- PDB-5uln: Synthesis of novel seleno ureido containing compounds as SLC-0111... -
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データベース: PDB / ID: 5uln
タイトル
Synthesis of novel seleno ureido containing compounds as SLC-0111 analogs. Investigations on carbonic anhydrases activity, glutathione peroxidase and X-ray crystallography
温度: 281 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 8.3 詳細: concentrated CA II at ~10 mg/mL was set up in SD-2 plates (Molecular Dimensions) with the following ratio of protein plus reservoir plus seeds: 250 nL + 225 nL + 25 nL. The plate was ...詳細: concentrated CA II at ~10 mg/mL was set up in SD-2 plates (Molecular Dimensions) with the following ratio of protein plus reservoir plus seeds: 250 nL + 225 nL + 25 nL. The plate was incubated at 8 C and the reservoir condition consisted of 2.9 M ammonium sulfate with 0.1 M Tris buffer at pH 8.3. Dry compound was added to the crystallization drop after crystals had formed and several days before data were c ollected.
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平均測定温度: 100 K
放射光源
由来: シンクロトロン / サイト: Australian Synchrotron / ビームライン: MX1 / 波長: 1.008 Å
検出器
タイプ: ADSC QUANTUM 210 / 検出器: CCD / 日付: 2016年6月7日
放射
プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
解像度: 1.35→41.6 Å / Cor.coef. Fo:Fc: 0.981 / Cor.coef. Fo:Fc free: 0.971 / SU B: 1.273 / SU ML: 0.024 / 交差検証法: THROUGHOUT / ESU R: 0.048 / ESU R Free: 0.046 / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS