Evidence: assay for oligomerization, NMR relaxation experiments establish the overall correlation time is consistent with a monomeric species in solution
Method to determine structure: SAD / Resolution: 1.85→27.9 Å / Cor.coef. Fo:Fc: 0.955 / Cor.coef. Fo:Fc free: 0.936 / SU B: 5.762 / SU ML: 0.088 / Cross valid method: THROUGHOUT / ESU R: 0.187 / ESU R Free: 0.156 / Details: HYDROGENS HAVE BEEN USED IF PRESENT IN THE INPUT
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.22579
1927
10 %
RANDOM
Rwork
0.18918
-
-
-
obs
0.19283
17296
98.47 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å