ADDITIONAL GLY -1 AND SER 0 ARE DERIVED FROM FUSION TAG CLEAVAGE. MET 1 IS MISSING DUE TO INSERTION ...ADDITIONAL GLY -1 AND SER 0 ARE DERIVED FROM FUSION TAG CLEAVAGE. MET 1 IS MISSING DUE TO INSERTION INTO THE EXPRESSION VECTOR PGEX-4T-1. CYS 2 IS THE FIRST RESIDUE OF THE WT PROTEIN.
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2.58 Å3/Da / 溶媒含有率: 52.34 % / 解説: NONE
結晶化
pH: 8.5 詳細: 16% (W/V) PEG 4000, 0.1 M TRIS/HCL, PH 8.5, 0.2 M SODIUM ACETATE
解像度: 2.9→46.91 Å / Cor.coef. Fo:Fc: 0.856 / Cor.coef. Fo:Fc free: 0.83 / SU B: 19.092 / SU ML: 0.346 / 交差検証法: THROUGHOUT / ESU R Free: 0.437 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. RESIDUES -1 TO 37, 175-17, 428-456, 506-541 HAVE NOT BEEN MODELLED BECAUSE DISORDERED.
Rfactor
反射数
%反射
Selection details
Rfree
0.28805
1394
5 %
RANDOM
Rwork
0.26528
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obs
0.26642
26474
96.67 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK