Mass: 18.015 Da / Num. of mol.: 681 / Source method: isolated from a natural source / Formula: H2O
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Details
Sequence details
THE SEQUENCE DATABASE REFERENCES FOR THREE ENTITIES DO NOT CURRENTLY EXIST. THE AUTHOR WILL BE ...THE SEQUENCE DATABASE REFERENCES FOR THREE ENTITIES DO NOT CURRENTLY EXIST. THE AUTHOR WILL BE SUBMITTED THE SEQUENCE TO THE DATABASE IN THE FUTURE.
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 2
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Sample preparation
Crystal
Density Matthews: 2.23 Å3/Da / Density % sol: 44.86 %
Crystal grow
Details: VAPOR DIFFUSION, HANGING DROP
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Data collection
Diffraction
ID
Mean temperature (K)
Crystal-ID
1
110
1
2
110
1
Diffraction source
Source
Site
Beamline
ID
SYNCHROTRON
NSRRC
BL13B1
1
SYNCHROTRON
SPring-8
BL26B2
2
Detector
Type
ID
Detector
Date
ADSC QUANTUM 315
1
CCD
Jan 5, 2009
ADSC QUANTUM 315r
2
CCD
Feb 23, 2009
Radiation
ID
Protocol
Monochromatic (M) / Laue (L)
Scattering type
Wavelength-ID
1
SINGLEWAVELENGTH
M
x-ray
1
2
SINGLEWAVELENGTH
M
x-ray
1
Radiation wavelength
Relative weight: 1
Reflection
Resolution: 2.05→30 Å / Num. obs: 112128 / % possible obs: 97.6 % / Redundancy: 3.6 % / Rmerge(I) obs: 0.083 / Rsym value: 0.067 / Net I/σ(I): 15.6
Reflection shell
Resolution: 2.05→2.12 Å / Redundancy: 2.5 % / Rmerge(I) obs: 0.261 / Mean I/σ(I) obs: 3.8 / Rsym value: 0.25 / % possible all: 83.1
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Processing
Software
Name
Classification
CNS
refinement
HKL-2000
datareduction
HKL-2000
datascaling
CNS
phasing
Refinement
Method to determine structure: MOLECULAR REPLACEMENT Starting model: 3OR1
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