温度: 288 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 9 詳細: Crystallized in plastic sitting drop trays, 30 nl of protein (concentration 10 mg/mL) combined with 30 nl precipitant: 0.0425 M BICINE pH 9.0 0.0425 M Sodium chloride 8.5% v/v Polyethylene ...詳細: Crystallized in plastic sitting drop trays, 30 nl of protein (concentration 10 mg/mL) combined with 30 nl precipitant: 0.0425 M BICINE pH 9.0 0.0425 M Sodium chloride 8.5% v/v Polyethylene glycol monomethyl ether 550 7.5% v/v Glycerol Solution was equilibrated against a reservoir of 60% PEG 3350.
解像度: 3.8→30 Å / Cor.coef. Fo:Fc: 0.936 / Cor.coef. Fo:Fc free: 0.931 / SU B: 51.885 / SU ML: 0.6 / 交差検証法: THROUGHOUT / ESU R Free: 0.596 / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS