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- PDB-6vsu: Arginase from Arabidopsis thaliana in Complex with Ornithine -

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Open data

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Basic information

Entry

Database: PDB / ID: 6vsu

Title

Arginase from Arabidopsis thaliana in Complex with Ornithine

Components

Arginase 1, mitochondrial

Keywords

HYDROLASE / arginine amidinohydrolase /

ureohydrolase /

agmatinase / agmatine amidinohydrolase

Function / homology

Function and homology information

agmatinase / putrescine biosynthetic process from arginine, using agmatinase /

agmatinase activity /

arginase /

arginase activity /

urea cycle / protein hexamerization / cobalt ion binding / arginine catabolic process / defense response to bacterium ...
Similarity search - Function

Biological species

Arabidopsis thaliana (thale cress)

Method

X-RAY DIFFRACTION /

SYNCHROTRON /

MOLECULAR REPLACEMENT / Resolution: 2.25 Å

Authors

Sekula, B.

Funding support

United States, 1items

Citation

Journal: Front Plant Sci / Year: 2020
Title: The Neighboring Subunit Is Engaged to Stabilize the Substrate in the Active Site of Plant Arginases.
Authors: Sekula, B.

History

Deposition	Feb 11, 2020	Deposition site: RCSB / Processing site: RCSB
Revision 1.0	Aug 12, 2020	Provider: repository / Type: Initial release
Revision 1.1	Aug 19, 2020	Group: Database references / Category: citation / citation_author Item: _citation.page_first / _citation.page_last ..._citation.page_first / _citation.page_last / _citation.pdbx_database_id_PubMed / _citation.title / _citation_author.identifier_ORCID
Revision 1.2	Oct 11, 2023	Group: Data collection / Database references / Refinement description Category: chem_comp_atom / chem_comp_bond ...chem_comp_atom / chem_comp_bond / database_2 / pdbx_initial_refinement_model Item: _database_2.pdbx_DOI / _database_2.pdbx_database_accession

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Structure visualization

Structure viewer	Molecule: MolmilJmol/JSmol

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Downloads & links

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Download

PDBx/mmCIF format	6vsu.cif.gz	2.9 MB	Display	PDBx/mmCIF format
PDB format	pdb6vsu.ent.gz	2.5 MB	Display	PDB format
PDBx/mmJSON format	6vsu.json.gz		Tree view	PDBx/mmJSON format
Others	Other downloads

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Validation report

Arichive directory	https://data.pdbj.org/pub/pdb/validation_reports/vs/6vsu ftp://data.pdbj.org/pub/pdb/validation_reports/vs/6vsu	HTTPS FTP

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Related structure data

Related structure data	6vssSC 6vstC S: Starting model for refinement C: citing same article (ref.)
Similar structure data	6vst-2 6vss-d 6vst-1 3fz3-d 5wxu-d 1i33-2 6v6h-d 3pkj-7 Search similar-shape structures by Omokage search (details) Search similar-shape structures by Omokage search (details) Search similar-shape structures by Omokage search (details) Search similar-shape structures by Omokage search (details) Search similar-shape structures by Omokage search (details) Similarity search - Function & homologyF&H Search Similarity search - FunctionF&H Search Similarity search - HomologyF&H Search

Related structure data

6vssSC

6vstC

S: Starting model for refinement

C: citing same article (ref.)

Similar structure data

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Links

PDB pages	PDBj / wwPDB / NCBI

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Assembly

Deposited unit

A: Arginase 1, mitochondrial

B: Arginase 1, mitochondrial

C: Arginase 1, mitochondrial

D: Arginase 1, mitochondrial

E: Arginase 1, mitochondrial

F: Arginase 1, mitochondrial

G: Arginase 1, mitochondrial

H: Arginase 1, mitochondrial

I: Arginase 1, mitochondrial

J: Arginase 1, mitochondrial

K: Arginase 1, mitochondrial

L: Arginase 1, mitochondrial

M: Arginase 1, mitochondrial

N: Arginase 1, mitochondrial

O: Arginase 1, mitochondrial

P: Arginase 1, mitochondrial

Q: Arginase 1, mitochondrial

R: Arginase 1, mitochondrial

S: Arginase 1, mitochondrial

T: Arginase 1, mitochondrial

U: Arginase 1, mitochondrial

V: Arginase 1, mitochondrial

W: Arginase 1, mitochondrial

X: Arginase 1, mitochondrial

hetero molecules

847 kDa, 24 polymers
Search similar-shape structures of this assembly by Omokage search (details)

A: Arginase 1, mitochondrial

B: Arginase 1, mitochondrial

C: Arginase 1, mitochondrial

D: Arginase 1, mitochondrial

E: Arginase 1, mitochondrial

F: Arginase 1, mitochondrial

hetero molecules

defined by author&software
Evidence: SAXS
212 kDa, 6 polymers
Search similar-shape structures of this assembly by Omokage search (details)

G: Arginase 1, mitochondrial

H: Arginase 1, mitochondrial

I: Arginase 1, mitochondrial

J: Arginase 1, mitochondrial

K: Arginase 1, mitochondrial

L: Arginase 1, mitochondrial

hetero molecules

defined by author&software
212 kDa, 6 polymers
Search similar-shape structures of this assembly by Omokage search (details)

M: Arginase 1, mitochondrial

N: Arginase 1, mitochondrial

O: Arginase 1, mitochondrial

P: Arginase 1, mitochondrial

Q: Arginase 1, mitochondrial

R: Arginase 1, mitochondrial

hetero molecules

defined by author&software
211 kDa, 6 polymers
Search similar-shape structures of this assembly by Omokage search (details)

S: Arginase 1, mitochondrial

T: Arginase 1, mitochondrial

U: Arginase 1, mitochondrial

V: Arginase 1, mitochondrial

W: Arginase 1, mitochondrial

X: Arginase 1, mitochondrial

hetero molecules

defined by author&software
211 kDa, 6 polymers
Search similar-shape structures of this assembly by Omokage search (details)

Unit cell

Length a, b, c (Å)	267.322, 267.322, 262.894
Angle α, β, γ (deg.)	90.000, 90.000, 90.000
Int Tables number	80
Space group name H-M	I4₁

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Components

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Protein , 1 types, 24 molecules ABCDEFGHIJKLMNOPQRSTUVWX

#1: Protein	... Arginase 1, mitochondrial / / Agmatinase ARGAH1 / Arginine amidohydrolase 1 Mass: 34958.746 Da / Num. of mol.: 24 Source method: isolated from a genetically manipulated source Source: (gene. exp.) Arabidopsis thaliana (thale cress) / Tissue: leaves / Gene: ARGAH1, At4g08900, T3H13.7 / Production host: Escherichia coli BL21(DE3) (bacteria) / References: UniProt: P46637, arginase, agmatinase

#1: Protein

...
Arginase 1, mitochondrial /

/ Agmatinase ARGAH1 / Arginine amidohydrolase 1

Mass: 34958.746 Da / Num. of mol.: 24
Source method: isolated from a genetically manipulated source
Source: (gene. exp.)

Arabidopsis thaliana (thale cress) / Tissue: leaves / Gene: ARGAH1, At4g08900, T3H13.7 / Production host:

Escherichia coli BL21(DE3) (bacteria) / References: UniProt: P46637,

arginase,

agmatinase

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Non-polymers , 6 types, 5067 molecules

#2: Chemical	... ChemComp-MN / MANGANESE (II) ION Mass: 54.938 Da / Num. of mol.: 48 / Source method: obtained synthetically / Formula: Mn / Feature type: SUBJECT OF INVESTIGATION
#3: Chemical	... ChemComp-NA / SODIUM ION Mass: 22.990 Da / Num. of mol.: 24 / Source method: obtained synthetically / Formula: Na
#4: Chemical	ChemComp-ORN / L-ornithine / Ornithine Type: L-peptide linking / Mass: 132.161 Da / Num. of mol.: 9 / Source method: obtained synthetically / Formula: C₅H₁₂N₂O₂ / Feature type: SUBJECT OF INVESTIGATION
#5: Chemical	... ChemComp-GOL / GLYCEROL / GLYCERIN / PROPANE-1,2,3-TRIOL / Glycerol Mass: 92.094 Da / Num. of mol.: 30 / Source method: obtained synthetically / Formula: C₃H₈O₃
#6: Chemical	ChemComp-PEG / DI(HYDROXYETHYL)ETHER / Diethylene glycol Mass: 106.120 Da / Num. of mol.: 5 / Source method: obtained synthetically / Formula: C₄H₁₀O₃
#7: Water	ChemComp-HOH / water / Water Mass: 18.015 Da / Num. of mol.: 4951 / Source method: isolated from a natural source / Formula: H₂O

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Details

Has ligand of interest	Y

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Experimental details

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Experiment

Experiment	Method: X-RAY DIFFRACTION / Number of used crystals: 1

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Sample preparation

Crystal	Density Matthews: 2.8 Å³/Da / Density % sol: 56.05 %
Crystal grow	Temperature: 292 K / Method: vapor diffusion, hanging drop Details: 50 mM L-arginine, 50 mM L-glutamic acid, 22% PEG Smear Broad, 5% glycerol

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Data collection

Diffraction	Mean temperature: 100 K / Serial crystal experiment: N
Diffraction source	Source: SYNCHROTRON / Site: APS / Beamline: 22-ID / Wavelength: 1 Å
Detector	Type: DECTRIS EIGER X 16M / Detector: PIXEL / Date: Jun 27, 2018
Radiation	Monochromator: Si (111) / Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength	Wavelength: 1 Å / Relative weight: 1
Reflection	Resolution: 2.25→30 Å / Num. obs: 429624 / % possible obs: 99 % / Observed criterion σ(I): -3 / Redundancy: 3.3 % / CC_1/2: 0.994 / R_merge(I) obs: 0.064 / Net I/σ(I): 17.1
Reflection shell	Resolution: 2.25→2.33 Å / Redundancy: 3.4 % / R_merge(I) obs: 0.483 / Mean I/σ(I) obs: 2.5 / Num. unique obs: 43258 / CC_1/2: 0.747 / % possible all: 99.9

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Processing

Software

Name	Version	Classification
REFMAC	5.8.0238	refinement
PDB_EXTRACT	3.25	data extraction
HKL-3000		data reduction
HKL-3000		data scaling
PHASER		phasing

Refinement

Method to determine structure:

MOLECULAR REPLACEMENT
Starting model: 6VSS

6vss

Resolution: 2.25→29.97 Å / Cor.coef. F_o:F_c: 0.965 / Cor.coef. F_o:F_c free: 0.953 / SU B: 11.042 / SU ML: 0.143 / Cross valid method: THROUGHOUT / σ(F): 0 / ESU R: 0.22 / ESU R Free: 0.173
Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS U VALUES : WITH TLS ADDED

	R_factor	Num. reflection	% reflection	Selection details
R_free	0.1968	2236	0.5 %	RANDOM
R_work	0.1592	-	-	-
obs	0.1594	424973	98.43 %	-

Solvent computation

Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å

Displacement parameters

B_iso max: 152.12 Å² / B_iso mean: 41.31 Å² / B_iso min: 14.06 Å²

	B_aniso -1	B_aniso -2	B_aniso -3
1-	0.05 Å²	-0 Å²	-0 Å²
2-	-	0.05 Å²	-0 Å²
3-	-	-	-0.11 Å²

Refinement step

Cycle: final / Resolution: 2.25→29.97 Å

	Protein	Nucleic acid	Ligand	Solvent	Total
Num. atoms	58150	0	362	4951	63463
B_iso mean	-	-	53.9	40.71	-
Num. residues	-	-	-	-	7594

Refine LS restraints

Refine-ID	Type	Dev ideal	Dev ideal target	Number
X-RAY DIFFRACTION	r_bond_refined_d	0.014	0.013	59384
X-RAY DIFFRACTION	r_bond_other_d	0.002	0.017	56927
X-RAY DIFFRACTION	r_angle_refined_deg	1.783	1.638	80143
X-RAY DIFFRACTION	r_angle_other_deg	1.412	1.581	131992
X-RAY DIFFRACTION	r_dihedral_angle_1_deg	7.05	5	7583
X-RAY DIFFRACTION	r_dihedral_angle_2_deg	31.173	21.589	3172
X-RAY DIFFRACTION	r_dihedral_angle_3_deg	14.846	15	10506
X-RAY DIFFRACTION	r_dihedral_angle_4_deg	17.451	15	529
X-RAY DIFFRACTION	r_chiral_restr	0.089	0.2	7514
X-RAY DIFFRACTION	r_gen_planes_refined	0.009	0.02	67014
X-RAY DIFFRACTION	r_gen_planes_other	0.002	0.02	11973

LS refinement shell

Resolution: 2.251→2.309 Å / R_factor R_free error: 0 / Total num. of bins used: 20

	R_factor	Num. reflection	% reflection
R_free	0.31	130	-
R_work	0.237	29865	-
all	-	29995	-
obs	-	-	93.87 %

Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°²)	L12 (°²)	L13 (°²)	L22 (°²)	L23 (°²)	L33 (°²)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å²)	T12 (Å²)	T13 (Å²)	T22 (Å²)	T23 (Å²)	T33 (Å²)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	2.1665	0.7858	-0.0998	2.216	0.6041	3.1699	-0.3454	1.0934	-0.627	-0.4866	0.0164	-0.0416	0.5489	-0.7866	0.329	0.3913	-0.218	0.1421	0.8492	-0.349	0.4343	106.383	143.433	127.59
2	4.6907	-1.4799	0.2081	2.3432	0.6819	0.3828	0.0986	0.677	-0.1951	-0.4427	-0.0346	0.1046	-0.1085	-0.1519	-0.064	0.3257	-0.1809	-0.0223	1.0104	0.1657	0.0841	100.668	160.202	130.077
3	4.8053	0.0711	0.1585	4.0247	-0.0361	3.5679	-0.0771	1.0979	-1.4809	-0.4689	0.1725	-0.2606	0.5697	-0.0998	-0.0953	0.3662	-0.1111	0.0532	0.4586	-0.2955	0.5896	111.334	142.067	131.133
4	2.1235	0.7134	-0.7817	2.2323	0.2418	3.0582	-0.295	1.1861	-0.6918	-0.4005	0.2691	-0.4176	0.344	-0.1888	0.0259	0.2934	-0.1265	0.173	0.7379	-0.3285	0.4247	118.959	152.87	128.123
5	5.5418	1.9909	-2.0974	3.5838	-1.1992	1.0834	-0.0517	0.5146	-0.6507	-0.2637	0.1244	-0.4289	0.1502	0.153	-0.0727	0.3064	0.1335	0.0531	0.6708	-0.4938	0.7688	127.04	150.755	133.655
6	3.4641	-0.4053	-1.4206	1.5435	0.9495	2.6702	0.021	0.8959	-0.029	-0.4326	0.1921	-0.5257	-0.1591	-0.0219	-0.2131	0.2131	-0.0653	0.1588	0.4227	-0.0121	0.2689	123.065	166.101	133.719
7	3.1283	0.1702	-2.1341	1.8441	0.0308	5.2012	0.0007	0.934	-0.1297	-0.3983	0.1367	-0.0891	-0.0667	-0.5922	-0.1373	0.1905	-0.0628	0.0184	0.4711	0.0417	0.1207	109.181	161.887	132.628
8	9.4871	-3.6673	-8.0823	2.9281	3.8414	11.5878	0.109	-0.4561	0.1392	0.0661	0.1425	-0.1417	-0.1277	0.3918	-0.2515	0.1686	-0.0852	-0.0533	0.1442	0.0355	0.2525	133.561	171.048	179.6
9	3.052	-0.8346	-0.871	1.781	0.7414	2.8809	0.0756	0.0383	-0.0842	0.0567	0.0762	-0.2375	-0.0281	0.189	-0.1518	0.071	-0.0168	-0.0007	0.054	0.0433	0.2085	126.871	169.501	161.687
10	1.6089	0.3049	-0.3213	1.4145	-0.4251	2.2695	0.2296	-0.0954	0.4122	0.2346	0.0385	0.0458	-0.626	0.0494	-0.2681	0.3027	-0.0629	0.1296	0.05	0.0168	0.2822	124.907	186.802	166.897
11	2.615	-1.2326	0.6628	1.5033	0.6442	3.5419	0.3065	0.6747	0.8267	-0.4578	0.0749	-0.2823	-0.6837	0.3679	-0.3814	0.3989	-0.0199	0.218	0.3517	0.3182	0.4916	121.836	191.258	144.779
12	2.2342	0.8905	0.4183	0.8097	0.1843	2.0382	0.0994	0.2518	0.1039	-0.0331	0.0978	-0.1208	-0.3151	0.1494	-0.1972	0.1452	-0.0071	0.0896	0.0705	0.065	0.203	123.499	178.125	154.099
13	2.2798	-0.6515	-0.9684	3.5814	0.1147	1.4045	0.1077	0.596	0.597	0.4606	0.2944	0.5833	-0.4909	-0.8537	-0.4021	0.4493	0.3568	0.1487	0.7548	0.4654	0.4521	79.894	192.266	149.076
14	1.778	-0.8056	0.0453	1.7077	1.888	4.3735	0.318	0.1813	0.7457	-0.0071	-0.0681	-0.2554	-0.4569	-0.4473	-0.2499	0.3603	0.1706	0.2383	0.2492	0.294	0.5272	97.424	190.386	154.188
15	0.4549	-0.0616	0.2973	0.8123	-0.0196	3.8565	0.0165	0.2381	0.3582	-0.2129	0.1068	0.2746	-0.476	-1.0119	-0.1232	0.3349	0.294	0.058	0.7752	0.4447	0.4813	83.235	190.803	141.32
16	3.0767	-1.8457	0.7768	1.5467	-1.6494	3.7752	0.2945	0.5126	-0.0009	-0.3939	-0.232	0.084	0.3131	-0.1558	-0.0626	0.4729	0.1355	-0.0716	0.9371	0.3471	0.3061	90.251	182.042	128.882
17	2.3237	-1.3595	0.6771	1.8221	-0.1055	1.542	0.193	0.7587	0.4787	-0.5432	0.0146	-0.1542	-0.3683	-0.3336	-0.2076	0.3648	0.0848	0.1424	0.8415	0.4631	0.2838	101.916	184.76	132.376
18	1.5055	-0.0401	0.855	4.113	-1.308	3.3006	0.0576	0.3342	0.4333	-0.1384	0.0177	-0.1868	-0.484	-0.465	-0.0753	0.1939	0.175	0.136	0.3768	0.3047	0.2866	98.309	186.819	145.816
19	1.63	-0.4596	0.1905	1.9878	-0.1816	1.4843	0.0162	0.4603	-0.2504	-0.3965	0.101	-0.2229	0.2691	0.0358	-0.1171	0.2369	-0.1199	0.001	0.2358	-0.0511	0.1381	98.813	135.881	144.174
20	2.1464	-0.1205	-0.1924	1.6883	0.4786	1.6068	0.002	0.5525	-0.2119	-0.4414	0.092	0.0242	0.1243	-0.1315	-0.094	0.221	-0.1381	-0.0615	0.2815	0.0048	0.0591	86.505	136.682	142.311
21	3.898	1.7335	-1.4621	3.741	-1.8067	2.8571	0.155	0.2837	0.0562	-0.2507	-0.0577	0.3173	0.0058	0.0649	-0.0973	0.1706	-0.1145	-0.1033	0.3171	0.072	0.0747	76.138	141.036	144.507
22	1.9722	0.6365	0.0326	1.5858	1.4315	1.9224	0.0112	-0.1361	-0.0375	0.1479	-0.0322	0.1861	0.2179	-0.2714	0.021	0.1383	-0.1275	-0.0317	0.2519	0.1319	0.1071	76.261	140.829	158.843
23	1.5795	0.2244	0.3445	1.852	0.4142	1.6003	0.0311	0.1569	-0.074	-0.0006	0.0557	-0.1171	0.1265	-0.1007	-0.0868	0.0613	-0.0805	-0.0392	0.1316	0.0436	0.0341	91.716	143.893	158.317
24	10.2266	-2.3433	-7.0695	1.8351	2.459	7.3005	-0.0465	-0.1856	0.1414	0.0797	0.2098	-0.2867	0.1747	0.384	-0.1633	0.151	-0.0648	-0.1053	0.1368	-0.0118	0.1527	127.944	164.081	186.322
25	1.8394	-0.5117	-0.1993	2.3681	0.6613	1.6888	0.0251	-0.0488	0.2356	0.018	0.0845	-0.103	-0.2074	-0.0286	-0.1097	0.0627	-0.0277	-0.0239	0.044	0.0357	0.077	108.686	163.125	180.642
26	1.8612	0.335	-0.3831	1.9337	0.0484	1.482	0.0243	-0.0738	-0.1492	0.027	0.0261	-0.3383	0.1437	0.1847	-0.0504	0.0631	-0.0149	-0.0638	0.0455	0.0271	0.123	118.143	150.104	181.898
27	1.3797	-0.3307	0.4178	1.3416	-0.0917	1.7193	0.037	-0.0659	-0.1262	0.0482	0.0219	0.0013	0.2018	-0.1293	-0.059	0.0563	-0.0478	-0.0427	0.0477	0.0468	0.0546	102.241	148.325	178.685
28	7.9182	8.9805	1.7911	12.7742	1.8717	1.8259	0.1655	-0.1219	0.4885	-0.0842	-0.2873	0.4567	-0.3081	-0.3002	0.1219	0.2114	0.1502	-0.0111	0.333	0.1254	0.3204	68.5	188.189	158.476
29	2.7179	0.2136	0.5553	1.5233	0.6565	1.5222	0.0054	0.4663	0.3878	-0.1526	-0.0713	0.2494	-0.1381	-0.2567	0.0658	0.0382	0.0389	-0.0076	0.2782	0.1848	0.201	76.335	170.242	159.9
30	5.1082	1.8912	1.9701	1.7167	1.0283	2.72	-0.1038	0.2007	0.748	-0.1412	-0.1118	0.0453	-0.6889	-0.205	0.2156	0.23	0.1124	0.0053	0.2302	0.2405	0.4176	75.925	186.013	165.161
31	2.3049	-0.4861	-0.0987	1.7871	0.3273	2.2807	0.1234	0.1661	0.4892	0.0034	-0.1482	0.1491	-0.2628	-0.373	0.0248	0.0384	0.0441	0.0266	0.1485	0.101	0.2325	73.804	176.013	173.889
32	4.5349	1.6506	-3.3147	2.2338	-2.0864	4.642	0.1983	-0.5592	0.52	-0.0253	-0.1978	0.0248	-0.2423	0.1413	-0.0005	0.0838	0.0213	0.0371	0.1801	0.0018	0.2973	79.952	179.491	181.382
33	6.78	-2.4358	-4.3406	4.2999	3.5552	4.9234	-0.0105	-0.6592	0.1824	0.3299	0.1239	-0.056	0.1334	0.0569	-0.1134	0.0886	0.0017	0.021	0.1818	0.0286	0.1214	83.96	170.147	186.786
34	6.8213	1.2725	1.6806	4.6156	1.8219	1.6448	-0.0344	-0.4747	-0.1151	0.4615	-0.0468	0.2954	0.3872	-0.3742	0.0812	0.1468	-0.0604	0.0549	0.2012	0.0835	0.108	81.022	156.954	183.435
35	7.1819	-0.8459	0.5056	2.0685	-0.9531	0.6899	-0.1453	0.0875	0.129	0.2627	0.0694	0.2508	0.0206	-0.2023	0.076	0.1286	-0.0924	0.1258	0.216	-0.0527	0.225	71.641	167.014	177.024
36	2.7052	-0.4896	-0.4821	1.2225	0.0256	0.7316	0.2093	0.1728	0.0057	0.1398	-0.094	0.0512	0.0828	-0.2026	-0.1153	0.0702	-0.0304	-0.0129	0.1167	0.0677	0.0509	85.258	160.429	170.548
37	7.8313	-0.0925	-3.1967	1.8867	0.9501	2.4806	0.1553	0.0471	0.391	-0.1069	-0.0965	0.0645	-0.1439	-0.0876	-0.0588	0.0493	-0.0038	-0.0175	0.1596	0.1107	0.1153	81.705	168.46	166.521
38	7.6079	-0.3238	1.5262	2.3784	0.3756	0.8264	0.2161	0.3076	0.0538	-0.0916	-0.2552	0.2242	0.0458	-0.2306	0.0391	0.0572	0.0069	-0.0217	0.2553	0.0638	0.1015	75.813	163.882	163.353
39	2.1895	-2.4686	3.5494	6.7257	-6.9449	10.1468	0.0891	0.1992	-0.0515	-0.2846	-0.0148	-0.0283	0.2663	0.097	-0.0743	0.1092	0.0084	0.084	0.1937	-0.0645	0.2094	96.713	2.349	-0.452
40	2.3468	-1.07	0.5469	2.2641	-0.0971	1.9934	0.1503	0.2031	-0.249	0.0819	-0.0937	-0.2569	0.1114	0.1038	-0.0567	0.0532	0.0068	-0.0226	0.0471	-0.0147	0.1267	96.262	9.342	18.029
41	1.5339	0.2834	-0.3294	1.4844	0.3646	1.68	0.0152	0.3879	-0.1477	-0.1064	-0.0302	-0.0918	0.0557	-0.234	0.015	0.0372	-0.0061	0.0314	0.1514	-0.0458	0.0505	85.693	7.889	8.242
42	3.9351	2.8656	-2.3043	4.1346	-2.299	2.8914	0.1538	0.3332	0.085	-0.0318	-0.1395	0.3635	-0.1161	-0.3636	-0.0143	0.0433	0.0327	-0.0102	0.2727	-0.0621	0.0738	74.409	12.739	9.752
43	1.2967	0.3161	-0.0494	1.9383	1.4315	1.7685	0.065	-0.0674	-0.1153	0.2303	-0.1969	0.2469	0.1543	-0.4342	0.1319	0.0552	-0.054	0.0497	0.2003	-0.0097	0.0809	73.429	11.672	23.986
44	1.6524	0.6916	0.1235	2.8508	0.1361	2.8229	0.1351	-0.0625	-0.0665	0.3121	-0.0233	-0.0197	-0.0163	-0.1827	-0.1118	0.0373	-0.005	-0.0037	0.0493	0.0217	0.0116	85.668	17.719	28.446
45	2.2164	1.8018	0.1219	5.4895	0.0923	2.4072	0.0835	0.1466	-0.1813	0.2576	0.0446	-0.2187	0.0883	-0.0891	-0.1281	0.0226	0.0113	-0.0025	0.0363	0.0139	0.0403	91.297	11.531	22.338
46	7.0448	7.4725	2.6181	10.8837	2.7836	1.6723	0.1744	0.1475	0.7501	0.0347	-0.2131	0.5445	-0.309	-0.1517	0.0388	0.3225	0.2054	0.1697	0.3426	0.0411	0.2781	68.43	59.646	25.544
47	2.3868	0.2838	0.7436	2.0994	0.8671	2.8535	0.053	0.2682	0.1847	-0.1151	-0.0757	0.0506	-0.304	-0.2504	0.0227	0.1372	0.0824	0.0939	0.1116	0.0521	0.0931	75.02	41.037	26.7
48	1.2002	-0.1098	-0.3354	1.9034	-0.1105	2.5261	0.2582	-0.0149	0.359	0.0993	-0.1646	0.0529	-0.6712	-0.2677	-0.0936	0.2719	0.0747	0.1346	0.1388	-0.0163	0.1625	72.879	50.506	37.379
49	4.7479	1.4866	-2.457	1.8305	-0.5122	3.1259	0.11	-0.4392	0.2429	0.1845	-0.2202	-0.1988	-0.2094	0.1427	0.1102	0.3208	-0.0087	0.082	0.1515	-0.0303	0.1804	77.076	48.635	48.913
50	2.0715	-0.4608	-0.4768	1.2132	0.5046	1.9725	0.166	-0.1845	0.0826	0.2183	-0.1454	0.0386	-0.0735	-0.1637	-0.0205	0.1269	-0.0302	0.0651	0.0873	0.002	0.0483	77.529	34.183	41.244
51	1.5691	0.1825	0.0499	1.6131	0.2554	1.6568	0.1342	-0.3873	0.091	0.4047	-0.0485	-0.3612	-0.1053	0.3161	-0.0858	0.2434	-0.1253	-0.0822	0.2239	0.0209	0.159	114.573	28.884	52.193
52	1.5663	-0.0351	0.5797	1.7898	-0.1773	1.5189	0.1997	-0.2741	-0.2251	0.3241	-0.0914	-0.1102	0.1646	-0.0138	-0.1083	0.1473	-0.0748	-0.0537	0.1105	0.0804	0.0789	102.319	15.388	47.714
53	2.0847	-1.7859	2.4609	10.243	-8.0818	9.0944	0.1681	0.092	-0.2798	-0.1908	-0.0568	0.0302	0.446	-0.0147	-0.1113	0.1268	-0.0099	0.064	0.2447	-0.0554	0.1165	103.911	8.885	-6.921
54	1.5368	-0.2077	0.3894	1.4234	0.0325	1.6215	0.1092	0.2068	-0.1202	-0.0353	-0.0431	0.0506	0.0416	-0.1072	-0.0661	0.0564	0.0197	0.043	0.1243	0.0265	0.0806	106.863	21.504	-0.544
55	1.477	-0.2922	-0.3061	1.2594	0.5845	1.3109	0.0556	0.12	0.0751	-0.0369	-0.0108	-0.1513	-0.0677	0.1221	-0.0448	0.0469	0.0241	0.0605	0.077	0.0591	0.1022	119.703	29.928	1.914
56	9.5786	7.4579	2.8228	8.824	3.1981	2.8911	-0.2036	-0.2458	0.4978	-0.0751	0.0321	0.5306	-0.1439	-0.3198	0.1715	0.2979	0.1522	0.1137	0.2138	0.0496	0.25	76.631	66.944	19.878
57	1.4239	0.344	0.1937	2.5668	1.1158	1.9495	0.0582	-0.1414	0.2422	0.2449	-0.0154	-0.0552	-0.2342	-0.1074	-0.0428	0.1769	0.0619	0.1174	0.0716	0.0573	0.2251	94.653	59.426	20.032
58	0.906	-0.0981	0.2066	2.2062	0.9326	2.8469	0.0857	0.0449	0.2607	-0.0182	-0.12	0.2047	-0.3418	-0.5417	0.0343	0.1666	0.1392	0.1344	0.1946	0.0968	0.2179	83.346	62.343	11.318
59	1.5664	-1.584	0.6555	1.6957	-1.1924	3.3775	0.2049	0.2103	0.0563	-0.1844	-0.1393	-0.0545	-0.1293	-0.3136	-0.0655	0.1458	0.1049	0.1464	0.1843	0.1256	0.1967	94.593	56.944	-0.594
60	3.4806	2.4187	-1.7835	6.8652	-2.297	5.3078	-0.0733	-0.1058	0.0966	-0.6885	-0.1543	0.0408	0.0072	-0.2312	0.2276	0.1664	0.1418	0.0826	0.1998	0.1129	0.1255	87.731	56.129	-2.313
61	4.2843	-1.7945	3.3084	6.5012	-4.9382	5.7693	0.1022	0.2493	0.0333	-0.6502	0.1167	0.0516	0.1862	-0.1021	-0.2189	0.1828	0.0525	0.1091	0.1482	0.0969	0.1308	97.565	52.21	-6.757
62	7.8913	4.1283	2.6355	5.052	4.142	3.5556	-0.122	0.5182	0.6089	-0.4651	0.3127	-0.1682	-0.3969	0.2812	-0.1907	0.1881	0.0028	0.1419	0.1925	0.1587	0.2676	110.351	55.273	-2.063
63	1.1709	-0.7614	0.1839	1.5887	-0.1248	0.9288	-0.0157	0.153	0.2966	-0.0915	0.0933	-0.1369	-0.2754	-0.045	-0.0775	0.1526	0.033	0.1071	0.0766	0.1004	0.1983	103.246	56.25	7.566
64	1.7058	0.6566	-0.3741	6.3653	-3.4869	3.1972	-0.0182	-0.0515	0.1259	-0.0002	0.0656	-0.0497	-0.1227	-0.1717	-0.0475	0.1047	0.0381	0.1064	0.0372	0.0311	0.1249	97.198	54.258	13.545
65	1.1732	-0.0078	0.4356	8.2125	-0.4322	0.6583	-0.0378	-0.0165	0.1384	0.1401	-0.0196	-0.0332	-0.1846	0.0628	0.0573	0.1731	0.0137	0.0792	0.1359	0.0239	0.2145	101.325	60.142	17.262
66	7.1057	-3.0753	-7.3253	2.2985	3.3675	10.9439	0.1059	-0.5804	-0.3607	0.1108	-0.1762	0.0215	-0.2147	0.3622	0.0702	0.3062	-0.1156	-0.1505	0.3282	0.0268	0.3691	131.21	36.514	50.055
67	1.6318	-0.6279	0.0188	2.4888	0.1538	1.6947	-0.0662	-0.3646	0.1417	0.4797	0.041	-0.3321	-0.1301	0.183	0.0251	0.1952	-0.0701	-0.0576	0.1594	-0.0202	0.1761	125.137	39.876	37.441
68	2.4224	0.4542	0.0982	2.7911	-0.2982	2.2912	0.117	-0.3393	0.1557	0.4937	-0.0762	-0.2694	-0.3677	0.1426	-0.0409	0.2616	-0.1131	-0.056	0.1455	-0.0609	0.1937	127.925	51.624	35.83
69	3.5556	3.7309	-1.2993	4.0241	-1.693	3.5295	0.1729	-0.2336	0.5683	0.3292	-0.1689	0.4524	-0.4092	-0.0452	-0.004	0.4709	-0.0178	-0.0621	0.18	-0.1792	0.3608	122.399	59.744	38.417
70	1.6729	0.1273	1.6338	1.8034	0.5229	2.266	-0.0623	0.0693	0.2711	-0.0779	0.0128	-0.1783	-0.4975	0.227	0.0494	0.323	-0.1212	0.0654	0.1074	-0.0084	0.2916	123.94	59.842	23.952
71	2.9409	0.4326	0.2087	1.2966	0.2103	1.7544	0.034	-0.0666	0.0928	0.1544	-0.0053	-0.1944	-0.1765	0.1331	-0.0287	0.0928	-0.0323	0.0253	0.0254	0.0037	0.1488	120.912	44.347	24.076
72	2.7709	-1.1119	-0.6483	2.6972	-1.4986	1.9075	0.166	0.3731	1.3378	-0.91	-0.383	-1.7639	0.5331	0.3106	0.2169	0.5209	0.09	0.7047	0.3739	0.013	1.8026	129.593	93.817	67.298
73	1.5699	1.7258	-1.1703	3.29	0.3049	2.7542	0.0762	-0.1496	-0.6661	0.0534	0.0058	-1.4094	-0.1413	0.4225	-0.0821	0.1669	-0.0102	0.1629	0.2989	-0.0088	1.8366	126.186	99.98	84.153
74	1.9377	0.4733	-0.2076	3.5289	-0.5247	1.3793	-0.183	0.2188	-0.2751	-0.9591	0.0571	-1.744	0.3684	0.2592	0.126	0.5281	-0.0154	0.5465	0.2917	-0.1065	1.3241	126.889	85.042	72.144
75	7.0368	-0.1088	3.2687	2.6387	-0.8632	6.0661	0.3613	0.2519	-0.4169	-0.0938	0.0227	-0.4705	0.6485	0.1995	-0.384	0.5534	0.0024	0.2282	0.1963	-0.0704	0.8931	121.69	73.847	74.134
76	2.048	-1.3181	-0.4865	3.0099	0.7264	2.3341	-0.0629	-0.1509	-0.1302	0.1151	0.1138	-1.5048	0.5413	0.3352	-0.0508	0.3022	0.0336	-0.0414	0.1918	-0.0121	1.2285	120.317	77.912	89.608
77	5.9728	-2.8855	0.0391	2.8186	-0.1262	2.372	-0.0632	-0.1335	0.3553	-0.1158	0.0448	-1.2473	0.1772	0.3046	0.0184	0.1988	-0.032	0.0761	0.1848	-0.0361	1.0104	122.869	91.635	85.601
78	12.0466	-9.4523	-2.9799	10.7235	2.7454	2.6861	-0.1046	0	-0.588	-0.0745	-0.0151	0.7849	0.1814	-0.4944	0.1196	0.3596	-0.2557	-0.0785	0.4179	0.0477	0.2132	74.059	70.284	89.332
79	1.1938	-0.2789	-0.4803	3.5251	1.0193	3.0212	0.0536	0.0312	-0.1434	-0.1355	-0.1109	-0.39	0.2694	-0.2806	0.0573	0.2256	-0.1386	-0.0738	0.1806	0.0398	0.1569	92.675	76.126	89.991
80	1.545	-0.4802	0.4966	2.9701	-0.2604	3.2296	-0.0092	-0.1299	-0.2297	0.3479	-0.044	0.3229	0.2661	-0.8146	0.0532	0.2686	-0.2001	-0.0313	0.4366	0.0359	0.1104	80.115	74.879	98.481
81	1.055	-0.1163	-0.7014	5.7358	-2.7427	2.976	-0.1361	-0.4014	0.1488	0.8613	0.157	0.078	-0.0398	-0.1002	-0.0209	0.5044	-0.1247	-0.149	0.3724	-0.0151	0.142	91.259	79.28	110.702
82	1.6829	0.2988	-0.6136	2.0756	-1.0085	1.4028	-0.0229	-0.5025	0.0144	1.0803	0.0452	-0.1125	-0.1486	-0.3552	-0.0223	0.7421	-0.1134	-0.1292	0.4719	0.0446	0.1147	89.222	82.175	114.543
83	5.3005	-0.6162	-0.2673	5.8466	1.9843	1.5283	0.2329	-0.6165	-0.4193	0.8927	-0.1052	-0.8957	0.4066	0.3563	-0.1278	0.6216	-0.0413	-0.375	0.4036	0.0966	0.444	106.892	79.729	113.524
84	1.0061	0.4501	-0.9936	3.3806	-1.0456	1.352	-0.1753	-0.1901	-0.0816	0.427	0.0573	-0.7443	0.1952	-0.0884	0.118	0.3283	-0.0801	-0.2204	0.2849	0.0815	0.2356	100.508	79.295	103.204
85	2.1919	0.0576	-0.5241	5.2588	-2.2466	2.4634	-0.1418	0.0002	-0.1444	0.0635	0.0494	-0.5251	0.2151	-0.1686	0.0924	0.2364	-0.0887	-0.1004	0.1718	0.0229	0.1141	97.121	78.534	95.111
86	2.0298	4.1931	-3.5906	13.3038	-9.055	9.874	-0.0935	0.0263	0.1879	0.6447	0.0087	-0.4522	-0.3042	-0.3415	0.0849	0.623	-0.0021	-0.2269	0.5247	-0.2326	0.5235	103.007	126.429	117.58
87	3.3666	-0.2234	-1.7037	3.1585	0.0798	2.3037	0.146	-0.4854	0.4055	0.7088	0.1509	-0.5457	-0.0334	0.0322	-0.2968	0.5104	-0.0447	-0.2686	0.2693	-0.1103	0.2884	103.107	107.937	111.111
88	3.5393	-0.0996	-0.6113	2.9625	1.2774	1.5246	0.1178	-0.4848	0.6556	0.7035	0.1899	-1.4312	-0.1286	0.3317	-0.3077	0.5487	-0.0607	-0.4529	0.3742	-0.2345	1.0705	116.889	116.225	112.121
89	2.4696	-0.4239	0.3677	2.5262	1.3477	2.7708	0.1766	-0.46	0.3086	0.8591	0.3197	-1.8488	0.3251	0.4746	-0.4963	0.5013	0.0001	-0.6506	0.3484	-0.1646	1.4935	123.665	99.785	108.944
90	2.4962	-0.5113	-0.0472	3.6623	-0.0145	2.1293	0.0043	-0.4129	0.1652	0.7781	0.1514	-0.9887	-0.0859	0.1198	-0.1557	0.3814	-0.0351	-0.3452	0.2204	-0.0724	0.4877	109.72	100.694	108.464
91	1.9571	0.8327	0.6593	2.3067	0.9192	2.5841	-0.0552	0.4545	-0.3731	-0.4463	0.1928	-0.7087	0.0817	0.4581	-0.1376	0.4032	0.037	0.315	0.2314	-0.0344	0.415	114.9	103.164	58.652
92	1.6723	-0.0772	0.2834	1.9773	0.0793	1.5329	-0.0792	0.1904	-0.0234	-0.2889	0.0548	-0.5501	-0.2441	0.3372	0.0243	0.405	-0.0403	0.303	0.2009	0.039	0.3374	116.88	116.724	60.384
93	1.5103	0.6764	-0.5527	1.8385	-0.4514	2.2218	-0.015	0.1742	0.103	-0.4144	0.0066	-0.2167	-0.3275	-0.145	0.0084	0.3635	0.0411	0.1503	0.1139	0.0453	0.1162	100.966	118.362	63.691
94	3.0906	0.0359	0.127	3.0714	-0.2909	1.0107	0.168	-0.3028	-0.4459	-0.1321	-0.1231	0.4424	0.418	-0.5331	-0.045	0.2653	-0.2013	-0.0822	0.4917	-0.0013	0.1528	70.775	81.961	79.971
95	2.2488	0.6934	-1.3606	2.822	1.6962	2.5982	0.0183	-0.087	0.0224	0.2614	-0.2161	0.2577	0.1681	-0.2483	0.1978	0.1153	-0.0027	-0.0186	0.4239	-0.0019	0.0534	74.254	99.219	85.202
96	1.7905	0.2669	-0.5662	2.2004	0.2655	2.7333	0.0147	0.0911	-0.1961	-0.2068	-0.0997	0.2009	0.4936	-0.5393	0.0849	0.2307	-0.1069	-0.0599	0.3272	-0.0441	0.0973	73.536	86.089	71.083
97	1.7329	-0.4659	1.5155	4.3535	-2.505	5.0485	0.0294	0.497	-0.2103	-0.5502	-0.0118	0.0546	0.1047	-0.2161	-0.0176	0.3825	-0.0355	-0.0594	0.3785	-0.0792	0.0457	78.666	87.298	59.84
98	2.1583	0.498	-0.0164	2.1708	0.7042	2.076	0.0325	0.2051	0.0573	-0.4938	-0.1031	0.1853	-0.1469	-0.4094	0.0706	0.2053	0.0528	-0.0446	0.245	0.0033	0.0238	79.229	102.1	67.293
99	2.0685	1.1403	-0.1161	4.4705	0.6486	1.9128	0.1948	-0.5594	0.438	0.8507	-0.0268	-0.3432	-0.4292	-0.0576	-0.168	0.4047	0.0304	-0.0841	0.3337	-0.1363	0.253	95.333	130.924	104.922
100	4.9256	2.1325	-0.9425	1.7352	0.7067	1.9217	0.2837	-0.199	-0.2919	-0.0553	-0.0592	-0.4796	-0.4527	0.1341	-0.2245	0.3224	-0.0163	-0.0554	0.1187	0.0362	0.3876	101.249	127.079	88.139
101	3.4187	0.5695	0.3753	2.5216	0.7826	1.6041	0.0717	-0.6315	0.3493	0.4214	-0.0941	-0.0227	-0.3137	-0.2621	0.0224	0.3234	0.0771	0.007	0.2773	-0.0996	0.1082	86.341	128.845	100.241
102	5.0465	-2.0408	1.1374	3.1639	-1.4939	4.3839	0.1831	-0.2227	0.2015	0.305	-0.2189	0.4219	-0.3055	-0.0862	0.0358	0.2226	0.1036	0.0464	0.3437	-0.1092	0.1382	74.905	124.474	98.04
103	2.8491	-0.371	-0.2808	2.2739	0.9042	1.3267	0.1014	0.1243	0.3008	-0.3212	-0.1333	0.2797	-0.3936	-0.4563	0.0319	0.2296	0.1566	-0.0141	0.2676	-0.0085	0.0931	78.851	123.025	82.675
104	2.8473	-0.3986	-0.4014	4.9289	-0.0937	1.586	0.0386	-0.1135	0.3094	-0.158	0.0619	-0.2225	-0.3154	-0.116	-0.1005	0.1888	0.0455	-0.0048	0.1358	-0.0041	0.0531	92.711	124.434	86.755
105	10.633	8.9047	-5.2667	8.7297	-5.2427	5.2144	0.0341	-0.3033	-0.0989	0.1399	-0.0822	-0.5163	0.1739	0.7396	0.0481	0.3601	0.227	-0.212	0.4754	-0.0767	0.5249	194.973	67.314	21.953
106	1.5879	0.0362	-0.5834	3.2442	-0.6173	2.3038	-0.0813	-0.2407	0.0056	0.5787	0.1212	-0.4104	0.2026	0.2589	-0.0398	0.2665	0.1422	-0.256	0.1773	-0.1236	0.3109	176.384	73.561	21.344
107	1.396	-0.1538	0.0311	2.5637	0.2905	1.8925	-0.0747	-0.0091	0.0484	0.1847	0.1202	-0.8725	0.2043	0.5666	-0.0455	0.1451	0.1419	-0.1719	0.2447	-0.1321	0.5176	185.421	71.206	10.45
108	1.6149	1.194	0.8765	4.2144	3.5065	3.7251	-0.1511	-0.4754	0.0311	-0.9423	0.1955	-0.6767	-0.4751	0.4467	-0.0444	0.4241	0.0856	0.2397	0.3435	-0.0409	0.6834	183.032	74.814	-1.235
109	6.1907	-2.771	-4.3169	6.0234	3.8559	4.9556	-0.0131	0.3412	0.1372	-0.7303	0.0899	-0.5068	-0.3461	-0.1467	-0.0768	0.196	0.0214	-0.0585	0.1349	-0.1057	0.2493	173.126	77.593	-6.222
110	0.6425	-1.4747	-0.4783	4.2029	0.6508	0.9761	0.0209	0.0779	-0.1191	-0.2189	-0.0457	0.0778	0.156	-0.0514	0.0248	0.1345	0.0309	-0.0859	0.1045	-0.1116	0.2207	165.602	74.614	5.705
111	0.7188	-0.4437	-0.9261	6.9049	1.4453	2.6141	-0.1582	-0.0839	-0.0258	0.394	0.1547	-0.2227	0.2009	0.2401	0.0034	0.1563	0.0865	-0.1635	0.1205	-0.0874	0.2459	171.659	75.022	16.453
112	2.2135	-1.9804	-1.3452	7.8078	4.1229	4.0949	0.108	0.2498	0.3271	-0.0585	-0.1528	-0.0471	-0.3953	0.1693	0.0447	0.7713	-0.0198	0.007	0.3374	0.0523	0.2064	164.151	120.502	-10.655
113	2.1454	-0.3543	-0.9642	2.2209	0.8734	2.6085	0.2493	0.1486	0.0068	-0.7651	-0.0793	-0.2384	-0.5348	0.223	-0.17	0.4577	0.0457	-0.0453	0.1205	-0.0536	0.1402	164.583	102.317	-2.519
114	2.0425	0.0664	-0.2072	2.1454	0.1806	2.1414	0.1785	0.3155	0.2183	-0.7675	-0.2556	0.2339	-0.7018	-0.0514	0.0771	0.5883	0.1563	-0.1824	0.1838	-0.0521	0.1415	153.184	110.888	-4.796
115	4.1708	2.0336	3.7041	5.4973	3.3703	6.5524	0.1169	0.0441	-0.0281	-0.3996	-0.2448	0.3069	-0.552	-0.3529	0.1279	0.2955	0.1326	-0.1811	0.1936	-0.1015	0.256	142.013	108.894	0.517
116	1.5965	-0.051	0.0761	1.953	-0.441	2.2779	0.0562	0.1539	-0.3351	-0.4722	-0.2773	0.5609	-0.0393	-0.4602	0.2211	0.2652	0.1311	-0.2674	0.233	-0.2181	0.355	142.298	94.59	0.793
117	1.2873	-0.5491	-0.1703	2.6543	0.827	2.4837	0.08	0.1354	-0.0973	-0.4359	-0.1243	0.0749	-0.2779	0.0235	0.0443	0.185	0.0784	-0.1258	0.0927	-0.0872	0.132	157.965	95.412	2.841
118	2.666	0.1854	-0.1051	1.9986	0.8829	2.4487	0.1335	-0.5215	0.2175	1.1655	-0.4215	0.8191	0.3167	-0.451	0.2879	0.844	-0.1883	0.3206	0.2271	-0.2254	0.5312	141.417	93.726	44.71
119	1.8789	-1.6716	-0.7145	2.8523	-0.8688	2.2216	-0.0041	0.1064	-0.2411	0.4129	-0.1157	0.5651	-0.2976	-0.1188	0.1199	0.282	-0.0312	0.101	0.1217	-0.2544	0.5922	143.519	97.864	26.735
120	1.0471	0.8389	-0.0997	2.5905	0.2912	1.6883	0.2122	-0.331	0.025	1.0839	-0.3259	0.4249	0.2615	-0.1367	0.1137	0.6355	-0.1419	0.1271	0.187	-0.1034	0.2863	144.068	84.626	40.977
121	3.7237	4.1003	-0.4578	5.3452	0.2422	0.7697	0.3108	-0.4197	-0.4796	0.6153	-0.3191	-0.4474	0.1675	0.1969	0.0083	0.7177	-0.102	-0.0162	0.2106	0.0055	0.3865	149.226	73.322	39.964
122	1.777	0.6933	-1.3568	1.6869	-0.6606	1.9858	0.0301	0.0852	-0.3273	0.3053	-0.2084	0.3217	0.4763	-0.1912	0.1783	0.4132	-0.0926	-0.0074	0.0972	-0.1418	0.3087	149.048	75.312	24.023
123	4.9715	2.0229	0.0498	2.4247	-0.3945	2.6204	0.1052	0.0636	0.0278	0.4951	-0.1791	0.4408	0.0212	-0.1987	0.0739	0.2499	-0.0158	0.0101	0.0787	-0.1322	0.2611	146.823	89.467	26.386
124	7.543	8.5904	-5.4889	14.0736	-6.8293	5.3299	0.1177	-0.4028	-0.1264	-0.1742	-0.2347	-0.3356	0.34	0.573	0.1169	0.3818	0.1208	-0.1793	0.5902	-0.0973	0.4598	201.68	74.96	27.968
125	1.3518	-0.4021	-0.5553	1.1022	-0.0881	2.0726	-0.0795	-0.0695	0.2664	0.1142	0.1222	-0.5226	0.1519	0.6206	-0.0427	0.3383	0.0758	-0.2888	0.4938	-0.1532	0.5772	194.706	93.167	26.481
126	1.49	-0.2649	0.4665	1.3781	0.8369	3.4093	0.0519	-0.1258	-0.206	0.2477	0.0722	-0.3045	0.5852	0.6097	-0.124	0.464	0.1956	-0.2939	0.515	-0.0905	0.4365	197.362	83.624	37.604
127	0.7142	-0.0613	1.2809	8.1583	-4.2148	4.4556	0.1099	-0.272	0.0575	0.3781	-0.3052	0.032	0.1238	-0.2241	0.1953	0.6218	0.1211	-0.187	0.4393	-0.0332	0.4562	184.537	87.927	49.069
128	2.2198	-1.524	0.7184	1.3399	-1.0964	2.027	-0.2747	-0.3198	0.3148	0.4758	0.0504	-0.3948	-0.2663	0.5306	0.2243	0.6006	0.0691	-0.4197	0.5274	-0.1779	0.4534	191.777	99.746	47.472
129	1.9323	-0.7371	0.407	1.9476	-0.6858	2.3587	0.0252	-0.029	0.1574	0.1008	-0.0384	-0.4246	-0.0942	0.5473	0.0132	0.3365	0.0348	-0.2962	0.3933	-0.1431	0.4372	191.101	100.608	32.929
130	1.7587	0.2414	1.5125	0.2519	-0.2017	3.3721	-0.1246	0.5134	0.4453	-0.1236	0.0223	0.0361	-0.8685	0.3582	0.1023	0.9559	-0.0686	0.1221	0.4272	0.1376	0.4635	172.742	126.023	0.473
131	4.7581	-0.9918	-0.4682	0.4694	-0.2819	4.3118	0.1696	0.1695	0.4689	-0.2163	-0.0656	-0.1287	-0.8279	0.1257	-0.104	0.5201	-0.0683	-0.0118	0.152	-0.0426	0.2686	168.088	124.125	17.881
132	3.3921	-0.9452	-0.3656	1.5726	0.6714	1.8543	0.0628	0.789	0.6154	-0.54	-0.0023	-0.4524	-0.9363	0.5701	-0.0605	0.7689	-0.28	0.1093	0.489	0.0835	0.4796	180.867	125.588	3.978
133	0.276	-0.4654	-0.6753	1.0063	0.3851	8.0196	0.1396	0.1206	0.2105	-0.4364	-0.0405	-0.4401	-0.0397	0.2953	-0.099	0.3778	-0.1716	0.0475	0.529	-0.0077	0.685	194.155	118.36	8.226
134	3.1077	0.4154	-0.6002	1.3437	-0.0939	2.3699	0.0935	-0.0963	0.2723	-0.0207	0.0315	-0.8162	-0.6426	0.8228	-0.125	0.3987	-0.2402	-0.0774	0.4923	-0.1522	0.7101	190.975	120.246	22.481
135	3.1374	1.5762	0.2851	5.4499	0.3938	3.662	0.0729	0.0176	0.4121	-0.1245	0.0803	-0.3975	-0.7545	0.5763	-0.1532	0.3415	-0.1531	-0.0152	0.2507	-0.0883	0.3151	176.965	121.72	19.273
136	1.4895	0.1473	0.1327	2.1175	-0.5461	3.8069	0.088	-0.2371	-0.0989	1.0985	-0.0553	0.3496	0.1628	-0.3797	-0.0327	0.8643	-0.0601	0.046	0.1777	-0.0637	0.1873	149.595	106.065	51.782
137	1.1758	-0.9158	-0.8463	3.3479	0.5543	0.677	-0.0831	-0.172	-0.19	0.8995	0.0125	-0.3273	0.2327	0.1966	0.0706	1.0566	0.0799	-0.3775	0.2267	-0.0721	0.2332	166.881	100.749	48.84
138	1.5999	0.2636	0.5171	2.4795	0.7372	3.2267	0.005	-0.2459	-0.0101	1.1122	-0.0873	0.3508	0.1041	-0.3719	0.0824	0.7879	-0.0286	0.0516	0.1708	-0.0628	0.1422	151.521	112.135	49.914
139	1.8236	0.0391	-1.5996	4.5108	2.1714	2.4854	0.1634	0.0046	0.0973	0.3984	-0.1397	0.0839	0.0158	-0.0711	-0.0237	0.4405	-0.0401	-0.1751	0.1712	-0.0702	0.145	161.906	124.537	43.83
140	2.7252	1.1778	0.5494	4.7028	3.1916	5.1827	-0.102	-0.0079	0.0106	0.1681	0.0717	-0.0197	-0.518	-0.1051	0.0303	0.4035	0.0228	-0.0635	0.1095	-0.0631	0.161	154.925	125.677	42.945
141	0.9545	-0.6702	-0.3674	2.866	2.0022	2.4509	-0.0247	-0.1181	0.2701	0.461	0.2374	-0.6011	-0.2462	0.3449	-0.2127	0.4587	-0.0408	-0.233	0.1925	-0.1063	0.2491	170.722	122.809	42.043
142	2.5026	0.0311	0.2502	4.1043	4.1085	7.0746	-0.0484	0.0206	0.0288	0.6097	-0.0293	-0.0661	0.2081	0.0151	0.0778	0.3729	-0.0166	-0.1628	0.0524	-0.0058	0.0891	165.531	110.483	42.033
143	1.9857	0.7657	0.9049	0.7212	-1.0106	9.8833	0.3196	-0.0751	-0.1252	0.4657	-0.0141	-0.1645	0.6288	0.6377	-0.3055	0.8545	0.1533	-0.3285	0.2187	-0.0768	0.1772	169.854	107.49	48.211

Refinement TLS group

ID	Refine-ID	Refine TLS-ID	Auth asym-ID	Auth seq-ID
1	X-RAY DIFFRACTION	1	A	27 - 80
2	X-RAY DIFFRACTION	2	A	81 - 113
3	X-RAY DIFFRACTION	3	A	114 - 148
4	X-RAY DIFFRACTION	4	A	149 - 193
5	X-RAY DIFFRACTION	5	A	194 - 216
6	X-RAY DIFFRACTION	6	A	217 - 301
7	X-RAY DIFFRACTION	7	A	302 - 342
8	X-RAY DIFFRACTION	8	B	26 - 58
9	X-RAY DIFFRACTION	9	B	59 - 120
10	X-RAY DIFFRACTION	10	B	121 - 238
11	X-RAY DIFFRACTION	11	B	239 - 255
12	X-RAY DIFFRACTION	12	B	256 - 342
13	X-RAY DIFFRACTION	13	C	27 - 80
14	X-RAY DIFFRACTION	14	C	81 - 113
15	X-RAY DIFFRACTION	15	C	114 - 184
16	X-RAY DIFFRACTION	16	C	185 - 226
17	X-RAY DIFFRACTION	17	C	227 - 301
18	X-RAY DIFFRACTION	18	C	302 - 342
19	X-RAY DIFFRACTION	19	D	27 - 120
20	X-RAY DIFFRACTION	20	D	121 - 193
21	X-RAY DIFFRACTION	21	D	194 - 216
22	X-RAY DIFFRACTION	22	D	217 - 273
23	X-RAY DIFFRACTION	23	D	274 - 342
24	X-RAY DIFFRACTION	24	E	25 - 58
25	X-RAY DIFFRACTION	25	E	59 - 113
26	X-RAY DIFFRACTION	26	E	114 - 216
27	X-RAY DIFFRACTION	27	E	217 - 342
28	X-RAY DIFFRACTION	28	F	27 - 58
29	X-RAY DIFFRACTION	29	F	59 - 113
30	X-RAY DIFFRACTION	30	F	114 - 147
31	X-RAY DIFFRACTION	31	F	148 - 193
32	X-RAY DIFFRACTION	32	F	194 - 216
33	X-RAY DIFFRACTION	33	F	217 - 238
34	X-RAY DIFFRACTION	34	F	239 - 255
35	X-RAY DIFFRACTION	35	F	256 - 273
36	X-RAY DIFFRACTION	36	F	274 - 301
37	X-RAY DIFFRACTION	37	F	302 - 323
38	X-RAY DIFFRACTION	38	F	324 - 342
39	X-RAY DIFFRACTION	39	G	27 - 58
40	X-RAY DIFFRACTION	40	G	59 - 113
41	X-RAY DIFFRACTION	41	G	114 - 193
42	X-RAY DIFFRACTION	42	G	194 - 216
43	X-RAY DIFFRACTION	43	G	217 - 273
44	X-RAY DIFFRACTION	44	G	274 - 301
45	X-RAY DIFFRACTION	45	G	302 - 342
46	X-RAY DIFFRACTION	46	H	26 - 58
47	X-RAY DIFFRACTION	47	H	59 - 113
48	X-RAY DIFFRACTION	48	H	114 - 193
49	X-RAY DIFFRACTION	49	H	194 - 216
50	X-RAY DIFFRACTION	50	H	217 - 342
51	X-RAY DIFFRACTION	51	I	27 - 148
52	X-RAY DIFFRACTION	52	I	149 - 342
53	X-RAY DIFFRACTION	53	J	26 - 58
54	X-RAY DIFFRACTION	54	J	59 - 148
55	X-RAY DIFFRACTION	55	J	149 - 342
56	X-RAY DIFFRACTION	56	K	27 - 58
57	X-RAY DIFFRACTION	57	K	59 - 113
58	X-RAY DIFFRACTION	58	K	114 - 175
59	X-RAY DIFFRACTION	59	K	176 - 193
60	X-RAY DIFFRACTION	60	K	194 - 216
61	X-RAY DIFFRACTION	61	K	217 - 238
62	X-RAY DIFFRACTION	62	K	239 - 255
63	X-RAY DIFFRACTION	63	K	256 - 301
64	X-RAY DIFFRACTION	64	K	302 - 323
65	X-RAY DIFFRACTION	65	K	324 - 342
66	X-RAY DIFFRACTION	66	L	26 - 58
67	X-RAY DIFFRACTION	67	L	59 - 148
68	X-RAY DIFFRACTION	68	L	149 - 193
69	X-RAY DIFFRACTION	69	L	194 - 216
70	X-RAY DIFFRACTION	70	L	217 - 273
71	X-RAY DIFFRACTION	71	L	274 - 342
72	X-RAY DIFFRACTION	72	M	27 - 80
73	X-RAY DIFFRACTION	73	M	81 - 113
74	X-RAY DIFFRACTION	74	M	114 - 193
75	X-RAY DIFFRACTION	75	M	194 - 216
76	X-RAY DIFFRACTION	76	M	217 - 301
77	X-RAY DIFFRACTION	77	M	302 - 342
78	X-RAY DIFFRACTION	78	N	27 - 58
79	X-RAY DIFFRACTION	79	N	59 - 116
80	X-RAY DIFFRACTION	80	N	117 - 175
81	X-RAY DIFFRACTION	81	N	176 - 193
82	X-RAY DIFFRACTION	82	N	194 - 238
83	X-RAY DIFFRACTION	83	N	239 - 255
84	X-RAY DIFFRACTION	84	N	256 - 301
85	X-RAY DIFFRACTION	85	N	302 - 342
86	X-RAY DIFFRACTION	86	O	27 - 58
87	X-RAY DIFFRACTION	87	O	59 - 113
88	X-RAY DIFFRACTION	88	O	114 - 216
89	X-RAY DIFFRACTION	89	O	217 - 283
90	X-RAY DIFFRACTION	90	O	284 - 342
91	X-RAY DIFFRACTION	91	P	27 - 113
92	X-RAY DIFFRACTION	92	P	114 - 216
93	X-RAY DIFFRACTION	93	P	217 - 342
94	X-RAY DIFFRACTION	94	Q	27 - 80
95	X-RAY DIFFRACTION	95	Q	81 - 113
96	X-RAY DIFFRACTION	96	Q	114 - 193
97	X-RAY DIFFRACTION	97	Q	194 - 216
98	X-RAY DIFFRACTION	98	Q	217 - 342
99	X-RAY DIFFRACTION	99	R	27 - 80
100	X-RAY DIFFRACTION	100	R	81 - 113
101	X-RAY DIFFRACTION	101	R	114 - 193
102	X-RAY DIFFRACTION	102	R	194 - 216
103	X-RAY DIFFRACTION	103	R	217 - 301
104	X-RAY DIFFRACTION	104	R	302 - 342
105	X-RAY DIFFRACTION	105	S	27 - 58
106	X-RAY DIFFRACTION	106	S	59 - 113
107	X-RAY DIFFRACTION	107	S	114 - 193
108	X-RAY DIFFRACTION	108	S	194 - 216
109	X-RAY DIFFRACTION	109	S	217 - 238
110	X-RAY DIFFRACTION	110	S	239 - 301
111	X-RAY DIFFRACTION	111	S	302 - 342
112	X-RAY DIFFRACTION	112	T	25 - 58
113	X-RAY DIFFRACTION	113	T	59 - 113
114	X-RAY DIFFRACTION	114	T	114 - 193
115	X-RAY DIFFRACTION	115	T	194 - 216
116	X-RAY DIFFRACTION	116	T	217 - 273
117	X-RAY DIFFRACTION	117	T	274 - 342
118	X-RAY DIFFRACTION	118	U	27 - 80
119	X-RAY DIFFRACTION	119	U	81 - 113
120	X-RAY DIFFRACTION	120	U	114 - 193
121	X-RAY DIFFRACTION	121	U	194 - 216
122	X-RAY DIFFRACTION	122	U	217 - 301
123	X-RAY DIFFRACTION	123	U	302 - 342
124	X-RAY DIFFRACTION	124	V	27 - 58
125	X-RAY DIFFRACTION	125	V	59 - 116
126	X-RAY DIFFRACTION	126	V	117 - 184
127	X-RAY DIFFRACTION	127	V	185 - 200
128	X-RAY DIFFRACTION	128	V	201 - 283
129	X-RAY DIFFRACTION	129	V	284 - 342
130	X-RAY DIFFRACTION	130	W	26 - 80
131	X-RAY DIFFRACTION	131	W	81 - 113
132	X-RAY DIFFRACTION	132	W	114 - 184
133	X-RAY DIFFRACTION	133	W	185 - 216
134	X-RAY DIFFRACTION	134	W	217 - 300
135	X-RAY DIFFRACTION	135	W	301 - 342
136	X-RAY DIFFRACTION	136	X	27 - 80
137	X-RAY DIFFRACTION	137	X	81 - 113
138	X-RAY DIFFRACTION	138	X	114 - 175
139	X-RAY DIFFRACTION	139	X	176 - 193
140	X-RAY DIFFRACTION	140	X	194 - 216
141	X-RAY DIFFRACTION	141	X	217 - 301
142	X-RAY DIFFRACTION	142	X	302 - 323
143	X-RAY DIFFRACTION	143	X	324 - 342

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