Mass: 18.015 Da / Num. of mol.: 105 / Source method: isolated from a natural source / Formula: H2O
Sequence details
FIRST METHIONINE CLEAVED. THE NUMBERING IS ACCORDING TO THE MATURE PROTEIN AND IS SHIFTED BY ONE ...FIRST METHIONINE CLEAVED. THE NUMBERING IS ACCORDING TO THE MATURE PROTEIN AND IS SHIFTED BY ONE COMPARED TO THE DEPOSITED ONE
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 2.8 Å3/Da / Density % sol: 56.2 % / Description: NONE
Crystal grow
pH: 6.5 Details: 30MM MGCL2, 30MM CACL2, 100MM MES/IMIDAZOLE PH 6.5, 12.5 % OF MPD, PEG1K AND PEG3350
Resolution: 1.5→36.2 Å / Cor.coef. Fo:Fc: 0.973 / Cor.coef. Fo:Fc free: 0.965 / SU B: 1.97 / SU ML: 0.034 / Cross valid method: THROUGHOUT / ESU R: 0.062 / ESU R Free: 0.057 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES REFINED INDIVIDUALLY. DISORDERED SIDE CHAIN WERE MODELED STEREOCHEMICALLY
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.1656
892
5.1 %
RANDOM
Rwork
0.13357
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obs
0.1351
16628
99.01 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK