A: Glial fibrillary acidic protein B: Glial fibrillary acidic protein C: Glial fibrillary acidic protein D: Glial fibrillary acidic protein E: Glial fibrillary acidic protein F: Glial fibrillary acidic protein G: Glial fibrillary acidic protein H: Glial fibrillary acidic protein
Resolution: 2.51→50 Å / Cor.coef. Fo:Fc: 0.886 / Cor.coef. Fo:Fc free: 0.853 / SU B: 31.932 / SU ML: 0.331 / Cross valid method: THROUGHOUT / ESU R Free: 0.407 / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.31086
1505
4.9 %
RANDOM
Rwork
0.2686
-
-
-
obs
0.27071
29465
84.61 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å
Displacement parameters
Biso mean: 57.085 Å2
Baniso -1
Baniso -2
Baniso -3
1-
-1.22 Å2
-0.88 Å2
1.74 Å2
2-
-
0.59 Å2
0.51 Å2
3-
-
-
0.51 Å2
Refinement step
Cycle: 1 / Resolution: 2.51→50 Å
Protein
Nucleic acid
Ligand
Solvent
Total
Num. atoms
6808
0
0
132
6940
Refine LS restraints
Refine-ID
Type
Dev ideal
Dev ideal target
Number
X-RAY DIFFRACTION
r_bond_refined_d
0.009
0.019
6834
X-RAY DIFFRACTION
r_bond_other_d
0.001
0.02
6792
X-RAY DIFFRACTION
r_angle_refined_deg
1.229
1.99
9180
X-RAY DIFFRACTION
r_angle_other_deg
1.725
3
15504
X-RAY DIFFRACTION
r_dihedral_angle_1_deg
3.593
5
812
X-RAY DIFFRACTION
r_dihedral_angle_2_deg
26.305
24.413
426
X-RAY DIFFRACTION
r_dihedral_angle_3_deg
16.268
15
1400
X-RAY DIFFRACTION
r_dihedral_angle_4_deg
14.458
15
102
X-RAY DIFFRACTION
r_chiral_restr
0.058
0.2
1066
X-RAY DIFFRACTION
r_gen_planes_refined
0.003
0.02
7782
X-RAY DIFFRACTION
r_gen_planes_other
0.002
0.02
1548
X-RAY DIFFRACTION
r_nbd_refined
X-RAY DIFFRACTION
r_nbd_other
X-RAY DIFFRACTION
r_nbtor_refined
X-RAY DIFFRACTION
r_nbtor_other
X-RAY DIFFRACTION
r_xyhbond_nbd_refined
X-RAY DIFFRACTION
r_xyhbond_nbd_other
X-RAY DIFFRACTION
r_metal_ion_refined
X-RAY DIFFRACTION
r_metal_ion_other
X-RAY DIFFRACTION
r_symmetry_vdw_refined
X-RAY DIFFRACTION
r_symmetry_vdw_other
X-RAY DIFFRACTION
r_symmetry_hbond_refined
X-RAY DIFFRACTION
r_symmetry_hbond_other
X-RAY DIFFRACTION
r_symmetry_metal_ion_refined
X-RAY DIFFRACTION
r_symmetry_metal_ion_other
X-RAY DIFFRACTION
r_mcbond_it
6.56
7.66
3272
X-RAY DIFFRACTION
r_mcbond_other
6.558
39.687
3271
X-RAY DIFFRACTION
r_scbond_it
7.297
6.191
3562
X-RAY DIFFRACTION
r_scangle_it
X-RAY DIFFRACTION
r_scangle_other
9.266
8.938
5105
X-RAY DIFFRACTION
r_rigid_bond_restr
9.928
3
6774
X-RAY DIFFRACTION
r_sphericity_free
X-RAY DIFFRACTION
r_sphericity_bonded
65.782
5
6750
LS refinement shell
Resolution: 2.508→2.573 Å / Total num. of bins used: 20
Rfactor
Num. reflection
% reflection
Rfree
0.317
44
-
Rwork
0.312
796
-
obs
-
-
29.98 %
+
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