: / positive regulation of single-species biofilm formation / negative regulation of elastin catabolic process / negative regulation of secondary metabolite biosynthetic process / quorum sensing / negative regulation of cell motility / regulation of DNA-templated transcription / DNA binding Similarity search - Function
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.97915 Å / Relative weight: 1
Reflection
Resolution: 2.4→40 Å / Num. obs: 13851 / % possible obs: 99.5 % / Redundancy: 3.4 % / Rmerge(I) obs: 0.087 / Net I/σ(I): 12.2
Reflection shell
Resolution: 2.4→2.49 Å / Redundancy: 3 % / Rmerge(I) obs: 0.489 / Mean I/σ(I) obs: 1.6 / % possible all: 97.8
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Processing
Software
Name
Version
Classification
REFMAC
5.7.0029
refinement
HKL-2000
datareduction
HKL-2000
datascaling
AutoSol
phasing
Refinement
Method to determine structure: SAD / Resolution: 2.4→39.93 Å / Cor.coef. Fo:Fc: 0.945 / Cor.coef. Fo:Fc free: 0.917 / SU B: 9.82 / SU ML: 0.232 / Cross valid method: THROUGHOUT / ESU R: 0.957 / ESU R Free: 0.296 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.25182
735
5 %
RANDOM
Rwork
0.22361
-
-
-
obs
0.22499
13851
99.78 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK