.0306	-0.169	-0.4039	0.1266	-0.0781	-0.0795	0.0003	0.9111	-0.3221	0.1782	1.1038	0.0094	0.8716	24.3679	-11.3058	-16.7242
58	0.0139	-0.0016	-0.0242	0.0118	0.016	0.0347	0.1113	-0.0517	-0.1453	-0.2107	0.4702	-0.085	0.2741	-0.2386	-0	0.8721	0.0015	0.2205	0.7928	0.199	0.9209	32.1342	-18.932	-9.3552
59	0.2218	0.0759	-0.0944	0.446	0.28	0.1777	0.0536	0.228	-0.0691	-0.3236	-0.0181	0.0603	0.3789	-0.1431	-0.0011	0.4992	-0.127	-0.1211	0.657	0.0622	0.4864	29.005	-3.762	-33.0932
60	0.0395	0.0082	0.0239	0.1554	0.1269	0.1105	-0.0799	-0.1177	0.0312	-0.0971	0.0192	0.5189	0.2721	-0.2346	0.002	0.794	-0.4948	-0.1513	1.1688	-0.0257	0.9171	27.1115	-15.4814	-32.3121
61	0.2678	-0.2345	0.2005	0.2196	-0.0576	0.0618	-0.1243	0.0093	0.0087	0.1101	-0.049	0.3718	-0.0638	-0.0788	0	0.4598	-0.1249	0.033	0.6012	0.0069	0.5401	35.6018	-9.1105	-21.5877
62	-0.006	-0.004	0.0114	0.036	-0.0122	0.0154	0.0223	0.0256	-0.0342	0.1206	-0.1864	0.5551	0.3484	0.0851	-0.0002	0.7672	-0.1979	0.0243	0.5481	0.0355	0.7388	37.736	-19.503	-25.5867
63	0.0276	-0.0674	-0.0413	0.0559	0.126	0.097	-0.3336	-0.0396	0.0518	-0.95	0.3667	-0.0355	0.1539	0.044	-0.0001	0.7309	-0.1667	-0.0505	0.7833	-0.05	0.4827	37.7062	-11.4812	-35.4068
64	0.0275	-0.0572	-0.0194	-0.03	0.0103	0.0056	-0.3127	-0.1589	0.2576	0.0172	0.1494	0.2458	-0.0274	-0.3095	-0.0009	0.6863	0.0855	0.0191	0.6748	0.1007	0.5309	44.8164	-14.7088	-5.5832
65	0.0763	0.0043	-0.0332	0.6309	-0.2209	0.0403	0.3573	-0.002	0.1196	-0.6179	-0.2455	-0.0866	0.3459	-0.0282	0.0191	0.5334	0.0662	-0.057	0.6914	0.0579	0.4853	-13.5011	-4.4415	-44.5029
66	0.0078	-0.0059	0.0119	-0.0019	0.0008	0.0098	0.1483	0.2024	-0.1086	-0.1081	-0.2766	0.0947	-0.0726	-0.1557	-0.0003	0.9434	-0.1197	-0.0364	1.1205	-0.0126	0.6431	-19.1485	-2.8982	-54.1317
67	0.5475	-0.2936	0.1212	0.1731	0.0199	0.1423	-0.3789	0.0781	-0.4704	-0.4993	-0.0313	-0.3137	0.4881	0.0584	-0.0011	0.7818	-0.0972	0.1047	0.6785	-0.0693	0.5658	-17.1879	-14.2714	-41.9243
68	0.001	-0.0185	0.0087	0.1902	0.1472	0.0898	0.018	-0.1191	-0.0554	-0.0676	0.0641	0.1256	-0.0736	-0.1491	0.0001	0.641	0.0918	0.0752	0.6392	0.0358	0.5881	-14.3123	-7.8816	-34.1994
69	0.0069	-0.0137	0.0158	0.067	-0.0403	0.0151	-0.3886	0.0915	-0.4061	-0.1137	0.1438	-0.1197	-0.086	-0.3643	0.0002	0.6792	0.1209	0.0477	0.4565	0.0166	0.57	-9.2185	8.8027	-44.0671
70	0.0268	-0.0136	-0.0199	0.0063	0.0167	0.0137	0.6914	0.0602	0.0142	0.0579	0.5582	0.1681	-0.4942	-0.3511	-0.0007	0.643	0.0542	-0.0288	0.7822	0.1013	0.7763	-23.2939	3.5315	-46.655
71	0.0021	-0.0016	0.0036	0.0368	-0.0131	0.0188	-0.1461	-0.1936	0.2749	0.0515	-0.1086	-0.3917	0.0405	0.2632	-0.0007	0.7111	0.1941	-0.0346	0.7545	-0.0958	0.513	-18.8465	0.685	-37.2277
72	0.055	-0.0167	-0.0448	0.0029	0.0091	0.0184	0.1155	0.0285	0.164	-0.0786	-0.0104	-1.0373	0.0962	0.1298	-0.0002	0.545	0.0903	0.0598	0.9245	-0.0544	0.7715	2.9262	0.1948	-29.3617
73	0.011	0.0015	0.0172	0.0535	-0.0445	0.0311	-0.2573	-0.0535	0.1038	0.1337	0.0507	-0.2043	0.4991	0.2029	0.0001	1.2049	0.3397	0.3015	1.1974	-0.008	0.9548	2.8243	-16.3663	-42.2129
74	0.1011	0.1856	-0.1857	0.5794	-0.5499	0.5354	-0.047	-0.087	-0.1425	-0.0422	-0.3547	-0.6833	0.4818	0.4495	-0.3553	0.4531	0.1666	-0.1716	0.7572	0.0599	0.721	0.859	-6.0287	-21.7551
75	0.07	-0.1846	0.0961	0.347	-0.1894	0.0871	-0.2361	-0.1991	-0.3117	0.2846	0.0795	-0.3728	0.4842	0.2587	-0.1162	0.6807	1.7861	-0.5752	0.9322	0.4942	0.7433	4.6447	-17.7022	-21.3232
76	0.0086	-0.0027	-0.0021	0.0199	-0.0044	0.0022	-0.2146	-0.1082	0.0943	0.0306	-0.2652	0.0737	-0.1011	-0.0121	-0.0004	1.4529	0.5638	0.292	1.4061	0.2073	1.2401	0.6748	-23.5961	-32.4379
77	0.102	0.2796	-0.1822	1.5771	-1.115	0.9007	-0.3464	-0.1021	0.2238	-0.6841	0.0733	-0.5352	0.2586	-0.0282	-0.0121	0.5102	0.1265	0.027	0.6734	-0.0169	0.5995	-6.8716	-6.584	-32.9362
78	0.2023	0.0767	0.0151	0.044	0.0298	0.0425	0.0955	-0.4746	-0.4171	0.0815	-0.1555	-0.6334	0.2638	0.3305	-0.0027	0.8137	0.2159	0.1224	0.6466	0.0422	0.7977	-7.0889	-19.7833	-26.7602
79	0.0099	0.0255	0.006	0.4378	-0.1117	0.0803	-0.1154	0.2855	-0.0826	0.9153	0.025	-0.2252	0.2772	0.0859	-0.0052	0.6225	0.2295	-0.0282	0.7264	0.0585	0.6275	-7.5564	-12.9937	-19.4196
80	0.0714	0.1149	0.016	0.0371	0.0248	0.0238	-0.0296	0.1825	-0.2042	-0.2167	0.1211	-0.0189	0.3169	-0.0424	-0.0001	0.7694	0.0485	0.1145	0.6196	-0.0892	0.5733	-13.858	-13.4667	-49.8819
81	0.0302	0.008	-0.0214	0.5476	-0.2115	0.2074	0.1342	0.3084	-0.2077	0.4018	0.213	0.7876	-0.4297	-0.4851	0.0039	0.698	0.2428	-0.0337	0.7518	0.2021	0.839	28.8476	25.2786	-16.7946
82	0.0493	0.12	-0.0176	0.2123	-0.0633	0.0157	-0.0867	0.2133	-0.1515	-0.5492	0.262	0.0172	-0.0232	-0.3354	0.0047	0.7496	0.1438	-0.1192	0.7544	0.151	0.595	36.7374	27.0925	-37.0337
83	0.0968	0.0361	-0.0787	0.4099	-0.3573	0.4075	0.5086	0.0366	0.2674	-0.1406	-0.0172	0.0941	-0.5585	-0.2302	0.014	0.8232	0.184	0.1771	0.7897	0.1393	0.7769	40.8904	34.0691	-26.8139
84	0.061	0.0414	0.076	0.0401	0.0548	0.0919	0.408	0.3152	0.2731	0.6115	-0.0973	-0.1445	-0.0527	-0.6386	-0.0019	0.6704	0.1332	-0.0208	0.7674	0.0975	0.9124	32.6736	17.7835	-21.9138
85	0.0138	-0.0014	-0.0038	0.0277	0.0079	0.0151	0.0543	-0.1744	-0.0255	0.0119	-0.3119	-0.264	-0.0507	-0.165	0.0001	0.8207	0.175	-0.2002	0.8317	0.1064	0.8937	34.1762	16.6972	-33.6791
86	0.1234	0.0194	0.0585	-0.0223	0.001	0.0417	0.3175	0.0302	0.1869	-0.1022	0.1554	0.7158	0.0813	0.1853	-0.0001	0.5434	0.0494	-0.009	0.6266	0.0695	0.6398	40.5639	19.5858	-24.7957
87	0.0172	-0.0064	0.0003	0.0596	0.0169	0.0213	0.4466	-0.4074	0.0844	0.4311	0.2943	0.3113	-0.1684	-0.0186	-0.0002	0.5415	0.0152	0.0393	0.5806	-0.008	0.6159	40.9312	19.7298	-3.7146
88	0.3062	0.2722	0.1318	0.8309	0.2784	0.1781	0.1843	0.0272	0.1728	0.3477	0.1321	-0.1278	-0.6553	-0.2137	0.231	0.5602	0.2212	0.2414	0.6218	0.0908	0.6223	35.5639	33.5553	-12.6828
89	0.0277	-0.0456	0.0358	0.0426	-0.0379	0.028	0.2078	-0.1942	-0.0935	0.387	0.0195	-0.1566	0.1597	0.2691	0.0001	0.7685	-0.0227	-0.0084	0.7449	-0.1362	0.5736	53.7466	19.9916	0.0059
90	0.0287	-0.0112	0.0013	0.0428	0.0105	-0.0021	0.3629	-0.2181	0.5882	0.1005	0.0245	0.2191	0.1799	-0.483	-0.001	0.9273	-0.0134	0.2203	0.6682	-0.1095	0.7858	43.6042	26.7057	6.7587
91	0.6504	-0.0313	-0.1141	0.5199	-0.1111	0.6015	0.4529	-0.3219	0.2684	0.1663	0.138	-0.3507	-0.9296	-0.1057	0.6815	1.1665	-0.0059	0.2737	0.6017	-0.0987	0.7136	47.7729	36.1771	-0.2551
92	0.4628	-0.0367	0.3451	0.0063	-0.0388	0.2815	-0.4593	0.1137	0.4897	-0.063	-0.0758	-0.2092	-0.1144	-0.3588	-0.0718	1.4149	0.3353	0.4626	0.7451	0.1221	1.0787	38.8958	39.8327	-7.3965
93	0.0664	-0.0388	0.124	-0.0084	-0.0235	0.3423	0.4468	0.5262	0.0048	-0.3244	0.2718	0.2971	-0.1883	0.0371	0.0125	0.4932	0.0497	0.0302	0.5981	-0.0253	0.6173	43.0733	22.1541	-15.744
94	0.3651	-0.2171	0.3516	0.9336	-0.1197	1.3734	0.4157	-0.1577	0.3226	-0.0424	0.2616	0.1811	-0.1629	-0.0593	0.5255	1.2895	0.0691	0.6092	0.286	0.0738	0.8129	45.2569	39.9269	-13.0387
95	0.0825	0.0087	0.0392	0.0083	0.0063	0.039	0.2217	0.368	-0.1268	0.023	0.1858	-0.1633	-0.5492	-0.0171	0.0002	0.8092	-0.1436	0.173	0.6709	-0.1252	0.6709	55.1842	32.134	-8.1806
96	0.0237	-0.0433	-0.0259	0.3542	0.0081	0.037	0.1844	-0.0197	-0.0446	-0.3343	0.2458	0.3692	-0.3167	-0.3727	0.3016	0.7948	0.2737	0.1064	0.7235	0.2261	0.7299	32.2175	35.0016	-27.6374
97	0.2205	-0.0077	-0.0527	0.168	-0.1737	0.1862	-0.3807	-0.2512	0.2619	0.0402	-0.1741	-0.5118	-0.1747	0.1376	-0.1202	1.007	0.286	-0.1969	0.7564	0.2056	1.0009	41.721	-30.8572	24.4101
98	0.0764	-0.0494	0.0274	0.2804	0.0069	0.1149	-0.5294	0.3252	-0.1735	-0.0648	0.5656	-0.1671	0.2894	0.4492	-0.0043	0.6391	-0.1215	0.0396	0.7207	-0.1052	0.625	27.7104	-24.2562	11.9431
99	0.1349	-0.2277	0.1507	0.4222	0.0113	0.093	0.1463	0.0934	0.0182	-0.0652	0.0157	-0.1307	-0.0184	-0.0747	0	0.6778	0.0328	0.0124	0.5889	-0.0557	0.7739	25.7158	-32.8946	17.2376
100	0.0325	0.0177	0.0083	0.013	-0.0182	0.0332	0.3507	0.036	-0.2345	0.5903	-0.1729	-0.1758	-0.4557	0.301	0.0002	0.7114	-0.008	0.0645	0.6807	-0.0017	0.9974	36.0367	-15.1101	23.5072
101	0.0785	-0.0829	0.0347	0.0543	-0.0076	-0.0042	-0.3467	0.2668	0.4149	-0.5804	-0.0579	-0.26	0.1342	0.0926	-0.0006	0.688	-0.0755	0.0319	0.7533	-0.0492	0.7296	29.4121	-16.443	10.9748
102	0.0221	0.0505	-0.0486	0.1577	0.0282	0.0619	-0.0742	0.1774	0.2032	0.3649	-0.2783	-0.486	-0.1358	-0.043	-0.0003	0.6399	0.0134	-0.1417	0.546	0.0073	0.6154	27.7667	-18.9378	30.2882
103	0.0067	-0.0195	0.0195	0.0059	-0.011	0.0199	-0.1259	-0.1985	-0.2224	0.0501	-0.2344	-0.3404	-0.0763	-0.0035	-0.0003	0.9652	0.0204	-0.2461	0.7118	0.1319	0.8754	32.2475	-27.9298	41.4468
104	0.026	0.0048	-0.0067	0.0115	0.0094	0.0085	-0.0995	0.208	-0.1489	-0.0168	0.0903	0.1088	-0.1982	0.1493	-0.0005	1.4158	0.3794	-0.3646	1.0194	0.1202	1.3902	42.9239	-36.9133	33.2599
105	0.2638	0.1354	0.1418	0.2038	0.0495	0.04	0.0984	-0.1897	-0.4604	0.6641	-0.1104	-0.1564	0.1369	0.0818	0.0928	0.8312	0.0902	-0.1845	0.5089	0.0318	0.7992	24.4784	-28.2493	34.3826
106	0.0181	-0.0113	0.0128	0.0247	0.0208	0.0568	-0.4363	0.1296	0.0696	0.378	0.4916	-0.0332	0.1754	0.1275	0.0005	1.353	-0.102	-0.2802	0.7345	0.0717	0.7635	25.7391	-29.2528	50.8201
107	0.0436	0.0319	-0.001	0.0663	-0.0324	-0.0008	-0.1755	-0.1907	-0.2999	0.1222	0.0148	-0.0809	0.1988	0.0275	0.0502	1.2409	0.1717	-0.3397	0.6401	0.1848	0.9981	27.1263	-40.3829	39.9869
108	0.135	-0.0264	-0.1699	0.024	-0.0134	0.1435	-0.1074	-0.0069	0.0467	0.2158	0.109	-0.5494	0.0691	-0.2299	0	0.5364	0.065	-0.1773	0.442	0.0364	0.6508	26.3897	-26.1908	29.2634
109	0.0595	0.0629	0.071	0.3825	0.172	0.1018	0.6644	-0.1622	-0.8985	0.3352	-0.1552	-0.3575	0.4051	-0.1653	0.0554	0.7628	0.0692	-0.2214	0.4427	0.0745	0.6425	19.8906	-41.2942	34.609
110	0.0357	0.0274	-0.0124	0.0186	-0.0299	0.0128	0.1316	-0.0641	0.231	0.2805	0.2367	0.5668	0.222	-0.1768	0.0004	0.7241	-0.0465	-0.1127	0.426	0.1086	0.5757	15.3711	-29.5301	38.027
111	0.0149	0.0139	-0.002	0.0296	0.0219	0.0121	0.1567	-0.0792	-0.0781	-0.0647	-0.2021	-0.1692	0.4532	-0.0298	0	0.7131	0.0248	-0.0835	0.5746	-0.1305	0.6983	26.0787	-33.9074	20.2438
112	0.0037	-0.021	0.0129	0.0245	-0.0466	0.0358	-0.1675	0.1471	-0.0513	-0.0433	0.1009	-0.0367	0.114	0.2404	-0.0001	0.7404	0.1778	0.149	1.0448	-0.0054	1.1882	38.8713	-35.7346	10.1349
113	0.014	0.0101	-0.0094	0.0022	-0.0062	0.0056	-0.3504	0.0211	0.032	0.0007	-0.03	-0.3704	0.1758	0.1169	-0.001	0.9531	0.0069	-0.093	0.9605	0.0056	0.7695	7.5032	30.9293	-32.1932
114	0.2349	-0.3387	0.1182	0.2774	-0.173	0.0639	0.2111	-0.0688	0.1855	0.1712	0.1316	-0.4526	-0.0075	0.1516	-0.0004	0.5861	-0.1618	0.0003	0.7599	-0.0787	0.7845	-2.6188	22.9253	-22.441
115	0.0696	-0.0638	-0.0084	1.0536	-1.0825	1.4951	0.3834	-0.1821	-0.1764	0.7067	0.0284	-0.841	-0.6997	1.2319	0.0784	0.6789	-0.2361	-0.0282	0.8874	-0.1956	0.9604	1.7276	29.4817	-18.8069
116	0.0761	-0.1598	0.2601	0.3487	-0.4289	0.6696	0.3818	-0.1667	-0.0496	-0.0544	0.2059	-0.2164	-0.9628	0.0344	0.0455	0.8574	-0.0635	0.1812	0.6622	-0.0491	0.7024	-11.1393	32.0586	-27.8757
117	0.0343	-0.057	0.038	0.0743	-0.0377	0.0321	0.3522	-0.1719	-0.3353	-0.1293	-0.0449	-0.158	-0.0221	0.0571	0.0003	0.53	-0.0287	-0.0974	0.8612	0.0124	0.7549	-0.1637	12.1186	-25.7718
118	0.1177	0.0249	-0.0051	0.0299	-0.0073	0.0249	0.2316	0.0588	-0.0512	0.0776	0.274	-0.5321	0.0058	-0.0141	-0.0015	0.6972	-0.0192	-0.06	0.7603	-0.0561	0.7445	-6.5516	19.0058	-19.0066
119	0.4411	-0.0848	0.5798	0.0513	-0.1574	0.8045	0.6053	-0.0377	0.2239	-0.4089	0.2602	-0.0765	-0.2184	0.1243	0.1024	0.7594	-0.082	0.2644	0.6424	-0.0694	0.8772	-7.1824	19.7873	-46.1818
120	0.0998	0.1225	-0.0365	0.0771	-0.0849	0.035	0.1888	0.3408	0.698	-0.3771	0.0712	-0.4353	-0.2083	0.2732	0.4875	0.8427	-0.8661	0.7735	0.5369	-0.0148	1.0087	2.5829	35.7874	-38.0407
121	0.0363	0.0279	0.0506	0.0361	0.0181	0.0607	0.3432	0.1476	0.1841	-0.5127	0.2514	-0.4593	-0.2335	-0.0178	0.0019	0.799	-0.0729	0.0908	0.5541	0.0404	0.6123	-19.3874	22.5207	-47.5286
122	0.5257	0.4685	0.4166	0.4106	0.3543	0.3263	-0.1343	0.4421	-0.0036	-0.2661	0.0319	-0.3829	-0.2556	0.1494	0.1172	1.3076	0.0938	0.218	0.6256	0.1602	0.6589	-11.5191	30.1227	-57.0521
123	0.3775	0.0299	0.0842	0.0268	-0.0156	0.0699	0.0005	0.1427	0.4989	-0.1046	-0.1479	-0.1566	-0.3938	0.0742	0.1849	1.4646	-0.884	0.3486	-1.9088	-0.7191	0.6892	-9.4055	39.9574	-46.146
124	0.994	-0.054	0.5777	0.0122	-0.0629	0.3362	0.3833	-0.3394	-0.1605	0.0218	-0.038	-0.329	-0.655	0.148	0.1471	0.6562	-0.1113	0.203	0.5298	-0.1751	0.5816	-8.4126	25.5404	-35.4733
125	1.4249	-0.2037	1.1549	0.8445	0.215	1.817	0.8149	-0.0572	0.2632	-0.4655	0.2099	-0.0853	-0.1662	0.1685	0.7936	1.5266	-0.1685	0.533	0.3504	-0.014	0.7478	-13.6457	40.0205	-38.0805
126	0.0443	-0.0408	0.0468	0.032	-0.0677	0.0598	0.3413	0.1257	0.216	-0.2002	0.0049	-0.0867	-0.471	-0.6336	0.0001	0.7677	0.1035	0.1619	0.5607	0.1027	0.6415	-21.1401	33.2447	-42.4511
127	0.0234	0.0091	0.0189	0.0011	-0.0003	0.015	-0.0796	-0.0257	-0.04	0.026	-0.0159	0.0422	-0.1782	-0.0235	-0.1262	0.8203	-0.1091	0.3635	0.4545	-0.2175	0.5838	-11.3197	30.7601	-28.2365
128	0.0041	-0.0259	0.0253	-0.0037	-0.0113	0.0281	-0.0778	0.245	0.077	-0.0866	0.3161	-0.1297	-0.266	0.5599	0.0004	1.0032	-0.1398	0.1565	1.1129	-0.1114	0.9694	7.7256	33.7686	-20.5014

Refinement TLS group

ID	Refine-ID	Refine TLS-ID	Selection details	Auth asym-ID	Auth seq-ID
1	X-RAY DIFFRACTION	1	(chain A and resid 3:16)	A	3 - 16
2	X-RAY DIFFRACTION	2	(chain A and resid 17:36)	A	17 - 36
3	X-RAY DIFFRACTION	3	(chain A and resid 37:61)	A	37 - 61
4	X-RAY DIFFRACTION	4	(chain A and resid 62:97)	A	62 - 97
5	X-RAY DIFFRACTION	5	(chain A and resid 98:107)	A	98 - 107
6	X-RAY DIFFRACTION	6	(chain A and resid 108:115)	A	108 - 115
7	X-RAY DIFFRACTION	7	(chain A and resid 116:127)	A	116 - 127
8	X-RAY DIFFRACTION	8	(chain A and resid 128:134)	A	128 - 134
9	X-RAY DIFFRACTION	9	(chain A and resid 135:150)	A	135 - 150
10	X-RAY DIFFRACTION	10	(chain A and resid 151:175)	A	151 - 175
11	X-RAY DIFFRACTION	11	(chain A and resid 176:203)	A	176 - 203
12	X-RAY DIFFRACTION	12	(chain A and resid 204:210)	A	204 - 210
13	X-RAY DIFFRACTION	13	(chain A and resid 211:233)	A	211 - 233
14	X-RAY DIFFRACTION	14	(chain A and resid 234:245)	A	234 - 245
15	X-RAY DIFFRACTION	15	(chain A and resid 246:262)	A	246 - 262
16	X-RAY DIFFRACTION	16	(chain A and resid 263:285)	A	263 - 285
17	X-RAY DIFFRACTION	17	(chain B and resid 3:27)	B	3 - 27
18	X-RAY DIFFRACTION	18	(chain B and resid 28:36)	B	28 - 36
19	X-RAY DIFFRACTION	19	(chain B and resid 37:61)	B	37 - 61
20	X-RAY DIFFRACTION	20	(chain B and resid 62:91)	B	62 - 91
21	X-RAY DIFFRACTION	21	(chain B and resid 92:105)	B	92 - 105
22	X-RAY DIFFRACTION	22	(chain B and resid 106:118)	B	106 - 118
23	X-RAY DIFFRACTION	23	(chain B and resid 119:132)	B	119 - 132
24	X-RAY DIFFRACTION	24	(chain B and resid 133:164)	B	133 - 164
25	X-RAY DIFFRACTION	25	(chain B and resid 165:175)	B	165 - 175
26	X-RAY DIFFRACTION	26	(chain B and resid 176:202)	B	176 - 202
27	X-RAY DIFFRACTION	27	(chain B and resid 203:214)	B	203 - 214
28	X-RAY DIFFRACTION	28	(chain B and resid 215:236)	B	215 - 236
29	X-RAY DIFFRACTION	29	(chain B and resid 237:245)	B	237 - 245
30	X-RAY DIFFRACTION	30	(chain B and resid 246:258)	B	246 - 258
31	X-RAY DIFFRACTION	31	(chain B and resid 259:271)	B	259 - 271
32	X-RAY DIFFRACTION	32	(chain B and resid 272:285)	B	272 - 285
33	X-RAY DIFFRACTION	33	(chain C and resid 3:7)	C	3 - 7
34	X-RAY DIFFRACTION	34	(chain C and resid 8:17)	C	8 - 17
35	X-RAY DIFFRACTION	35	(chain C and resid 18:33)	C	18 - 33
36	X-RAY DIFFRACTION	36	(chain C and resid 34:46)	C	34 - 46
37	X-RAY DIFFRACTION	37	(chain C and resid 47:81)	C	47 - 81
38	X-RAY DIFFRACTION	38	(chain C and resid 82:95)	C	82 - 95
39	X-RAY DIFFRACTION	39	(chain C and resid 96:114)	C	96 - 114
40	X-RAY DIFFRACTION	40	(chain C and resid 115:129)	C	115 - 129
41	X-RAY DIFFRACTION	41	(chain C and resid 130:142)	C	130 - 142
42	X-RAY DIFFRACTION	42	(chain C and resid 143:160)	C	143 - 160
43	X-RAY DIFFRACTION	43	(chain C and resid 161:174)	C	161 - 174
44	X-RAY DIFFRACTION	44	(chain C and resid 175:206)	C	175 - 206
45	X-RAY DIFFRACTION	45	(chain C and resid 207:235)	C	207 - 235
46	X-RAY DIFFRACTION	46	(chain C and resid 236:245)	C	236 - 245
47	X-RAY DIFFRACTION	47	(chain C and resid 246:263)	C	246 - 263
48	X-RAY DIFFRACTION	48	(chain C and resid 264:285)	C	264 - 285
49	X-RAY DIFFRACTION	49	(chain D and resid 3:11)	D	3 - 11
50	X-RAY DIFFRACTION	50	(chain D and resid 12:31)	D	12 - 31
51	X-RAY DIFFRACTION	51	(chain D and resid 32:47)	D	32 - 47
52	X-RAY DIFFRACTION	52	(chain D and resid 48:64)	D	48 - 64
53	X-RAY DIFFRACTION	53	(chain D and resid 65:91)	D	65 - 91
54	X-RAY DIFFRACTION	54	(chain D and resid 92:105)	D	92 - 105
55	X-RAY DIFFRACTION	55	(chain D and resid 106:124)	D	106 - 124
56	X-RAY DIFFRACTION	56	(chain D and resid 125:131)	D	125 - 131
57	X-RAY DIFFRACTION	57	(chain D and resid 132:140)	D	132 - 140
58	X-RAY DIFFRACTION	58	(chain D and resid 141:153)	D	141 - 153
59	X-RAY DIFFRACTION	59	(chain D and resid 154:191)	D	154 - 191
60	X-RAY DIFFRACTION	60	(chain D and resid 192:205)	D	192 - 205
61	X-RAY DIFFRACTION	61	(chain D and resid 206:235)	D	206 - 235
62	X-RAY DIFFRACTION	62	(chain D and resid 236:245)	D	236 - 245
63	X-RAY DIFFRACTION	63	(chain D and resid 246:264)	D	246 - 264
64	X-RAY DIFFRACTION	64	(chain D and resid 265:285)	D	265 - 285
65	X-RAY DIFFRACTION	65	(chain E and resid 3:31)	E	3 - 31
66	X-RAY DIFFRACTION	66	(chain E and resid 32:39)	E	32 - 39
67	X-RAY DIFFRACTION	67	(chain E and resid 40:71)	E	40 - 71
68	X-RAY DIFFRACTION	68	(chain E and resid 72:89)	E	72 - 89
69	X-RAY DIFFRACTION	69	(chain E and resid 90:99)	E	90 - 99
70	X-RAY DIFFRACTION	70	(chain E and resid 100:109)	E	100 - 109
71	X-RAY DIFFRACTION	71	(chain E and resid 110:117)	E	110 - 117
72	X-RAY DIFFRACTION	72	(chain E and resid 118:132)	E	118 - 132
73	X-RAY DIFFRACTION	73	(chain E and resid 133:151)	E	133 - 151
74	X-RAY DIFFRACTION	74	(chain E and resid 152:188)	E	152 - 188
75	X-RAY DIFFRACTION	75	(chain E and resid 189:205)	E	189 - 205
76	X-RAY DIFFRACTION	76	(chain E and resid 206:212)	E	206 - 212
77	X-RAY DIFFRACTION	77	(chain E and resid 213:237)	E	213 - 237
78	X-RAY DIFFRACTION	78	(chain E and resid 238:247)	E	238 - 247
79	X-RAY DIFFRACTION	79	(chain E and resid 248:265)	E	248 - 265
80	X-RAY DIFFRACTION	80	(chain E and resid 266:285)	E	266 - 285
81	X-RAY DIFFRACTION	81	(chain F and resid 3:17)	F	3 - 17
82	X-RAY DIFFRACTION	82	(chain F and resid 18:36)	F	18 - 36
83	X-RAY DIFFRACTION	83	(chain F and resid 37:83)	F	37 - 83
84	X-RAY DIFFRACTION	84	(chain F and resid 84:96)	F	84 - 96
85	X-RAY DIFFRACTION	85	(chain F and resid 97:107)	F	97 - 107
86	X-RAY DIFFRACTION	86	(chain F and resid 108:121)	F	108 - 121
87	X-RAY DIFFRACTION	87	(chain F and resid 122:132)	F	122 - 132
88	X-RAY DIFFRACTION	88	(chain F and resid 133:162)	F	133 - 162
89	X-RAY DIFFRACTION	89	(chain F and resid 163:179)	F	163 - 179
90	X-RAY DIFFRACTION	90	(chain F and resid 180:190)	F	180 - 190
91	X-RAY DIFFRACTION	91	(chain F and resid 191:206)	F	191 - 206
92	X-RAY DIFFRACTION	92	(chain F and resid 207:214)	F	207 - 214
93	X-RAY DIFFRACTION	93	(chain F and resid 215:233)	F	215 - 233
94	X-RAY DIFFRACTION	94	(chain F and resid 234:246)	F	234 - 246
95	X-RAY DIFFRACTION	95	(chain F and resid 247:263)	F	247 - 263
96	X-RAY DIFFRACTION	96	(chain F and resid 264:285)	F	264 - 285
97	X-RAY DIFFRACTION	97	(chain G and resid 3:11)	G	3 - 11
98	X-RAY DIFFRACTION	98	(chain G and resid 12:34)	G	12 - 34
99	X-RAY DIFFRACTION	99	(chain G and resid 35:86)	G	35 - 86
100	X-RAY DIFFRACTION	100	(chain G and resid 87:93)	G	87 - 93
101	X-RAY DIFFRACTION	101	(chain G and resid 94:110)	G	94 - 110
102	X-RAY DIFFRACTION	102	(chain G and resid 111:128)	G	111 - 128
103	X-RAY DIFFRACTION	103	(chain G and resid 129:136)	G	129 - 136
104	X-RAY DIFFRACTION	104	(chain G and resid 137:143)	G	137 - 143
105	X-RAY DIFFRACTION	105	(chain G and resid 144:173)	G	144 - 173
106	X-RAY DIFFRACTION	106	(chain G and resid 174:193)	G	174 - 193
107	X-RAY DIFFRACTION	107	(chain G and resid 194:213)	G	194 - 213
108	X-RAY DIFFRACTION	108	(chain G and resid 214:236)	G	214 - 236
109	X-RAY DIFFRACTION	109	(chain G and resid 237:252)	G	237 - 252
110	X-RAY DIFFRACTION	110	(chain G and resid 253:264)	G	253 - 264
111	X-RAY DIFFRACTION	111	(chain G and resid 265:271)	G	265 - 271
112	X-RAY DIFFRACTION	112	(chain G and resid 272:285)	G	272 - 285
113	X-RAY DIFFRACTION	113	(chain H and resid 3:8)	H	3 - 8
114	X-RAY DIFFRACTION	114	(chain H and resid 9:31)	H	9 - 31
115	X-RAY DIFFRACTION	115	(chain H and resid 32:61)	H	32 - 61
116	X-RAY DIFFRACTION	116	(chain H and resid 62:89)	H	62 - 89
117	X-RAY DIFFRACTION	117	(chain H and resid 90:103)	H	90 - 103
118	X-RAY DIFFRACTION	118	(chain H and resid 104:118)	H	104 - 118
119	X-RAY DIFFRACTION	119	(chain H and resid 119:132)	H	119 - 132
120	X-RAY DIFFRACTION	120	(chain H and resid 133:157)	H	133 - 157
121	X-RAY DIFFRACTION	121	(chain H and resid 158:178)	H	158 - 178
122	X-RAY DIFFRACTION	122	(chain H and resid 179:193)	H	179 - 193
123	X-RAY DIFFRACTION	123	(chain H and resid 194:213)	H	194 - 213
124	X-RAY DIFFRACTION	124	(chain H and resid 214:236)	H	214 - 236
125	X-RAY DIFFRACTION	125	(chain H and resid 237:248)	H	237 - 248
126	X-RAY DIFFRACTION	126	(chain H and resid 249:263)	H	249 - 263
127	X-RAY DIFFRACTION	127	(chain H and resid 264:269)	H	264 - 269
128	X-RAY DIFFRACTION	128	(chain H and resid 270:285)	H	270 - 285

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About Yorodumi

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News

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Feb 9, 2022. New format data for meta-information of EMDB entries

New format data for meta-information of EMDB entries

Version 3 of the EMDB header file is now the official format.
The previous official version 1.9 will be removed from the archive.

Related info.:EMDB header

External links:wwPDB to switch to version 3 of the EMDB data model

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Aug 12, 2020. Covid-19 info

Covid-19 info

URL: https://pdbj.org/emnavi/covid19.php

New page: Covid-19 featured information page in EM Navigator.

Related info.:Covid-19 info / Mar 5, 2020. Novel coronavirus structure data

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