A: Gamma-butyrolactone receptor protein H: Gamma-butyrolactone receptor protein B: Gamma-butyrolactone receptor protein C: Gamma-butyrolactone receptor protein D: Gamma-butyrolactone receptor protein E: Gamma-butyrolactone receptor protein F: Gamma-butyrolactone receptor protein G: Gamma-butyrolactone receptor protein
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.9686 Å / Relative weight: 1
Reflection
Resolution: 2.3→19.81 Å / Num. obs: 98807 / % possible obs: 99.7 % / Redundancy: 3.5 % / Net I/σ(I): 2.8
Reflection shell
Resolution: 2.3→2.42 Å / % possible obs: 96.1 % / Redundancy: 3.9 % / Rmerge(I) obs: 0.407 / Mean I/σ(I) obs: 2.8 / Rsym value: 0.481
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Processing
Software
Name
Version
Classification
REFMAC
5.6.0117
refinement
XDS
dataprocessing
Aimless
datascaling
Auto-Rickshaw
phasing
Refinement
Method to determine structure: SAD / Resolution: 2.3→19.81 Å / Cor.coef. Fo:Fc: 0.964 / Cor.coef. Fo:Fc free: 0.942 / SU B: 6.57 / SU ML: 0.155 / Cross valid method: THROUGHOUT / ESU R: 0.271 / ESU R Free: 0.22 / Details: HYDROGENS HAVE BEEN USED IF PRESENT IN THE INPUT
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.25258
992
1 %
RANDOM
Rwork
0.20401
-
-
-
obs
0.20451
97167
99.25 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å