DTV: DTT FROM PROTEIN BUFFER DERIVATISES CYSTEINE TO FORM (2R)-2-AZANIUMYL-3-[[(2S,3S)-2,3- ...DTV: DTT FROM PROTEIN BUFFER DERIVATISES CYSTEINE TO FORM (2R)-2-AZANIUMYL-3-[[(2S,3S)-2,3-DIHYDROXY-4-SULFANYL] PROPANOATE
配列の詳細
CODON OPTIMISED SEQUENCE, SIX MUTATIONS INTRODUCED TO ENHANCE CRYSTALLISABILITY ...CODON OPTIMISED SEQUENCE, SIX MUTATIONS INTRODUCED TO ENHANCE CRYSTALLISABILITY K617A,Q618A,K619A,E688A,K689A, K690A
解像度: 2→27.35 Å / Cor.coef. Fo:Fc: 0.955 / Cor.coef. Fo:Fc free: 0.94 / SU B: 8.39 / SU ML: 0.1 / 交差検証法: THROUGHOUT / ESU R: 0.2 / ESU R Free: 0.17 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.24139
1961
5 %
RANDOM
Rwork
0.20356
-
-
-
obs
0.20548
37234
98.62 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: BABINET MODEL WITH MASK