Software | Name | Version | Classification |
---|
ADSC | Quantumdata collectionSOLVE | | phasingPHENIX | (phenix.refine: 1.7.2_869)refinementXDS | | data reductionXSCALE | | data scaling | | | | | | |
|
---|
Refinement | Method to determine structure: SIRAS / Resolution: 2.1→32.866 Å / SU ML: 0.44 / σ(F): 1.38 / Phase error: 23.22 / Stereochemistry target values: ML
| Rfactor | Num. reflection | % reflection | Selection details |
---|
Rfree | 0.2279 | 339 | 4.7 % | RANDOM |
---|
Rwork | 0.22 | - | - | - |
---|
obs | 0.2203 | 7214 | 99.24 % | - |
---|
all | - | 7257 | - | - |
---|
|
---|
Solvent computation | Shrinkage radii: 0.86 Å / VDW probe radii: 1.1 Å / Solvent model: FLAT BULK SOLVENT MODEL / Bsol: 49.946 Å2 / ksol: 0.37 e/Å3 |
---|
Displacement parameters | Biso mean: 46.54 Å2
| Baniso -1 | Baniso -2 | Baniso -3 |
---|
1- | 3.8036 Å2 | -0 Å2 | -0 Å2 |
---|
2- | - | 3.8036 Å2 | -0 Å2 |
---|
3- | - | - | -7.6071 Å2 |
---|
|
---|
Refinement step | Cycle: LAST / Resolution: 2.1→32.866 Å
| Protein | Nucleic acid | Ligand | Solvent | Total |
---|
Num. atoms | 627 | 0 | 0 | 38 | 665 |
---|
|
---|
Refine LS restraints | Refine-ID | Type | Dev ideal | Number |
---|
X-RAY DIFFRACTION | f_bond_d0.008 | 632 | X-RAY DIFFRACTION | f_angle_d1.073 | 838 | X-RAY DIFFRACTION | f_dihedral_angle_d18.412 | 252 | X-RAY DIFFRACTION | f_chiral_restr0.069 | 98 | X-RAY DIFFRACTION | f_plane_restr0.003 | 104 | | | | | |
|
---|
LS refinement shell | Resolution (Å) | Rfactor Rfree | Num. reflection Rfree | Rfactor Rwork | Num. reflection Rwork | Refine-ID | % reflection obs (%) |
---|
2.1-2.6458 | 0.2589 | 176 | 0.2341 | 3333 | X-RAY DIFFRACTION | 100 | 2.6458-32.8703 | 0.2196 | 163 | 0.2164 | 3542 | X-RAY DIFFRACTION | 99 |
|
---|
Refinement TLS params. | Method: refined / Origin x: 1.5593 Å / Origin y: 14.6822 Å / Origin z: 6.4597 Å
| 11 | 12 | 13 | 21 | 22 | 23 | 31 | 32 | 33 |
---|
T | 0.1993 Å2 | 0.0178 Å2 | 0.0282 Å2 | - | 0.3356 Å2 | 0.112 Å2 | - | - | 0.2675 Å2 |
---|
L | 3.3137 °2 | -2.1789 °2 | 1.8248 °2 | - | 3.2909 °2 | -1.2279 °2 | - | - | 4.0659 °2 |
---|
S | 0.0648 Å ° | -0.0089 Å ° | 0.0874 Å ° | 0.0616 Å ° | 0.0814 Å ° | 0.045 Å ° | -0.0286 Å ° | -0.1461 Å ° | -0.1143 Å ° |
---|
|
---|
Refinement TLS group | Selection details: all |
---|