A: DNA (5'-D(*CP*CP*AP*AP*TP*AP*AP*TP*CP*GP*CP*GP*AP*TP*TP*AP*TP*TP*GP*G)-3') B: DNA (5'-D(*CP*CP*AP*AP*TP*AP*AP*TP*CP*GP*CP*GP*AP*TP*TP*AP*TP*TP*GP*G)-3') C: DNA (5'-D(*CP*CP*AP*AP*TP*AP*AP*TP*CP*GP*CP*GP*AP*TP*TP*AP*TP*TP*GP*G)-3') D: DNA (5'-D(*CP*CP*AP*AP*TP*AP*AP*TP*CP*GP*CP*GP*AP*TP*TP*AP*TP*TP*GP*G)-3')
A: DNA (5'-D(*CP*CP*AP*AP*TP*AP*AP*TP*CP*GP*CP*GP*AP*TP*TP*AP*TP*TP*GP*G)-3') B: DNA (5'-D(*CP*CP*AP*AP*TP*AP*AP*TP*CP*GP*CP*GP*AP*TP*TP*AP*TP*TP*GP*G)-3')
C: DNA (5'-D(*CP*CP*AP*AP*TP*AP*AP*TP*CP*GP*CP*GP*AP*TP*TP*AP*TP*TP*GP*G)-3') D: DNA (5'-D(*CP*CP*AP*AP*TP*AP*AP*TP*CP*GP*CP*GP*AP*TP*TP*AP*TP*TP*GP*G)-3')
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.97949 Å / Relative weight: 1
Reflection
Resolution: 3→40 Å / Num. obs: 5042 / % possible obs: 98.79 % / Redundancy: 5.9 % / Rmerge(I) obs: 0.14 / Net I/σ(I): 6.91
Reflection shell
Resolution: 3→3.24 Å / Rmerge(I) obs: 0.27 / Mean I/σ(I) obs: 2.45 / % possible all: 99.9
-
Processing
Software
Name
Version
Classification
REFMAC
5.8.0135
refinement
XDS
20141118
datareduction
XDS
20141118
datascaling
MOLREP
11.4.03
phasing
Refinement
Method to determine structure: MOLECULAR REPLACEMENT / Resolution: 3→40 Å / Cor.coef. Fo:Fc: 0.965 / Cor.coef. Fo:Fc free: 0.946 / SU B: 39.914 / SU ML: 0.342 / Cross valid method: THROUGHOUT / ESU R Free: 0.44 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.25019
156
3.1 %
RANDOM
Rwork
0.22582
-
-
-
obs
0.22662
4886
98.71 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK