温度: 298 K / 手法: microbatch under oil / pH: 6.8 詳細: 25 mM HEPES, 325 mM NaCl, 20% PEG. PEG increased to 30% for cryo. Soaked with THF under anaerobic conditions. , pH 6.8, Microbatch under oil, temperature 298K
解像度: 1.6→36.11 Å / Cor.coef. Fo:Fc: 0.977 / Cor.coef. Fo:Fc free: 0.962 / SU B: 2.966 / SU ML: 0.048 / Isotropic thermal model: ANISOTROPIC / 交差検証法: THROUGHOUT / ESU R Free: 0.078 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.17645
2389
2.5 %
RANDOM
Rwork
0.12641
-
-
-
obs
0.12762
94862
98.65 %
-
all
-
98575
-
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: BABINET MODEL WITH MASK