PDB-3u41: Crystal structure of Escherichia coli DmsD in space group P212121

Basic information

• Entry: Database: PDB / ID: 3u41
• Title: Crystal structure of Escherichia coli DmsD in space group P212121
• Components: Twin-arginine leader-binding protein dmsD
• Keywords: CHAPERONE / TorD-like DmsD / Chaperone Translocation TorD-like TAT / preDmsA / Cytosol

Function / homology

Function:

signal sequence binding / : / protein maturation / plasma membrane / cytoplasm

Domain/homology:

Tat proofreading chaperone DmsD / Tat proofreading chaperone DmsD-type / : / TorD-like / TorD-like / DMSO/Nitrate reductase chaperone / TorD-like superfamily / Nitrate reductase delta subunit / Orthogonal Bundle / Mainly Alpha

Component:

DI(HYDROXYETHYL)ETHER / Tat proofreading chaperone DmsD

• Biological species: Escherichia coli (E. coli)
• Method: X-RAY DIFFRACTION / SYNCHROTRON / MOLECULAR REPLACEMENT / Resolution: 2.5 Å
• Authors: Stevens, C.M. / Paetzel, M.

History

Deposition	Oct 6, 2011	Deposition site: RCSB / Processing site: RCSB
Revision 1.0	Feb 6, 2013	Provider: repository / Type: Initial release
Revision 1.1	Nov 8, 2017	Group: Refinement description / Category: software Item: _software.classification / _software.contact_author / _software.contact_author_email / _software.date / _software.language / _software.location / _software.name / _software.type / _software.version
Revision 1.2	Sep 13, 2023	Group: Data collection / Database references / Derived calculations / Refinement description Category: chem_comp_atom / chem_comp_bond / database_2 / pdbx_initial_refinement_model / struct_ref_seq_dif / struct_site Item: _database_2.pdbx_DOI / _database_2.pdbx_database_accession / _struct_ref_seq_dif.details / _struct_site.pdbx_auth_asym_id / _struct_site.pdbx_auth_comp_id / _struct_site.pdbx_auth_seq_id

Assembly

Deposited unit

A: Twin-arginine leader-binding protein dmsD

B: Twin-arginine leader-binding protein dmsD

C: Twin-arginine leader-binding protein dmsD

D: Twin-arginine leader-binding protein dmsD

E: Twin-arginine leader-binding protein dmsD

F: Twin-arginine leader-binding protein dmsD

G: Twin-arginine leader-binding protein dmsD

H: Twin-arginine leader-binding protein dmsD

hetero molecules

Summary:

• 194 kDa, 8 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	193,587	57
Polymers	189,166	8
Non-polymers	4,421	49
Water	8,251	458

1

A: Twin-arginine leader-binding protein dmsD

hetero molecules

Summary:

• defined by author&software
• 24.3 kDa, 1 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	24,294	8
Polymers	23,646	1
Non-polymers	649	7
Water	18	1

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

2

B: Twin-arginine leader-binding protein dmsD

hetero molecules

Summary:

• defined by author&software
• 24.2 kDa, 1 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	24,228	7
Polymers	23,646	1
Non-polymers	583	6
Water	18	1

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

3

C: Twin-arginine leader-binding protein dmsD

hetero molecules

Summary:

• defined by author&software
• 24.5 kDa, 1 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	24,540	11
Polymers	23,646	1
Non-polymers	894	10
Water	18	1

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

4

D: Twin-arginine leader-binding protein dmsD

hetero molecules

Summary:

• defined by author&software
• 24.6 kDa, 1 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	24,581	11
Polymers	23,646	1
Non-polymers	935	10
Water	18	1

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

5

E: Twin-arginine leader-binding protein dmsD

hetero molecules

Summary:

• defined by author&software
• 24.4 kDa, 1 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	24,383	9
Polymers	23,646	1
Non-polymers	737	8
Water	18	1

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

6

F: Twin-arginine leader-binding protein dmsD

hetero molecules

Summary:

• defined by author&software
• 24.2 kDa, 1 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	24,177	8
Polymers	23,646	1
Non-polymers	531	7
Water	18	1

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

7

G: Twin-arginine leader-binding protein dmsD

Summary:

• defined by author&software
• 23.6 kDa, 1 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	23,646	1
Polymers	23,646	1
Non-polymers	0	0
Water	18	1

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

8

H: Twin-arginine leader-binding protein dmsD

hetero molecules

Summary:

• defined by author&software
• 23.7 kDa, 1 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	23,738	2
Polymers	23,646	1
Non-polymers	92	1
Water	18	1

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

Unit cell

Length a, b, c (Å)	94.275, 96.221, 210.243
Angle α, β, γ (deg.)	90.00, 90.00, 90.00
Int Tables number	19
Space group name H-M	P212121

Components

Protein , 1 types, 8 molecules A B C D E F G H

#1: Protein

A B C D E F G H
Twin-arginine leader-binding protein dmsD

Details:

Mass: 23645.797 Da / Num. of mol.: 8
Source method: isolated from a genetically manipulated source
Source: (gene. exp.) Escherichia coli (E. coli) / Strain: K12 / Gene: b1591, dmsD, JW5262, ynfI / Plasmid: pET-15b / Production host: Escherichia coli (E. coli) / Strain (production host): BL21(DE3) / References: UniProt: P69853

Non-polymers , 6 types, 507 molecules

#2: Chemical

A-301 A-302 A-303 A-304 A-305 A-306 B-301 B-302 B-303 B-304 B-305 C-301 C-302 C-303 C-304 C-305 C-306 C-307 C-308 D-301 ...
ChemComp-GOL / GLYCEROL / GLYCERIN / PROPANE-1,2,3-TRIOL

Details:

Mass: 92.094 Da / Num. of mol.: 42 / Source method: obtained synthetically / Formula: C₃H₈O₃

#3: Chemical

A-307 ChemComp-SO4 / SULFATE ION

Details:

Mass: 96.063 Da / Num. of mol.: 1 / Source method: obtained synthetically / Formula: SO₄

#4: Chemical

B-306 C-309 ChemComp-TRS / 2-AMINO-2-HYDROXYMETHYL-PROPANE-1,3-DIOL / TRIS BUFFER

Details:

Mass: 122.143 Da / Num. of mol.: 2 / Source method: obtained synthetically / Formula: C₄H₁₂NO₃ / Comment: pH buffer*YM

#5: Chemical

C-310 F-306 F-307 ChemComp-CL / CHLORIDE ION

Details:

Mass: 35.453 Da / Num. of mol.: 3 / Source method: obtained synthetically / Formula: Cl

#6: Chemical

D-310 ChemComp-PEG / DI(HYDROXYETHYL)ETHER

Details:

Mass: 106.120 Da / Num. of mol.: 1 / Source method: obtained synthetically / Formula: C₄H₁₀O₃

#7: Water

ChemComp-HOH / water

Details:

Mass: 18.015 Da / Num. of mol.: 458 / Source method: isolated from a natural source / Formula: H₂O

Experimental details

Experiment

• Experiment: Method: X-RAY DIFFRACTION / Number of used crystals: 1

Sample preparation

• Crystal: Density Matthews: 2.5 ų/Da / Density % sol: 50.82 %
• Crystal grow: Temperature: 294 K / Method: vapor diffusion, hanging drop / pH: 6.5 ; Details: 1.25M Ammonium Sulfate, 11% (v/v) Glycerol, 0.1M Bis-Tris pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K

Data collection

• Diffraction: Mean temperature: 100 K
• Diffraction source: Source: SYNCHROTRON / Site: CLSI / Beamline: 08B1-1 / Wavelength: 1.105 Å
• Detector: Type: RAYONIX MX300HE / Detector: CCD / Date: May 26, 2011; Details: DCM with cryo-cooled 1st crystal sagittally bent 2nd crystal followed by vertically focusing mirror.
• Radiation: Monochromator: double crystal monochromator (DCM) / Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
• Radiation wavelength: Wavelength: 1.105 Å / Relative weight: 1
• Reflection: Resolution: 2.12→50 Å / Num. obs: 63206 / % possible obs: 98.4 % / Observed criterion σ(F): 2 / Observed criterion σ(I): -3 / Redundancy: 8.6 % / R_merge(I) obs: 0.109 / Net I/σ(I): 12.4

Reflection shell

Resolution (Å)	Redundancy (%)	Rmerge(I) obs	Diffraction-ID	% possible all
2.12-2.2	5.2	0.981	1	94.4
2.2-2.28	7.6	0.889	1	98.5
2.28-2.39	8.5	0.642	1	98.4
2.39-2.51	8.7	0.489	1	98.3
2.51-2.67	8.6	0.354	1	98.1
2.67-2.88	8.6	0.256	1	98.1
2.88-3.17	8.6	0.176	1	99.1
3.17-3.62	9	0.115	1	99.8
3.62-4.57	9.8	0.087	1	99.6
4.57-50	10.5	0.069	1	99.6

Processing

Software

Name	Version	Classification	NB
DENZO		data reduction
SCALEPACK		data scaling
REFMAC		refinement
PDB_EXTRACT	3.1	data extraction
MxDC		data collection
HKL-2000		data reduction
PHASES		phasing

Refinement

Method to determine structure: MOLECULAR REPLACEMENT
Starting model: 3EFP(a)

3efp

Resolution: 2.5→48.6 Å / Cor.coef. F_o:F_c: 0.922 / Cor.coef. F_o:F_c free: 0.892 / Occupancy max: 1 / Occupancy min: 0.38 / SU B: 19.273 / SU ML: 0.246 / SU R Cruickshank DPI: 0.8727 / Cross valid method: THROUGHOUT / ESU R: 1.084 / ESU R Free: 0.338 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS

	Rfactor	Num. reflection	% reflection	Selection details
Rfree	0.27068	3180	5 %	RANDOM
Rwork	0.2298	-	-	-
obs	0.23189	59979	94.1 %	-
all	-	107698	-	-

• Solvent computation: Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK

Displacement parameters

B_iso mean: 49.563 Ų

	Baniso -1	Baniso -2	Baniso -3
1-	4.01 Å2	-0 Å2	0 Å2
2-	-	-1.38 Å2	-0 Å2
3-	-	-	-2.63 Å2

Refinement step

Cycle: LAST / Resolution: 2.5→48.6 Å

	Protein	Nucleic acid	Ligand	Solvent	Total
Num. atoms	13167	0	282	458	13907

Refine LS restraints

Refine-ID	Type	Dev ideal	Dev ideal target	Number
X-RAY DIFFRACTION	r_bond_refined_d	0.005	0.019	13887
X-RAY DIFFRACTION	r_bond_other_d	0.001	0.02	12825
X-RAY DIFFRACTION	r_angle_refined_deg	0.903	1.946	18924
X-RAY DIFFRACTION	r_angle_other_deg	0.71	3	29442
X-RAY DIFFRACTION	r_dihedral_angle_1_deg	4.442	5	1632
X-RAY DIFFRACTION	r_dihedral_angle_2_deg	29.671	23.754	658
X-RAY DIFFRACTION	r_dihedral_angle_3_deg	13.168	15	2063
X-RAY DIFFRACTION	r_dihedral_angle_4_deg	14.816	15	78
X-RAY DIFFRACTION	r_chiral_restr	0.048	0.2	2021
X-RAY DIFFRACTION	r_gen_planes_refined	0.003	0.021	15524
X-RAY DIFFRACTION	r_gen_planes_other	0.001	0.02	3398
X-RAY DIFFRACTION	r_nbd_refined
X-RAY DIFFRACTION	r_nbd_other
X-RAY DIFFRACTION	r_nbtor_refined
X-RAY DIFFRACTION	r_nbtor_other
X-RAY DIFFRACTION	r_xyhbond_nbd_refined
X-RAY DIFFRACTION	r_xyhbond_nbd_other
X-RAY DIFFRACTION	r_metal_ion_refined
X-RAY DIFFRACTION	r_metal_ion_other
X-RAY DIFFRACTION	r_symmetry_vdw_refined
X-RAY DIFFRACTION	r_symmetry_vdw_other
X-RAY DIFFRACTION	r_symmetry_hbond_refined
X-RAY DIFFRACTION	r_symmetry_hbond_other
X-RAY DIFFRACTION	r_symmetry_metal_ion_refined
X-RAY DIFFRACTION	r_symmetry_metal_ion_other
X-RAY DIFFRACTION	r_mcbond_it	0.122	1.5	8212
X-RAY DIFFRACTION	r_mcbond_other
X-RAY DIFFRACTION	r_mcangle_it	0.236	2	13184
X-RAY DIFFRACTION	r_scbond_it	0.366	3	5690
X-RAY DIFFRACTION	r_scangle_it	0.611	4.5	5753
X-RAY DIFFRACTION	r_rigid_bond_restr
X-RAY DIFFRACTION	r_sphericity_free
X-RAY DIFFRACTION	r_sphericity_bonded

LS refinement shell

Resolution: 2.498→2.563 Å / Total num. of bins used: 20

	Rfactor	Num. reflection	% reflection
Rfree	0.358	217	-
Rwork	0.288	4406	-
obs	-	-	95.05 %

Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°2)	L12 (°2)	L13 (°2)	L22 (°2)	L23 (°2)	L33 (°2)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å2)	T12 (Å2)	T13 (Å2)	T22 (Å2)	T23 (Å2)	T33 (Å2)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	23.4453	6.0381	9.2733	2.9844	-3.0277	25.2309	0.3861	-1.2728	0.7204	0.5408	-0.2354	0.1128	-1.2849	-1.1009	-0.1507	0.4006	-0.039	-0.0431	0.3765	-0.0285	0.6303	25.4525	35.6481	50.2705
2	0.748	0.3302	-0.7823	0.6045	0.9048	5.1146	0.0531	-0.0171	-0.0565	-0.1453	-0.1209	0.0693	-0.1902	-0.1339	0.0679	0.2841	-0.0437	-0.0063	0.4105	-0.0176	0.5725	27.5072	23.9124	37.7409
3	4.6272	0.5256	1.8466	15.4399	-4.2723	8.2282	0.0104	0.2646	-0.2211	0.2456	-0.0967	0.2233	-0.3874	-0.1395	0.0863	0.3328	-0.0581	0.0476	0.4414	-0.0502	0.4318	24.3897	20.2735	26.6117
4	2.0002	-0.593	5.544	13.6916	2.7464	16.826	-0.1008	-0.098	-0.0408	0.0202	0.1422	0.1881	-0.3838	-0.2897	-0.0413	0.3768	-0.012	0.0962	0.3637	0.038	0.4374	24.6764	34.1436	31.1463
5	19.9011	-8.5334	3.9795	3.6694	-1.7237	0.8327	0.0847	0.3731	-0.1648	0.0268	-0.0864	0.0916	-0.1165	-0.0132	0.0017	0.6705	0.0805	0.0074	0.5152	0.0309	0.4898	29.7641	34.1252	24.0311
6	5.9103	-1.2377	3.6604	0.6831	-1.9971	5.9583	-0.1598	0.2806	-0.2409	-0.1223	0.1594	-0.0373	0.1421	-0.4338	0.0004	0.471	-0.1111	0.098	0.4887	-0.1234	0.5701	36.3605	16.8261	21.0143
7	2.5704	-0.4105	0.091	0.4489	1.572	6.6348	0.0397	0.3071	-0.0135	-0.0026	-0.022	0.0402	0.0426	0.1628	-0.0178	0.3132	-0.0838	0.0278	0.3931	-0.0148	0.5128	44.5166	13.8618	33.337
8	3.8834	8.6784	1.332	19.4791	3.9356	11.524	0.2695	-0.0022	-0.5282	0.6036	0.068	-1.1796	-0.2337	0.824	-0.3375	0.1816	-0.0153	0.0551	0.421	0.0155	0.6056	51.5185	18.8588	43.9967
9	17.5583	-0.4919	-6.0722	5.1243	3.3122	7.7547	0.0018	-0.164	0.298	0.1045	0.4043	-0.596	-0.1587	0.4215	-0.4061	0.2857	-0.0369	-0.0002	0.4454	-0.0019	0.4037	46.463	13.7483	47.5576
10	9.7073	3.5934	-1.4954	1.3767	0.0274	8.9517	0.1848	-0.0884	-0.3219	0.0789	-0.076	-0.1512	0.2541	0.1977	-0.1087	0.2612	-0.0164	0.0601	0.3756	-0.0594	0.5527	38.1334	17.1563	54.1702
11	17.4756	-1.9973	5.7111	16.2196	-6.5632	36.3722	0.091	0.1953	-0.1887	0.6606	0.1369	-0.4059	-0.0727	0.8346	-0.2279	0.2817	0.001	0.0215	0.4424	0.0355	0.4309	33.25	17.2135	58.2109
12	24.7335	-16.4049	-15.2874	31.5041	13.4493	15.1213	-0.6668	-0.8125	-1.5365	1.4769	-0.0878	0.0669	1.1791	1.1229	0.7546	0.3324	-0.0791	0.0028	0.4082	0.0806	0.602	29.9452	11.7269	47.8105
13	14.1839	14.0881	9.9698	38.0385	24.6938	16.1075	0.407	-0.026	-0.8851	0.123	-0.6849	0.5691	0.0995	-0.41	0.278	0.3452	-0.0089	0.0099	0.476	0.0163	0.4486	37.3254	8.3189	44.4003
14	9.7665	-3.5205	-4.9817	2.2401	3.0192	4.0835	-0.1599	-0.0443	-0.0791	-0.0032	0.0761	0.0781	0.0016	0.0881	0.0839	0.3015	-0.0202	0.0555	0.3885	-0.0039	0.4993	31.7273	20.3358	44.1201
15	17.6353	7.9209	3.9373	9.3034	2.9379	4.7009	0.2898	-0.599	-0.1015	0.1207	-0.2324	0.0714	0.2926	0.0988	-0.0575	0.2889	0.004	0.0234	0.4099	-0.0103	0.4316	26.05	25.7679	52.7347
16	1.2165	-0.2208	-3.0113	2.0897	1.0986	8.133	-0.0397	-0.0393	-0.12	0.2527	-0.0445	0.0099	-0.2158	-0.0257	0.0842	0.3237	-0.0286	0.0198	0.425	-0.0126	0.5731	38.6028	26.6035	48.5098
17	4.8371	-1.3797	0.6067	0.4857	0.7489	10.2311	-0.001	0.4119	0.3302	0.0055	-0.2175	-0.0786	-0.0773	-0.0303	0.2185	0.2663	-0.1221	0.0783	0.5172	0.0125	0.5677	44.1245	25.9855	34.889
18	2.6076	2.7377	4.3192	8.6176	3.5529	7.3685	-0.1283	0.3807	-0.1215	-0.4399	0.1859	-0.4468	-0.198	0.5535	-0.0577	0.2922	-0.0601	0.0924	0.5216	-0.0277	0.4561	39.3714	24.56	25.0347
19	1.3395	-0.2213	1.6702	4.909	2.8103	16.7107	-0.1068	0.0104	0.1945	-0.2991	0.11	0.1372	-0.6306	0.2668	-0.0032	0.2547	-0.0633	0.0394	0.3736	0.0299	0.5396	35.0095	33.9475	40.6306
20	13.6724	-6.0834	-10.22	4.5072	8.4544	16.1449	0.1168	-0.0795	0.932	0.3343	0.0744	-0.2306	0.7879	0.1615	-0.1912	0.2775	-0.0261	0.0903	0.3401	0.0027	0.6163	49.0756	26.7906	46.0723
21	10.5662	2.5619	10.8596	13.5841	-2.1043	28.1029	-0.1649	0.5404	0.431	0.3642	-0.2957	-1.0376	-0.7422	2.0537	0.4606	0.2955	-0.0089	0.03	0.5473	0.0629	0.446	60.6842	3.1803	40.0427
22	1.5769	0.818	-0.9437	4.3253	5.993	11.482	-0.077	0.2774	-0.1859	-0.2786	0.395	-0.482	-0.4055	0.4546	-0.318	0.2116	-0.0113	-0.0196	0.4584	0.0926	0.6355	53.9628	3.5581	34.2563
23	1.8257	-2.9926	0.3159	5.0367	-1.3461	6.2157	0.0508	0.0915	-0.1557	-0.0369	-0.0563	0.3318	-0.0833	-0.1498	0.0055	0.2571	0.0339	0.0171	0.4632	0.0163	0.5725	38.7927	-2.761	29.6308
24	3.0195	-0.9608	1.8044	2.68	0.1967	5.3673	-0.0457	0.4191	0.2597	-0.2323	-0.1292	-0.0901	-0.5481	0.2215	0.1749	0.292	-0.0262	0.0142	0.4946	-0.0296	0.4749	42.0408	1.5621	21.2068
25	3.3871	2.5091	-1.5418	6.9582	-0.8748	17.2278	0.3759	0.6503	1.0556	0.0214	0.2444	-0.2241	-0.4337	-0.2536	-0.6204	0.1672	-0.0369	0.1109	0.5538	0.1255	0.7017	54.3735	1.1154	23.036
26	24.3333	0.7512	0.6707	11.0266	17.6807	28.3666	0.7807	1.4293	0.6025	-0.1491	-0.1394	-0.4245	-0.2421	-0.2585	-0.6413	0.4003	0.0047	0.0807	0.6202	0.1287	0.4876	57.5556	-4.2241	18.1058
27	2.3045	-1.0718	3.2858	11.237	3.4184	6.9656	-0.1684	-0.0495	0.1317	-0.6212	0.0344	-0.2133	-0.5452	-0.0845	0.134	0.3265	-0.0055	0.0783	0.549	-0.0055	0.3786	45.9866	-6.7927	14.4649
28	5.9059	-2.565	0.8802	6.3182	-10.2406	18.8385	0.0508	0.2144	-0.0804	-0.0315	-0.0509	0.0827	0.0856	-0.0828	0.0002	0.2135	-0.0503	0.0245	0.4275	-0.0545	0.5561	34.2354	-12.0326	22.3489
29	8.9284	-0.4495	2.7638	1.8451	1.3268	5.2777	-0.1369	-0.193	-0.4067	0.0809	0.1743	0.1208	0.3732	-0.1204	-0.0374	0.2235	-0.0022	0.0704	0.3894	0.0334	0.5982	38.5408	-20.1513	37.04
30	3.8239	3.4179	-1.2778	7.9232	-0.5812	0.5413	0.262	-0.4434	0.2957	0.4635	-0.1878	0.3453	-0.0997	0.1447	-0.0742	0.2058	0.0247	0.0361	0.4766	-0.0163	0.5104	40.2982	-15.5764	47.8286
31	11.0934	-5.669	-3.8526	6.1233	6.4305	18.7848	0.3349	-0.492	-0.0519	0.3138	-0.1191	0.4039	-0.1146	-0.1624	-0.2158	0.2612	-0.0573	0.0458	0.3691	0.0141	0.4739	43.1913	-6.6069	53.2831
32	18.5923	2.0633	17.9999	3.4805	-0.2751	26.8517	-0.1199	-0.5368	0.2955	0.3558	-0.1835	0.5218	-0.4153	-0.117	0.3034	0.2749	0.0636	0.1045	0.3969	-0.0554	0.4721	42.0898	-0.961	49.4503
33	19.2803	-4.3816	-5.9613	7.0576	2.1808	7.0449	0.5722	0.9552	0.1591	-0.6494	-0.2909	0.6003	-0.7622	-0.29	-0.2813	0.2943	0.0222	0.0178	0.3981	0.0362	0.4895	33.8013	-8.9116	43.2607
34	1.662	2.6661	1.5224	9.861	3.8483	1.7663	0.0592	0.1052	0.0013	0.0958	0.019	-0.0073	0.0181	0.09	-0.0782	0.2156	-0.0016	0.0285	0.4552	-0.02	0.5295	45.1002	-2.0348	39.6194
35	5.8266	-2.1058	3.7345	21.2432	-8.1177	4.6911	0.0145	-0.1203	-0.1293	1.2815	-0.0312	0.0503	-0.477	0.0805	0.0167	0.2825	-0.0518	-0.0275	0.5361	0.0124	0.4233	53.2832	0.8627	46.6263
36	2.8721	2.2846	2.6419	2.0752	2.9825	5.6363	-0.0604	0.0522	-0.1114	-0.0804	-0.0467	0.0032	-0.1911	0.0375	0.1072	0.2275	0.0263	0.0205	0.4646	-0.0205	0.5445	49.6758	-13.9	36.9687
37	0.1244	0.0483	-0.6425	0.8932	-0.3952	5.1029	-0.0277	0.0297	-0.144	-0.5253	0.1358	-0.2685	0.4397	0.108	-0.1081	0.349	0.011	0.0492	0.498	-0.0631	0.7092	45.3364	-12.9723	22.6964
38	6.9131	2.0369	8.6548	2.3715	-0.7966	17.1669	-0.2792	0.2604	-0.0308	-0.046	-0.028	-0.2162	-0.4429	0.5599	0.3071	0.1948	0.0611	0.0289	0.5341	-0.076	0.4841	57.7332	-6.5507	33.3706
39	7.4646	2.5517	-6.2548	17.0355	-4.7272	27.1145	0.4947	-0.605	0.1462	1.4654	-0.2157	0.1219	-0.3109	-0.2755	-0.2791	0.2014	0.0296	-0.0369	0.4405	0.0219	0.515	60.2846	-9.6923	44.2961
40	14.6408	0.0411	8.4687	9.1446	2.873	24.5783	-0.0231	-0.0435	0.165	0.0927	0.1125	-0.169	-0.0716	-0.0977	-0.0893	0.2681	0.0804	0.0369	0.3558	0.0216	0.49	49.3598	-23.2908	41.3597
41	9.397	4.6117	4.3454	2.3326	3.3269	32.4327	0.5991	-0.5134	-0.9926	0.3712	-0.2123	-0.366	1.3995	0.8047	-0.3868	0.2984	0.0423	0.0349	0.3379	0.0664	0.7575	28.0713	-32.8139	44.5969
42	7.3928	-3.9987	6.3395	5.1781	1.9514	15.0652	0.5317	0.7948	-0.1881	0.0361	-0.525	0.1904	1.0811	0.6335	-0.0067	0.2582	-0.02	0.0589	0.4682	0.0206	0.5444	26.8286	-27.2167	37.5525
43	1.3409	2.2278	0.1349	7.1441	-2.4113	2.0586	-0.0681	0.183	0.018	-0.3162	-0.0942	-0.3582	0.1467	0.3398	0.1623	0.1971	0.0252	0.0799	0.4385	-0.0257	0.6385	19.4824	-17.1266	34.8166
44	2.7063	1.4317	-0.5141	5.6746	2.6516	6.8865	-0.0578	0.448	0.0993	-0.0813	0.1518	-0.123	0.0164	0.1087	-0.0941	0.2071	-0.0049	0.0099	0.4314	0.0114	0.5405	20.0119	-12.3991	27.5098
45	3.1397	3.2921	1.5431	7.5875	3.0326	11.6771	-0.0762	0.276	-0.4457	-0.0759	0.0438	-0.4435	0.1127	0.2914	0.0324	0.2778	0.0823	0.0581	0.4317	-0.0225	0.5008	20.7385	-28.9691	26.6847
46	10.2845	0.6728	-5.0306	0.7637	0.7482	4.1237	-0.0693	0.6248	0.2207	-0.1449	0.2891	-0.0112	-0.0466	0.156	-0.2197	0.4495	0.0721	-0.0718	0.4993	-0.0629	0.5222	12.2862	-24.5195	21.636
47	4.7925	3.0719	0.4975	24.0048	2.9412	15.1024	0.3236	0.6143	0.2229	-1.4966	-0.0959	0.6253	-0.0922	-0.1168	-0.2277	0.3219	0.0557	0.0004	0.4544	0.0471	0.457	7.6165	-8.5461	22.4301
48	0.9193	-0.2374	1.7896	0.0669	-0.4378	3.656	0.0348	0.0468	-0.0413	-0.0467	-0.0087	0.0255	-0.108	-0.0874	-0.0262	0.2933	0.0026	0	0.4263	0.0028	0.5808	5.9368	-8.8156	37.5764
49	8.9807	1.5478	3.9991	6.7891	1.6679	1.9291	-0.1709	-0.5892	-0.0165	0.191	0.1653	0.1956	-0.0262	-0.2355	0.0056	0.2578	-0.0372	0.0818	0.4297	0.05	0.5339	7.0667	-13.577	53.3561
50	18.1972	-1.7236	0.828	8.2591	3.7538	1.8685	-0.2167	-0.9286	0.2537	0.1689	0.3615	-0.1845	-0.005	0.0216	-0.1448	0.5364	0.1764	0.2012	0.5442	0.1192	0.5995	20.4451	-15.0367	57.2825
51	2.0144	-4.8899	5.2653	13.1991	-16.4251	27.5826	-0.0545	-0.2403	0.1198	0.4622	0.2997	-0.1735	-0.1613	0.3671	-0.2451	0.2856	-0.0175	0.0117	0.413	-0.0382	0.5375	25.6456	-13.7424	52.4645
52	2.443	-3.7886	-0.5651	20.0951	0.8349	3.4632	0.0822	0.2553	0.4352	-0.6758	0.2992	-0.4463	-0.1171	0.5287	-0.3814	0.4215	-0.0238	0.0595	0.4765	-0.042	0.4725	17.1084	-3.7177	46.716
53	10.5305	0.8172	2.6814	1.8253	-3.5807	8.8385	0.0544	-0.0115	-0.1767	0.1318	0.1462	0.0249	-0.2696	-0.3872	-0.2006	0.2615	0.0236	0.036	0.419	0.0514	0.5959	14.7147	-13.8418	44.7828
54	5.6764	0.1229	0.6611	0.2464	-0.8202	2.9525	-0.0401	-0.1466	0.2736	-0.0266	0.0017	-0.0191	0.092	0.025	0.0384	0.2283	-0.0084	0.002	0.4287	-0.0142	0.5672	26.3094	-20.0965	45.379
55	12.679	-0.8355	-6.562	13.6285	-2.6976	4.1236	-0.136	-0.2627	-0.074	0.2321	0.0343	-0.2288	0.0563	0.1625	0.1017	0.277	0.0365	-0.0009	0.4094	-0.0172	0.5115	20.4361	-25.1858	51.0783
56	0.401	-1.0276	0.1011	2.7962	0.5625	4.2329	0.0048	-0.0387	-0.0005	0.0626	0.0487	-0.0318	0.3075	-0.1743	-0.0535	0.2313	-0.0372	0.0411	0.4318	0.0283	0.5471	8.712	-22.0029	43.7247
57	6.2016	5.1464	2.4957	4.6132	2.8293	7.1987	0.0865	0.0398	0.4804	-0.1768	0.0245	0.5262	-0.1561	-0.6924	-0.111	0.2451	0.0135	-0.0382	0.4378	0.0194	0.5482	3.0517	-17.1506	30.0993
58	1.6524	-1.6219	1.0902	1.8273	-0.231	3.777	0.0689	-0.0634	-0.0251	-0.1112	0.0523	-0.0546	-0.0816	-0.0622	-0.1212	0.2638	-0.0427	0.0095	0.414	-0.0344	0.5415	11.5741	-23.0039	31.9988
59	3.7327	-6.6334	0.4511	16.3649	-7.5966	16.8401	-0.2396	0.1602	-0.7008	0.1131	-0.7867	-0.166	0.2692	0.4775	1.0262	0.2828	-0.0238	0.0427	0.3857	0.0484	0.8258	18.3692	-32.4168	43.1179
60	13.9935	-3.1008	2.9914	0.7176	-0.9568	4.129	-0.3052	-0.3627	0.2442	0.1151	0.0707	-0.0795	-0.1375	0.0212	0.2344	0.3209	-0.0461	0.0154	0.3611	-0.0152	0.6017	6.5877	-24.5926	51.6363
61	21.9674	1.885	-3.7571	21.9723	-7.2466	22.19	-0.3453	-0.6017	-0.1114	0.7217	0.6741	1.3318	0.6184	-1.4625	-0.3288	0.3593	-0.0123	0.0378	0.4545	0.0267	0.4674	-6.6996	-0.1723	54.2065
62	2.2922	3.4427	-1.6692	6.8111	-2.3691	4.9976	-0.2836	0.3071	-0.1433	-0.0676	0.1696	0.1508	0.2428	-0.0625	0.114	0.2214	0.0151	-0.0094	0.3806	-0.012	0.5706	0.8451	3.6524	42.9452
63	2.8812	0.3716	2.1538	4.5709	2.2941	4.6883	-0.236	0.3294	0.1544	-0.5055	0.3064	-0.1193	-0.1771	0.0501	-0.0705	0.2527	0.0062	0.0835	0.4484	0.0289	0.513	11.1072	6.6544	32.9814
64	14.6173	9.0175	-4.308	6.3393	1.2904	21.8386	-1.1822	0.8324	0.0335	-0.7449	0.5595	0.1553	0.1862	-0.4616	0.6228	0.4206	0.0029	-0.1213	0.4247	0.0266	0.5218	-1.6088	4.7047	27.5092
65	14.8189	-3.9049	-0.8708	8.3135	0.8651	10.425	-0.7943	0.3075	-0.4329	0.1385	0.4301	0.4871	0.3862	-0.6742	0.3642	0.2181	-0.0764	-0.006	0.3728	0.0008	0.5584	-8.4698	4.6544	36.0279
66	2.5105	4.3699	-0.9691	7.7685	-1.7346	0.3976	-0.2967	0.3388	0.2015	-0.3464	0.4484	0.3743	0.0682	-0.135	-0.1517	0.4232	0.0985	-0.1539	0.8165	0.1409	0.5591	-9.8677	11.6298	31.8025
67	11.3895	3.9087	-2.541	2.6776	-3.0731	4.7303	-0.4414	1.3224	0.7473	-0.6184	0.4206	0.3137	0.3016	-0.1279	0.0208	0.8627	-0.0701	-0.1924	0.4365	0.0311	0.5158	4.0995	16.1162	24.4363
68	18.4987	8.2673	4.5952	5.7804	6.2103	13.8637	-0.1521	0.1301	0.1436	0.1898	0.4068	-0.45	0.2379	-0.086	-0.2547	0.275	0.0221	0.0211	0.4378	-0.0422	0.5256	12.7503	18.8596	33.7299
69	1.6021	0.6754	1.8676	3.0073	1.1572	2.2276	-0.1446	-0.0654	0.0117	-0.3523	0.1282	0.0544	-0.217	-0.0556	0.0164	0.2444	0.0207	0.0428	0.431	0.0159	0.5866	13.413	23.1062	41.809
70	19.6988	5.0468	-2.2993	5.0639	-10.2295	24.9617	0.3095	-0.9171	0.5996	0.2853	-0.2965	0.1376	-0.4774	0.4158	-0.013	0.3003	0.1208	-0.0554	0.4295	-0.0757	0.723	10.1647	26.3071	54.1912
71	3.2164	2.2282	-1.506	7.8505	-3.4542	4.0012	0.0054	-0.2273	0.201	0.4182	0.1421	-0.1688	-0.2247	-0.0769	-0.1475	0.2054	0.0266	0.0252	0.4351	-0.0203	0.5425	14.5329	15.5559	56.8944
72	0.9916	-1.567	-4.7651	15.3535	0.1804	27.1807	-0.2741	-0.1413	0.0785	1.1471	0.281	-1.0012	0.9704	0.7832	-0.0069	0.2601	0.0167	-0.0119	0.5152	-0.0565	0.5232	13.6816	3.0545	58.8501
73	24.2465	27.0713	-7.5627	31.8713	-6.4846	4.7073	-0.397	0.1298	-0.9705	-0.0818	0.2639	-1.1684	0.5403	0.1718	0.1331	0.2405	-0.042	0.0338	0.4339	-0.0578	0.6	21.1223	8.2358	47.7212
74	0.2304	0.8209	-0.4167	7.0569	0.1307	1.3979	0.0082	0.0041	0.0062	-0.2581	0.0327	0.1326	-0.1581	0.0292	-0.0409	0.2425	-0.0055	0.0017	0.4405	-0.0081	0.553	9.8379	8.1079	48.5656
75	7.4838	0.1026	-5.2465	16.8372	5.9752	5.8582	0.4719	-0.2727	0.0363	1.165	-0.2035	-0.6586	0.1255	0.0912	-0.2684	0.3373	0.0186	-0.0196	0.4082	0.0548	0.5305	3.7105	-1.2812	55.7708
76	1.5014	1.3195	0.164	1.1819	0.1529	0.0242	0.0839	0.0066	0.0039	0.0868	-0.0781	0.0804	0.0011	-0.0512	-0.0059	0.241	0.0233	0.0517	0.4434	-0.0179	0.5971	2.253	15.3799	51.5082
77	7.7469	-0.3471	-5.4742	0.0617	0.2784	3.9019	0.5488	0.2089	0.5318	-0.2131	-0.097	0.0202	-0.5742	-0.1504	-0.4518	0.8412	0.0634	-0.0726	0.3985	0.0234	0.529	2.0916	20.2533	33.2294
78	4.9002	-1.855	-9.5399	10.725	7.7355	20.2699	-0.0873	0.6486	1.0047	-1.5415	1.2987	1.4434	-0.4761	-0.6212	-1.2114	0.3978	-0.119	-0.2875	0.6198	0.198	0.8484	-4.1757	15.398	39.6589
79	3.7227	3.9477	-7.066	10.7341	-3.3045	16.186	-0.2948	0.4256	0.0155	-0.3279	0.0883	0.5044	0.3608	-0.9474	0.2066	0.2608	-0.0064	0.0259	0.5037	0.0154	0.5609	-5.9221	10.6471	48.1069
80	5.0683	2.5267	-0.2869	8.3032	-1.2822	0.972	0.0033	-0.128	-0.2499	-0.0084	0.1062	0.1	0.052	-0.2591	-0.1095	0.2661	0.0326	0.0544	0.455	-0.0334	0.5113	-0.3864	18.1509	56.394
81	7.5592	4.669	1.6849	3.2483	1.6734	5.5474	-0.3558	-0.8299	-0.3169	-0.0655	-0.338	-0.5592	-0.1031	0.9393	0.6938	0.2933	-0.2036	-0.0029	0.6853	-0.1688	1.1038	58.7205	0.3158	-5.7671
82	3.2097	-0.1626	-3.5475	2.9693	6.5379	17.7276	-0.0038	0.0583	0.5991	-0.3257	0.1956	0.2562	-0.98	0.4301	-0.1918	0.5939	-0.001	0.0929	0.3734	-0.1148	0.4893	49.5744	-1.8105	-13.8867
83	6.0611	-2.9832	1.1596	2.2828	0.5181	1.6811	-0.4924	-0.2917	0.1641	0.1897	-0.0183	0.2401	-0.1798	-0.2883	0.5108	0.2846	0.0359	0.036	0.4391	-0.0354	0.5367	40.4253	-7.059	-19.4047
84	11.8766	1.8444	-4.6802	5.388	0.2905	4.8977	0.3177	-0.2945	0.2478	-0.5566	-0.1455	0.3249	-0.4047	0.0499	-0.1722	0.4037	0.081	-0.0046	0.3805	-0.0309	0.4257	41.5817	-0.3671	-24.7651
85	4.3413	3.6093	2.0516	4.5932	6.1026	14.4062	0.1585	0.0056	1.112	-0.046	-0.1388	0.5932	-0.9857	0.4977	-0.0197	0.4217	-0.2615	-0.0812	0.6749	0.1244	0.6832	56.3218	0.3192	-23.7609
86	18.1435	7.0453	-3.4931	8.4679	3.819	5.358	-0.3425	0.2196	0.0172	-0.9599	0.7021	-0.391	-0.7238	0.5874	-0.3596	0.3925	-0.1133	-0.0029	0.5104	-0.0215	0.5059	58.2568	-5.4714	-28.314
87	3.4752	-0.7267	4.1313	0.3765	-0.1737	7.1034	-0.0303	0.2159	0.2257	-0.0682	0.078	-0.1156	-0.14	0.5717	-0.0477	0.3463	-0.0606	-0.0259	0.4571	-0.0184	0.5133	43.7446	-9.2137	-35.4537
88	7.4176	4.8608	-2.93	3.9396	-2.6091	1.8016	0.2292	-0.2744	0.2478	0.0247	-0.0487	0.2831	-0.0044	-0.094	-0.1805	0.255	0.0347	-0.0397	0.5275	-0.0788	0.5084	36.3278	-17.4089	-25.4701
89	5.1433	0.0793	0.992	7.7709	-2.6622	10.2541	-0.0458	-0.7003	-0.9911	0.1292	0.6067	0.0187	0.4301	0.1368	-0.5609	0.2341	0.0534	-0.0508	0.4529	0.0151	0.5663	42.2518	-24.339	-11.7454
90	5.2392	3.9472	2.8823	16.0404	7.3094	3.6089	0.1034	-0.2903	-0.5555	0.6125	0.1321	-0.2602	0.2899	0.005	-0.2354	0.2624	0.0939	-0.0034	0.5272	0.0747	0.4399	38.063	-22.685	-5.2991
91	2.3595	6.4668	0.2353	20.197	6.7159	16.5142	0.2518	0.0066	0.0316	0.7428	0.2316	0.0599	0.703	-0.3123	-0.4833	0.346	-0.0486	-0.0937	0.6309	0.0336	0.4761	40.8738	-13.5469	2.8724
92	0.3528	-0.1543	0.4538	7.9734	-16.6405	34.7949	0.4849	0.0114	0.2683	-0.0462	0.5107	0.5345	0.2632	-0.9805	-0.9956	0.8092	0.0417	0.1456	0.4476	-0.0355	0.6663	40.1822	-5.7452	1.0489
93	15.8739	6.3827	11.2012	32.7254	14.3475	11.1229	-0.3378	0.53	0.769	1.1411	0.062	-0.4482	0.1314	0.3147	0.2758	0.3692	-0.1141	0.1027	0.4825	-0.0241	0.8062	31.3567	-9.7986	-7.9583
94	0.0392	-0.1311	0.0954	5.0376	-0.1703	0.8904	0.0205	-0.0628	0.0303	0.2119	0.1401	0.1924	-0.0561	0.2833	-0.1606	0.2964	-0.0027	0.0199	0.5382	-0.0612	0.4621	42.5669	-8.8988	-8.624
95	1.4598	-2.1492	2.016	16.5174	2.2011	4.7891	-0.4306	-0.0204	-0.0804	1.3647	0.3784	0.5573	-0.3253	0.1506	0.0523	0.3028	-0.0312	0.0444	0.5717	-0.1538	0.4695	50.384	-3.5932	-0.0458
96	0.5674	-1.1969	-3.3631	4.5822	7.7822	20.2534	0.1421	-0.1938	-0.0049	0.6151	0.0606	-0.0699	-0.5904	0.9681	-0.2027	0.4928	-0.0934	-0.0736	0.5964	-0.0245	0.516	50.3145	-15.3352	-5.5046
97	1.5281	0.5056	2.3157	1.0973	-2.5962	15.7343	0.133	-0.053	-0.3667	0.0026	-0.1314	-0.3108	0.4223	0.2527	-0.0016	0.217	0.0084	-0.0082	0.5207	-0.0618	0.5459	49.7394	-19.9778	-20.2381
98	2.3682	-1.8847	0.5286	4.8167	-1.3327	5.0536	-0.0097	0.0462	-0.2092	-0.1561	0.129	-0.0234	-0.1354	0.2525	-0.1192	0.2189	-0.0105	-0.0066	0.4825	-0.0844	0.4958	50.884	-12.1312	-24.5072
99	7.9886	-2.7353	6.1552	2.1627	3.1886	27.8939	0.1552	-0.3809	0.1553	-0.3565	0.0227	-0.2144	-1.2322	-0.6116	-0.1779	0.29	-0.096	0.0245	0.6259	-0.0427	0.7226	59.7885	-9.4794	-8.3498
100	5.0046	4.7088	2.0145	13.1151	4.6475	6.5724	0.3808	-0.584	-0.5457	0.4136	-0.3132	-0.6345	0.3585	-0.2103	-0.0676	0.1456	0.1027	-0.0725	0.5221	0.0189	0.5258	51.9464	-23.6447	-6.4184
101	20.6674	22.6634	-10.457	24.8571	-11.472	5.2981	-0.5837	0.2174	-0.8569	-0.6858	0.1801	-0.9199	0.3791	-0.0554	0.4036	1.2324	0.5124	-0.1277	0.6837	-0.1245	0.5043	27.991	-37.0328	-13.2177
102	4.5731	-0.7626	2.5916	2.4422	-1.8304	4.2991	-0.0401	0.2915	0.1595	-0.2975	-0.1269	-0.2712	0.3619	0.1346	0.167	0.2201	-0.0403	-0.0043	0.4719	-0.0049	0.5301	25.8499	-26.3524	-19.9668
103	3.124	2.1104	0.8933	1.7438	1.0036	10.9706	-0.2028	0.0029	0.2632	-0.0806	0.108	0.104	-0.5061	0.4895	0.0948	0.3373	-0.0153	-0.117	0.3318	-0.0203	0.4908	22.2426	-14.177	-26.3764
104	4.5953	-4.3757	4.6485	13.2071	-3.0174	6.6528	0.0754	0.4958	0.2197	-0.7356	-0.051	-0.382	0.623	0.7289	-0.0244	0.3375	0.0403	-0.0809	0.46	-0.0754	0.442	25.5494	-29.2055	-31.3492
105	13.4663	4.2193	7.4971	1.8764	-0.9719	24.8917	-1.325	0.4622	-1.4905	-0.4082	0.172	-0.7376	-0.5989	-0.401	1.153	0.5806	0.0122	0.0795	0.4983	-0.1657	0.6409	19.8313	-33.5292	-34.6625
106	2.9441	-3.5187	6.0878	4.469	-5.9396	19.8582	0.1462	0.2927	0.2263	-0.2405	-0.3752	-0.2876	0.1471	0.071	0.2289	0.347	-0.0844	-0.0429	0.4171	-0.0124	0.5241	17.3435	-22.7759	-37.8461
107	3.5227	0.9095	-9.0374	5.7243	-3.8829	23.6281	0.233	0.1349	-0.0299	-0.0129	-0.2742	0.1641	-0.6249	-0.2775	0.0413	0.3687	0.0255	-0.1022	0.4247	0.018	0.466	11.1514	-11.0297	-30.0662
108	10.1603	1.1048	3.6738	0.154	0.4229	1.4302	0.2542	-0.1766	0.3862	0.0118	-0.1535	-0.0053	0.0329	-0.0411	-0.1008	0.8252	0.102	0.0653	0.6961	-0.1093	0.5876	3.9207	-9.8543	-22.0886
109	9.3896	-2.3427	-0.3456	1.3161	-2.6495	10.2564	-0.2111	-1.0404	0.3165	0.1077	0.3596	-0.0347	-0.245	-0.3517	-0.1485	0.1724	-0.0219	0.0027	0.6421	-0.1884	0.5704	6.1603	-19.2789	-12.9749
110	13.1334	-0.9537	-4.0502	0.0717	0.2951	1.2556	-0.072	-0.4195	-0.0124	0.0249	0.0484	0.0188	0.0594	0.0793	0.0236	0.3913	-0.0567	-0.0031	0.7293	-0.1436	0.6253	4.2928	-17.6475	-5.4225
111	20.9928	-5.2012	10.3097	9.1093	-0.8267	5.4522	-0.7713	-1.6466	0.4249	0.9265	0.3431	0.8161	-0.174	-0.8447	0.4282	0.3301	-0.0568	0.1393	0.5498	-0.1034	0.5338	16.1419	-21.1934	-0.1434
112	10.6699	5.1831	-4.8961	26.0411	-23.9346	22.0163	0.574	-0.741	0.4466	0.7593	-0.5329	0.0356	-0.6276	0.4517	-0.0412	0.4685	-0.1142	-0.0388	0.5047	-0.1688	0.394	23.3605	-19.0633	-2.9021
113	11.8835	17.3309	0.7611	36.6493	5.0339	2.2463	0.2684	0.214	0.6214	-1.0118	-0.3437	-0.054	-0.3095	-0.0299	0.0752	0.2763	0.0151	0.1452	0.7002	-0.0958	0.5437	16.0073	-9.9413	-8.3559
114	15.9102	-2.3752	3.8742	0.522	-1.1513	2.9912	-0.2172	-0.1378	0.3541	0.1046	0.0658	-0.0858	-0.205	-0.013	0.1514	0.2922	0.0236	-0.0426	0.4536	-0.0778	0.4783	18.3392	-20.7012	-13.6765
115	8.3665	0.4493	-0.978	24.4155	2.4073	3.254	0.0699	-0.3065	-0.0596	0.536	-0.2636	-0.0147	0.0896	-0.0319	0.1937	0.2694	-0.0091	-0.0378	0.4605	0.0095	0.4138	29.1081	-26.0246	-8.5903
116	10.2542	-2.5594	1.5924	4.8564	-1.531	3.2164	-0.3367	-0.364	0.1839	0.2914	0.0365	-0.0065	0.4117	0.1111	0.3002	0.2065	-0.031	0.0156	0.5177	-0.0349	0.4779	16.2205	-29.3284	-8.9788
117	9.7909	-2.3358	0.5758	0.5578	-0.1365	0.0382	0.0847	0.2847	-0.0709	-0.0107	-0.0529	0.0185	0.0258	0.0186	-0.0319	0.1629	-0.0163	-0.0396	0.5511	-0.0678	0.6428	6.5276	-24.7676	-21.8942
118	1.7922	2.5571	-0.9087	4.8479	-2.111	1.0236	-0.0798	-0.1379	0.2768	0.1814	0.0332	0.2018	-0.2101	-0.1191	0.0467	0.3825	0.1088	-0.1267	0.64	-0.1394	0.5543	10.071	-20.2711	-30.4376
119	0.1579	0.5264	-0.7026	10.2261	-8.6191	7.7856	-0.2639	-0.0179	-0.1155	-0.5706	0.118	0.0354	0.9786	-0.0495	0.1459	0.5705	-0.0295	0.0116	0.4873	-0.0233	0.5278	17.2796	-33.1281	-20.7638
120	19.3615	-5.4444	4.5651	2.3862	-2.1739	3.0374	-0.7083	-1.4042	-0.1305	0.4075	0.6327	-0.0404	-0.216	-0.199	0.0755	0.2395	-0.015	0.0436	0.6192	-0.1137	0.4968	7.2166	-31.4357	-9.5576
121	18.241	-11.0746	3.0594	6.7348	-1.853	0.5157	-0.1071	0.1792	0.8201	0.0489	-0.0497	-0.4658	-0.0538	0.0542	0.1568	1.0305	-0.1176	0.048	0.3487	-0.1481	0.493	21.8531	28.8674	-1.6567
122	1.3946	-0.6911	-1.2433	9.1059	3.8755	8.0375	-0.2836	0.3791	-0.1201	-0.6099	0.1667	0.2059	-0.3919	-0.1937	0.1169	0.779	-0.0171	-0.0154	0.2781	-0.008	0.3554	29.4463	16.4522	-13.65
123	0.5951	1.9723	2.3213	6.5523	7.7116	9.0789	0.0468	0.0473	-0.011	0.181	0.0895	-0.0911	0.1821	0.1572	-0.1362	0.8942	-0.0369	-0.1145	0.3314	0.0485	0.5012	26.9781	18.1233	-22.2838
124	8.3321	-1.4294	8.5939	37.8636	-28.7653	28.684	-0.5083	0.9561	1.298	-0.2226	-0.0572	0.831	-0.2061	0.8474	0.5655	0.8364	-0.0233	-0.0404	0.5893	0.0486	0.5962	24.0028	30.0741	-20.8193
125	2.126	4.5958	-5.9309	13.8311	-15.7215	18.7357	-0.5024	0.5048	-0.1457	1.0207	-0.1725	-0.7391	-0.2859	-0.5518	0.6749	1.6892	-0.4742	-0.0913	0.7897	0.0578	0.74	28.9532	34.034	-14.6173
126	2.128	-2.6275	3.95	3.3505	-5.0594	7.6453	0.042	0.5092	0.2775	0.3595	-0.5326	-0.3149	-0.6077	0.8181	0.4906	1.4874	0.024	0.0029	0.4224	0.1875	0.2887	33.3545	30.4445	-23.2623
127	11.6978	-2.7183	1.6791	25.5545	-12.441	6.0749	0.258	0.4586	-0.0564	0.6694	-0.1378	0.3607	-0.321	0.1055	-0.1202	0.8523	0.0096	0.0205	0.7519	0.0415	0.4914	40.4606	20.6685	-31.0267
128	20.8651	-10.5474	7.2256	5.3885	-3.284	8.8894	-0.2045	0.4319	0.643	0.0767	-0.171	-0.2413	-0.0153	-0.253	0.3754	0.7413	-0.1063	0.1171	0.3299	-0.0718	0.4754	41.2133	11.5119	-21.254
129	3.4881	-0.4804	-0.2167	5.8565	7.5718	9.8871	0.2068	-0.1356	0.6637	-0.3869	0.1138	-0.3415	-0.3799	0.2498	-0.3207	0.6237	-0.0426	0.1861	0.3856	-0.0733	0.5474	46.3772	12.6235	-7.4964
130	21.5437	20.5728	14.8914	37.928	18.4031	11.2662	0.2666	0.9561	-0.0692	0.3005	-0.1313	-0.6989	0.1974	0.4796	-0.1353	0.6216	-0.0931	0.0792	0.7526	-0.0873	0.4708	50.5463	9.7676	0.7548
131	12.641	-2.1067	-8.6734	3.0728	-0.5422	7.4048	-0.0603	-0.6154	0.2803	0.0081	0.3047	-0.0101	0.0195	0.2844	-0.2444	0.4267	-0.0722	-0.0153	0.4767	-0.1762	0.4137	37.6246	9.8623	5.4676
132	17.3227	-8.4537	-4.2205	15.1981	13.7496	24.8934	0.3649	-0.7211	-0.8908	0.7567	0.0487	0.1955	-0.5698	-0.4567	-0.4136	0.4463	-0.0753	0.045	0.4648	-0.0091	0.3035	27.3779	9.908	8.9461
133	30.2155	-10.7147	-12.9667	7.453	8.3667	9.4589	-0.5818	-0.746	-1.814	-0.6402	-0.2715	0.7772	-0.6658	-0.1594	0.8533	0.6421	-0.0845	0.0714	0.4377	-0.0301	0.5324	30.5631	4.1206	-3.9098
134	4.2223	-0.5081	0.3796	0.6146	0.0724	2.673	0.122	0.2961	-0.0514	-0.3374	0.0184	-0.0087	-0.574	-0.0289	-0.1405	0.5995	-0.0067	0.0377	0.2969	-0.0526	0.4275	31.2941	13.8298	-3.856
135	25.5224	1.8742	0.7891	10.7267	5.9517	3.3092	0.5847	-1.0616	0.6514	0.2933	-0.5848	0.0219	0.1385	-0.3551	0.0001	0.7198	0.0547	-0.0246	0.4732	-0.0641	0.3005	22.3421	19.7276	3.5517
136	4.638	-5.1023	-6.6035	7.9993	3.467	15.5828	-0.048	-0.0562	0.22	-0.0099	0.0047	-0.3814	-0.007	-0.0071	0.0432	0.5755	-0.0727	0.0068	0.3419	-0.1235	0.5168	35.4748	21.1625	2.596
137	0.0851	0.0667	-1.191	9.3111	0.3711	22.4971	0.0928	0.0686	0.0505	-0.5131	0.384	-0.6125	0.6433	-0.7008	-0.4768	0.8337	-0.1148	0.1427	0.4712	0.0149	0.3931	44.6795	22.3702	-14.0988
138	6.1189	-7.4682	2.049	9.1204	-2.2338	20.657	0.5894	0.1225	0.0994	-0.7554	-0.1152	-0.1119	0.1107	2.3003	-0.4742	1.0107	-0.1781	0.0621	0.3247	0.0358	0.323	37.457	23.6993	-18.1803
139	4.24	-0.8989	4.2384	12.6753	3.7005	5.9339	0.1516	0.1662	-0.1233	1.1256	-0.2684	0.7483	0.5471	0.0643	0.1168	0.85	-0.0616	0.1114	0.3491	0.0424	0.5978	35.2366	29.6687	-8.292
140	10.7081	-6.21	0.499	6.3901	1.6032	1.4163	-0.0739	-0.6019	0.5413	-0.4868	0.4063	-0.5973	-0.5626	0.1504	-0.3323	0.7941	-0.2481	0.1661	0.384	-0.1449	0.4296	39.1327	25.6385	2.2463
141	34.9094	4.5479	-5.1967	28.8296	15.0709	9.5576	-0.0557	-1.3791	-0.1172	0.2509	0.1493	-0.1729	0.1682	0.3881	-0.0936	0.4658	0.0903	-0.0519	0.6324	-0.0535	0.6075	-7.5264	-6.6298	-7.657
142	23.676	6.6227	2.6426	14.1583	6.2846	2.8325	-0.5902	0.5624	-1.3077	-0.6579	0.1739	0.5799	-0.4258	-0.1083	0.4163	0.6599	0.518	-0.4176	0.8207	-0.37	0.526	0.9643	-1.8189	-15.3798
143	6.2935	9.3236	-8.9045	23.4728	-9.8379	15.0196	-0.7225	0.7638	1.0326	-1.1488	1.1341	0.7584	-0.0656	-0.811	-0.4116	1.6318	-0.0431	-0.9965	0.2627	0.5013	1.692	13.3981	5.1244	-19.2697
144	2.2639	-3.359	-1.7412	5.0162	2.5971	1.3705	-0.2472	0.1054	-0.255	0.4456	-0.071	0.4088	0.2653	-0.0919	0.3182	1.072	-0.2316	-0.2001	0.4598	0.0796	0.8069	4.782	1.6589	-27.1361
145	0.1241	1.1071	1.1906	10.5836	11.3504	12.1994	-0.1055	-0.0101	0.0273	-0.2832	-0.2842	0.3781	-0.3793	-0.436	0.3897	0.8753	0.1049	-0.1414	0.8352	-0.0549	0.7407	-7.3261	-0.3881	-23.0851
146	21.4643	5.3883	-7.5972	1.4836	-1.0357	8.7195	0.6636	-0.5038	-1.3526	0.2804	-0.2164	-0.4602	0.3885	-0.1385	-0.4472	0.8251	0.0421	-0.1039	0.5572	-0.0416	0.7091	-5.6795	8.4327	-27.971
147	4.4084	-1.7421	-6.7228	0.6902	2.6638	10.3849	0.2595	-0.0107	-0.0293	-0.0651	0.0253	-0.006	-0.3504	0.3015	-0.2849	1.0144	0.0932	-0.3024	0.968	-0.314	1.2857	11.0529	14.902	-30.221
148	13.3137	5.394	0.7485	7.2793	-6.2194	8.4343	-0.2329	0.111	0.5324	-0.4957	0.0283	0.0614	0.2946	0.0015	0.2046	1.1254	0.266	-0.0168	0.243	-0.0785	0.4764	14.4683	17.4983	-16.2872
149	9.4818	-8.7866	2.4409	16.2585	0.0581	7.5449	0.7947	-0.0938	0.3628	-1.1705	-0.6874	0.3495	-0.9401	0.1691	-0.1073	0.5647	0.2534	-0.0971	0.396	-0.1649	0.3975	10.3946	17.4829	-0.7637
150	3.0165	4.9768	-0.5717	29.189	-8.0297	11.9133	0.2784	-0.6251	-0.4085	0.8152	-0.3462	0.5601	0.1178	-1.0421	0.0677	0.2004	0.0592	-0.0341	0.6193	-0.1402	0.5055	8.3971	3.6365	5.0589
151	12.1232	8.4514	5.0528	7.0397	5.7074	6.3303	-0.0047	0.1041	-0.7791	-0.4155	-0.2858	-0.2679	-0.7668	-0.528	0.2904	0.4311	0.2208	-0.0331	0.3878	-0.0864	0.4475	13.6559	3.4302	-4.6951
152	5.252	3.4575	2.2264	29.4778	-1.327	1.2623	-0.1789	-0.6664	0.1342	-0.895	-0.0047	0.2383	-0.0703	-0.4381	0.1836	0.271	0.2455	-0.1526	0.6382	-0.3514	0.6512	5.2393	-3.3695	-7.4556
153	5.1111	7.1592	0.6599	16.3962	1.3469	0.1149	0.4676	-0.6255	-0.5611	-0.2567	-0.5005	1.0288	-0.0033	-0.0249	0.0329	0.6126	-0.0155	-0.1091	0.7431	-0.0479	0.7865	-0.916	-6.0408	-1.1145
154	6.0172	5.5271	-5.8357	13.0625	9.9521	35.0814	-0.0895	-0.0964	0.9564	0.1184	-0.6491	1.7179	0.4297	-1.2098	0.7386	0.1417	0.2917	-0.1584	0.7648	-0.3619	0.7332	-1.0871	4.7514	-1.1683
155	0.0613	-0.1896	0.3145	9.3693	-11.2182	13.681	0.1723	0.0819	0.0628	0.4487	-0.0699	0.3952	-0.3759	0.2299	-0.1024	0.7229	0.3127	-0.0739	0.4921	-0.0978	0.8618	0.8755	15.7851	-9.1401
156	16.8437	8.7924	-6.0987	6.287	-6.9753	10.9613	-1.4914	-0.7364	1.0028	-2.1694	0.2682	-0.0644	3.6558	-0.7613	1.2232	1.5089	-0.2593	0.1305	1.0846	-0.0803	0.8342	3.8705	20.514	-19.1457
157	43.2304	-13.7171	-15.962	8.4938	19.6625	57.4306	-0.5966	-0.3797	0.6059	-0.2633	0.5967	-0.1562	-1.2834	1.5863	-0.0001	0.8553	-0.3359	-0.5097	0.7118	-0.2501	0.6545	3.8319	13.3304	-24.079
158	30.8267	8.8522	-29.0092	3.711	-11.8674	38.2588	-0.1281	-0.9211	-0.2617	0.0867	-0.5953	-0.1069	-0.4982	1.6666	0.7234	0.4839	0.1604	-0.4702	0.373	-0.1156	0.9034	-4.6269	8.3739	-15.6803
159	11.1396	1.1625	7.4429	5.528	-1.2987	5.771	0.533	-1.184	1.1167	-0.439	-0.6241	1.8	0.554	-0.6235	0.0911	0.4764	0.1667	-0.0684	0.6335	-0.3109	0.858	-9.2185	3.9192	-5.1175
160	10.543	-8.8297	-0.8388	9.3445	3.7441	4.8142	0.6952	-0.1314	-0.8721	-1.0448	-0.0333	0.2418	-0.7998	-0.2299	-0.6618	0.5666	0.3009	-0.1151	0.3928	-0.0509	0.6712	1.5646	19.7583	-0.8037

Refinement TLS group

ID	Refine-ID	Refine TLS-ID	Auth asym-ID	Auth seq-ID
1	X-RAY DIFFRACTION	1	A	1 - 5
2	X-RAY DIFFRACTION	2	A	6 - 25
3	X-RAY DIFFRACTION	3	A	26 - 40
4	X-RAY DIFFRACTION	4	A	41 - 49
5	X-RAY DIFFRACTION	5	A	50 - 61
6	X-RAY DIFFRACTION	6	A	62 - 75
7	X-RAY DIFFRACTION	7	A	76 - 90
8	X-RAY DIFFRACTION	8	A	91 - 95
9	X-RAY DIFFRACTION	9	A	96 - 104
10	X-RAY DIFFRACTION	10	A	105 - 110
11	X-RAY DIFFRACTION	11	A	111 - 115
12	X-RAY DIFFRACTION	12	A	116 - 120
13	X-RAY DIFFRACTION	13	A	121 - 125
14	X-RAY DIFFRACTION	14	A	126 - 139
15	X-RAY DIFFRACTION	15	A	140 - 147
16	X-RAY DIFFRACTION	16	A	148 - 158
17	X-RAY DIFFRACTION	17	A	159 - 166
18	X-RAY DIFFRACTION	18	A	167 - 179
19	X-RAY DIFFRACTION	19	A	180 - 195
20	X-RAY DIFFRACTION	20	A	196 - 204
21	X-RAY DIFFRACTION	21	B	1 - 5
22	X-RAY DIFFRACTION	22	B	6 - 14
23	X-RAY DIFFRACTION	23	B	15 - 28
24	X-RAY DIFFRACTION	24	B	29 - 41
25	X-RAY DIFFRACTION	25	B	42 - 49
26	X-RAY DIFFRACTION	26	B	50 - 55
27	X-RAY DIFFRACTION	27	B	56 - 64
28	X-RAY DIFFRACTION	28	B	65 - 76
29	X-RAY DIFFRACTION	29	B	77 - 96
30	X-RAY DIFFRACTION	30	B	97 - 106
31	X-RAY DIFFRACTION	31	B	107 - 111
32	X-RAY DIFFRACTION	32	B	112 - 119
33	X-RAY DIFFRACTION	33	B	120 - 126
34	X-RAY DIFFRACTION	34	B	127 - 140
35	X-RAY DIFFRACTION	35	B	141 - 149
36	X-RAY DIFFRACTION	36	B	150 - 167
37	X-RAY DIFFRACTION	37	B	168 - 183
38	X-RAY DIFFRACTION	38	B	184 - 192
39	X-RAY DIFFRACTION	39	B	193 - 198
40	X-RAY DIFFRACTION	40	B	199 - 204
41	X-RAY DIFFRACTION	41	C	1 - 5
42	X-RAY DIFFRACTION	42	C	6 - 13
43	X-RAY DIFFRACTION	43	C	14 - 21
44	X-RAY DIFFRACTION	44	C	22 - 40
45	X-RAY DIFFRACTION	45	C	41 - 50
46	X-RAY DIFFRACTION	46	C	51 - 63
47	X-RAY DIFFRACTION	47	C	64 - 70
48	X-RAY DIFFRACTION	48	C	71 - 90
49	X-RAY DIFFRACTION	49	C	91 - 106
50	X-RAY DIFFRACTION	50	C	107 - 111
51	X-RAY DIFFRACTION	51	C	112 - 119
52	X-RAY DIFFRACTION	52	C	120 - 124
53	X-RAY DIFFRACTION	53	C	125 - 129
54	X-RAY DIFFRACTION	54	C	130 - 145
55	X-RAY DIFFRACTION	55	C	146 - 153
56	X-RAY DIFFRACTION	56	C	154 - 165
57	X-RAY DIFFRACTION	57	C	166 - 173
58	X-RAY DIFFRACTION	58	C	174 - 187
59	X-RAY DIFFRACTION	59	C	188 - 194
60	X-RAY DIFFRACTION	60	C	195 - 204
61	X-RAY DIFFRACTION	61	D	1 - 5
62	X-RAY DIFFRACTION	62	D	6 - 21
63	X-RAY DIFFRACTION	63	D	22 - 34
64	X-RAY DIFFRACTION	64	D	35 - 41
65	X-RAY DIFFRACTION	65	D	42 - 50
66	X-RAY DIFFRACTION	66	D	51 - 58
67	X-RAY DIFFRACTION	67	D	59 - 70
68	X-RAY DIFFRACTION	68	D	71 - 78
69	X-RAY DIFFRACTION	69	D	79 - 90
70	X-RAY DIFFRACTION	70	D	91 - 95
71	X-RAY DIFFRACTION	71	D	96 - 110
72	X-RAY DIFFRACTION	72	D	111 - 117
73	X-RAY DIFFRACTION	73	D	118 - 122
74	X-RAY DIFFRACTION	74	D	123 - 139
75	X-RAY DIFFRACTION	75	D	140 - 146
76	X-RAY DIFFRACTION	76	D	147 - 165
77	X-RAY DIFFRACTION	77	D	166 - 178
78	X-RAY DIFFRACTION	78	D	179 - 184
79	X-RAY DIFFRACTION	79	D	185 - 191
80	X-RAY DIFFRACTION	80	D	192 - 204
81	X-RAY DIFFRACTION	81	E	1 - 9
82	X-RAY DIFFRACTION	82	E	10 - 17
83	X-RAY DIFFRACTION	83	E	18 - 25
84	X-RAY DIFFRACTION	84	E	26 - 37
85	X-RAY DIFFRACTION	85	E	38 - 49
86	X-RAY DIFFRACTION	86	E	50 - 60
87	X-RAY DIFFRACTION	87	E	61 - 69
88	X-RAY DIFFRACTION	88	E	70 - 83
89	X-RAY DIFFRACTION	89	E	84 - 95
90	X-RAY DIFFRACTION	90	E	96 - 104
91	X-RAY DIFFRACTION	91	E	105 - 112
92	X-RAY DIFFRACTION	92	E	113 - 117
93	X-RAY DIFFRACTION	93	E	118 - 122
94	X-RAY DIFFRACTION	94	E	123 - 139
95	X-RAY DIFFRACTION	95	E	140 - 149
96	X-RAY DIFFRACTION	96	E	150 - 158
97	X-RAY DIFFRACTION	97	E	159 - 169
98	X-RAY DIFFRACTION	98	E	170 - 186
99	X-RAY DIFFRACTION	99	E	187 - 194
100	X-RAY DIFFRACTION	100	E	195 - 204
101	X-RAY DIFFRACTION	101	F	1 - 5
102	X-RAY DIFFRACTION	102	F	6 - 20
103	X-RAY DIFFRACTION	103	F	21 - 38
104	X-RAY DIFFRACTION	104	F	39 - 49
105	X-RAY DIFFRACTION	105	F	50 - 55
106	X-RAY DIFFRACTION	106	F	56 - 63
107	X-RAY DIFFRACTION	107	F	64 - 76
108	X-RAY DIFFRACTION	108	F	77 - 84
109	X-RAY DIFFRACTION	109	F	85 - 92
110	X-RAY DIFFRACTION	110	F	93 - 103
111	X-RAY DIFFRACTION	111	F	104 - 111
112	X-RAY DIFFRACTION	112	F	112 - 119
113	X-RAY DIFFRACTION	113	F	120 - 125
114	X-RAY DIFFRACTION	114	F	126 - 136
115	X-RAY DIFFRACTION	115	F	137 - 144
116	X-RAY DIFFRACTION	116	F	145 - 159
117	X-RAY DIFFRACTION	117	F	160 - 167
118	X-RAY DIFFRACTION	118	F	168 - 180
119	X-RAY DIFFRACTION	119	F	181 - 192
120	X-RAY DIFFRACTION	120	F	193 - 204
121	X-RAY DIFFRACTION	121	G	2 - 9
122	X-RAY DIFFRACTION	122	G	10 - 27
123	X-RAY DIFFRACTION	123	G	28 - 39
124	X-RAY DIFFRACTION	124	G	40 - 45
125	X-RAY DIFFRACTION	125	G	46 - 52
126	X-RAY DIFFRACTION	126	G	53 - 61
127	X-RAY DIFFRACTION	127	G	62 - 66
128	X-RAY DIFFRACTION	128	G	67 - 79
129	X-RAY DIFFRACTION	129	G	80 - 93
130	X-RAY DIFFRACTION	130	G	94 - 98
131	X-RAY DIFFRACTION	131	G	99 - 110
132	X-RAY DIFFRACTION	132	G	111 - 116
133	X-RAY DIFFRACTION	133	G	117 - 122
134	X-RAY DIFFRACTION	134	G	123 - 139
135	X-RAY DIFFRACTION	135	G	140 - 147
136	X-RAY DIFFRACTION	136	G	148 - 158
137	X-RAY DIFFRACTION	137	G	159 - 173
138	X-RAY DIFFRACTION	138	G	174 - 182
139	X-RAY DIFFRACTION	139	G	183 - 188
140	X-RAY DIFFRACTION	140	G	189 - 204
141	X-RAY DIFFRACTION	141	H	2 - 7
142	X-RAY DIFFRACTION	142	H	8 - 19
143	X-RAY DIFFRACTION	143	H	20 - 28
144	X-RAY DIFFRACTION	144	H	29 - 42
145	X-RAY DIFFRACTION	145	H	43 - 50
146	X-RAY DIFFRACTION	146	H	51 - 61
147	X-RAY DIFFRACTION	147	H	62 - 71
148	X-RAY DIFFRACTION	148	H	72 - 86
149	X-RAY DIFFRACTION	149	H	87 - 101
150	X-RAY DIFFRACTION	150	H	102 - 113
151	X-RAY DIFFRACTION	151	H	114 - 130
152	X-RAY DIFFRACTION	152	H	131 - 141
153	X-RAY DIFFRACTION	153	H	142 - 147
154	X-RAY DIFFRACTION	154	H	148 - 156
155	X-RAY DIFFRACTION	155	H	157 - 165
156	X-RAY DIFFRACTION	156	H	166 - 171
157	X-RAY DIFFRACTION	157	H	172 - 178
158	X-RAY DIFFRACTION	158	H	179 - 187
159	X-RAY DIFFRACTION	159	H	188 - 197
160	X-RAY DIFFRACTION	160	H	198 - 204