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- PDB-436d: THE DICKERSON-DREW B-DNA DODECAMER REVISITED-AT ATOMIC RESOLUTION -
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Open data
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Basic information
Entry | Database: PDB / ID: 436d | ||||||||||||||||||
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Title | THE DICKERSON-DREW B-DNA DODECAMER REVISITED-AT ATOMIC RESOLUTION | ||||||||||||||||||
![]() | 5'-D(*![]() DNA / B-DNA DODECAMER / HIGH RESOLUTION | Function / homology | DNA / DNA (> 10) | ![]() Method | ![]() ![]() ![]() Tereshko, V. / Minasov, G. / Egli, M. | ![]() Journal: J.Am.Chem.Soc. / Year: 1999 | Title: The Dickerson-Drew B-DNA Dodecamer Revisited-At Atomic Resolution Authors: Tereshko, V. / Minasov, G. / Egli, M. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 45.4 KB | Display | ![]() |
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PDB format | ![]() | 32.4 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Arichive directory | ![]() ![]() | HTTPS FTP |
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-Related structure data
Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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Unit cell |
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Components
#1: DNA chain | Mass: 3681.383 Da / Num. of mol.: 2 / Source method: obtained synthetically #2: Chemical | ChemComp-MG / #3: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 2.08 Å3/Da / Density % sol: 40.93 % | ||||||||||||||||||||||||||||||||||||
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Crystal grow | Temperature: 295 K / Method: vapor diffusion, sitting drop / pH: 7 Details: SODIUM CACODYLATE, MAGNESIUM ACETATE, SPERMINE; PRECIPITANT: MPD, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K | ||||||||||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS pH: 6.9 | ||||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 100 K |
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Diffraction source | Source: ![]() ![]() ![]() |
Detector | Type: MARRESEARCH / Detector: CCD / Date: Feb 2, 1998 |
Radiation | Monochromator: MIRRORS / Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength: 0.978 Å / Relative weight: 1 |
Reflection | Resolution: 1.1→30 Å / Num. all: 26878 / Num. obs: 26878 / % possible obs: 99.5 % / Observed criterion σ(F): 0 / Observed criterion σ(I): 0 / Redundancy: 5.2 % / Rmerge(I) obs: 0.066 |
Reflection shell | Resolution: 1.1→1.2 Å / Rmerge(I) obs: 0.154 / % possible all: 99.7 |
Reflection | *PLUS Highest resolution: 1.1 Å |
Reflection shell | *PLUS Highest resolution: 1.1 Å / Lowest resolution: 1.2 Å / % possible obs: 99.7 % / Num. unique obs: 6060 / Mean I/σ(I) obs: 8.5 |
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Processing
Software |
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Refinement | Resolution: 1.1→20 Å / σ(F): 0 / σ(I): 0
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Refinement step | Cycle: LAST / Resolution: 1.1→20 Å
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Refine LS restraints |
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Software | *PLUS Name: SHELXL-97 / Classification: refinement | |||||||||||||||||||||||||||||||||
Refinement | *PLUS Highest resolution: 1.1 Å / Lowest resolution: 20 Å / σ(F): 0 / % reflection Rfree: 10 % / Rfactor Rfree: 0.21 / Rfactor Rwork: 0.162 | |||||||||||||||||||||||||||||||||
Solvent computation | *PLUS | |||||||||||||||||||||||||||||||||
Displacement parameters | *PLUS | |||||||||||||||||||||||||||||||||
Refine LS restraints | *PLUS Type: s_angle_d / Dev ideal: 0.02 | |||||||||||||||||||||||||||||||||
LS refinement shell | *PLUS Highest resolution: 1.1 Å / Lowest resolution: 1.2 Å / Rfactor obs: 0.22 |