分子量: 11038.354 Da / 分子数: 1 / 変異: H46W / 由来タイプ: 組換発現 / 詳細: loops IV and VII deleted, apo form / 由来: (組換発現) Homo sapiens (ヒト) / 遺伝子: SOD1 / 発現宿主: Escherichia coli (大腸菌) / 参照: superoxide dismutase
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実験情報
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実験
実験
手法: 溶液NMR
NMR実験
Conditions-ID
Experiment-ID
Solution-ID
Sample state
Spectrometer-ID
タイプ
1
1
1
isotropic
1
3D 1H-15N NOESY
1
2
1
isotropic
1
3D 1H-13C NOESY aliphatic
1
3
1
isotropic
1
3D 1H-13C NOESY aromatic
1
4
1
isotropic
1
2D 1H-15N HSQC
1
5
1
isotropic
1
2D 1H-13C HSQC aliphatic
1
10
1
isotropic
1
2D 1H-13C HSQC aromatic
1
9
1
isotropic
1
3D HNCO
1
8
1
isotropic
1
3DHN(CA)CO
1
7
1
isotropic
1
3D HNCA
1
17
1
isotropic
1
3DHN(CO)CA
1
16
1
isotropic
1
3DCBCA(CO)NH
1
15
1
isotropic
1
3D HN(CA)CB
1
14
1
isotropic
1
3DCC(CO)NH
1
13
1
isotropic
1
3D (H)CCH-COSY
1
12
1
isotropic
1
3D (H)CCH-TOCSY
1
11
1
isotropic
1
3DH(CCO)NH
1
23
1
isotropic
1
2D (HB)CB(CGCD)HD
1
22
1
isotropic
1
2D (HB)CB(CGCDCE)HE
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試料調製
詳細
タイプ: solution 内容: 1 mM [U-13C; U-15N] Monomeric Human Cu,Zn Superoxide dismutase, loops IV and VII deleted, apo form, with an additional mutation H46W, 10 mM Bis-Tris, 95% H2O/5% D2O Label: 13C/15N_sample / 溶媒系: 95% H2O/5% D2O