ソフトウェア | 名称 | バージョン | 分類 |
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SBC-Collect | | データ収集 | PHENIX | | モデル構築 | REFMAC | 5.5.0102精密化 | HKL-3000 | | データ削減 | HKL-3000 | | データスケーリング | PHENIX | | 位相決定 | |
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精密化 | 構造決定の手法: 単波長異常分散 / 解像度: 1.95→50 Å / Cor.coef. Fo:Fc: 0.974 / Cor.coef. Fo:Fc free: 0.947 / SU B: 7.566 / SU ML: 0.103 / TLS residual ADP flag: LIKELY RESIDUAL / 交差検証法: THROUGHOUT / σ(F): 0 / ESU R: 0.207 / ESU R Free: 0.162 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
| Rfactor | 反射数 | %反射 | Selection details |
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Rfree | 0.19921 | 1457 | 5.1 % | RANDOM |
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Rwork | 0.14518 | - | - | - |
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all | 0.14792 | 28740 | - | - |
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obs | 0.14792 | 28740 | 99.58 % | - |
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溶媒の処理 | イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK |
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原子変位パラメータ | Biso mean: 10.118 Å2
| Baniso -1 | Baniso -2 | Baniso -3 |
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1- | -0.39 Å2 | 0 Å2 | 0.66 Å2 |
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2- | - | 0.62 Å2 | 0 Å2 |
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3- | - | - | 0.27 Å2 |
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精密化ステップ | サイクル: LAST / 解像度: 1.95→50 Å
| タンパク質 | 核酸 | リガンド | 溶媒 | 全体 |
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原子数 | 4000 | 0 | 10 | 440 | 4450 |
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拘束条件 | Refine-ID | タイプ | Dev ideal | Dev ideal target | 数 |
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X-RAY DIFFRACTION | r_bond_refined_d0.012 | 0.022 | 4224 | X-RAY DIFFRACTION | r_bond_other_d | | | X-RAY DIFFRACTION | r_angle_refined_deg1.275 | 1.971 | 5734 | X-RAY DIFFRACTION | r_angle_other_deg | | | X-RAY DIFFRACTION | r_dihedral_angle_1_deg5.648 | 5 | 528 | X-RAY DIFFRACTION | r_dihedral_angle_2_deg31.376 | 22.273 | 220 | X-RAY DIFFRACTION | r_dihedral_angle_3_deg13.368 | 15 | 719 | X-RAY DIFFRACTION | r_dihedral_angle_4_deg18.725 | 15 | 63 | X-RAY DIFFRACTION | r_chiral_restr0.091 | 0.2 | 638 | X-RAY DIFFRACTION | r_gen_planes_refined0.005 | 0.021 | 3299 | X-RAY DIFFRACTION | r_gen_planes_other | | | X-RAY DIFFRACTION | r_nbd_refined | | | X-RAY DIFFRACTION | r_nbd_other | | | X-RAY DIFFRACTION | r_nbtor_refined | | | X-RAY DIFFRACTION | r_nbtor_other | | | X-RAY DIFFRACTION | r_xyhbond_nbd_refined | | | X-RAY DIFFRACTION | r_xyhbond_nbd_other | | | X-RAY DIFFRACTION | r_metal_ion_refined | | | X-RAY DIFFRACTION | r_metal_ion_other | | | X-RAY DIFFRACTION | r_symmetry_vdw_refined | | | X-RAY DIFFRACTION | r_symmetry_vdw_other | | | X-RAY DIFFRACTION | r_symmetry_hbond_refined | | | X-RAY DIFFRACTION | r_symmetry_hbond_other | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_refined | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_other | | | X-RAY DIFFRACTION | r_mcbond_it0.584 | 1.5 | 2591 | X-RAY DIFFRACTION | r_mcbond_other | | | X-RAY DIFFRACTION | r_mcangle_it1.053 | 2 | 4176 | X-RAY DIFFRACTION | r_scbond_it1.744 | 3 | 1633 | X-RAY DIFFRACTION | r_scangle_it2.833 | 4.5 | 1558 | X-RAY DIFFRACTION | r_rigid_bond_restr | | | X-RAY DIFFRACTION | r_sphericity_free | | | X-RAY DIFFRACTION | r_sphericity_bonded | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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LS精密化 シェル | 解像度: 1.948→1.999 Å / Total num. of bins used: 20
| Rfactor | 反射数 | %反射 |
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Rfree | 0.222 | 98 | - |
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Rwork | 0.15 | 1921 | - |
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obs | - | 2019 | 95.96 % |
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精密化 TLS | 手法: refined / Refine-ID: X-RAY DIFFRACTION ID | L11 (°2) | L12 (°2) | L13 (°2) | L22 (°2) | L23 (°2) | L33 (°2) | S11 (Å °) | S12 (Å °) | S13 (Å °) | S21 (Å °) | S22 (Å °) | S23 (Å °) | S31 (Å °) | S32 (Å °) | S33 (Å °) | T11 (Å2) | T12 (Å2) | T13 (Å2) | T22 (Å2) | T23 (Å2) | T33 (Å2) | Origin x (Å) | Origin y (Å) | Origin z (Å) |
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1 | 2.9545 | -1.4588 | -1.6942 | 3.6753 | 0.0488 | 1.6614 | 0.1018 | 0.3077 | 0.0791 | -0.1191 | 0.022 | 0.0267 | 0.0536 | -0.2264 | -0.1238 | 0.039 | -0.0106 | -0.0232 | 0.0846 | 0.0219 | 0.028 | 11.9928 | 22.9727 | -8.4723 | 2 | 8.9199 | -1.3294 | -0.9242 | 0.3532 | -0.255 | 0.9273 | -0.0854 | 0.2228 | -0.7512 | -0.067 | -0.026 | 0.1021 | 0.0974 | -0.0057 | 0.1114 | 0.0999 | 0.009 | 0.0059 | 0.0545 | -0.0147 | 0.101 | 31.9205 | 11.9949 | -8.2095 | 3 | 3.1522 | 0.558 | -0.5198 | 2.4207 | -0.9265 | 3.9219 | 0.028 | 0.0811 | 0.1324 | -0.1919 | -0.1787 | -0.1258 | 0.0548 | 0.1349 | 0.1507 | 0.057 | 0.0297 | 0.0085 | 0.0564 | 0.0265 | 0.0269 | 34.57 | 24.8935 | -8.8494 | 4 | 1.7153 | -0.2904 | 0.4993 | 0.864 | 0.0194 | 3.2243 | 0.0182 | -0.0557 | -0.1161 | -0.0211 | -0.0849 | -0.1176 | 0.103 | 0.232 | 0.0667 | 0.0395 | 0.0211 | 0.0035 | 0.0481 | 0.0232 | 0.0526 | 38.6275 | 15.8467 | 2.0251 | 5 | 4.4479 | 0.569 | -0.053 | 8.1264 | -0.7078 | -0.6103 | -0.0591 | -0.1323 | 0.4554 | 0.1268 | 0.0607 | 0.1022 | -0.0972 | -0.0196 | -0.0016 | 0.1345 | 0.0196 | -0.0097 | 0.0886 | -0.0126 | 0.0882 | 28.1707 | 30.7083 | 2.7848 | 6 | 5.2759 | -0.5061 | -1.9192 | 3.4853 | -0.676 | 4.2947 | 0.1725 | 0.0841 | 0.4136 | -0.1118 | -0.1383 | 0.0054 | -0.3785 | 0.3157 | -0.0343 | 0.1298 | -0.0463 | -0.0201 | 0.0595 | -0.0102 | 0.185 | 37.0596 | 34.9933 | 2.0916 | 7 | 4.3075 | -1.7925 | -1.8854 | 0.6687 | 0.4899 | 2.7682 | -0.0706 | -0.3486 | 0.2217 | 0.0682 | 0.1484 | -0.0163 | -0.1192 | 0.0974 | -0.0778 | 0.0926 | -0.0081 | -0.0239 | 0.0709 | -0.0248 | 0.0733 | 33.714 | 26.0167 | 13.6115 | 8 | 4.4335 | 2.2789 | -1.7172 | 4.0391 | -1.8213 | 1.948 | 0.0104 | -0.2418 | 0.1142 | 0.0262 | -0.0256 | 0.0433 | 0.2259 | 0.1121 | 0.0151 | 0.0723 | 0.0139 | -0.0107 | 0.0757 | -0.009 | 0.0375 | 35.4595 | 22.272 | 7.9139 | 9 | 7.4484 | 0.693 | 1.6424 | 0.1085 | -0.0399 | 0.9913 | 0.2541 | -0.312 | -0.6392 | 0.0425 | -0.0797 | 0.015 | 0.1068 | -0.1375 | -0.1744 | 0.1208 | -0.0231 | -0.0026 | 0.152 | 0.0041 | 0.1634 | 15.623 | 10.9254 | 6.2419 | 10 | 2.8415 | -0.3129 | -0.857 | 4.0595 | -0.0604 | 2.2318 | 0.0925 | -0.1411 | 0.1355 | 0.2517 | -0.1201 | 0.0393 | -0.1225 | -0.0189 | 0.0276 | 0.0945 | -0.0221 | 0.0199 | 0.0787 | -0.0268 | 0.0181 | 13.1174 | 23.8719 | 8.9004 | 11 | 0.63 | 0.3931 | 0.8537 | 0.9225 | -0.8139 | 2.9046 | 0.061 | 0.049 | -0.0064 | 0.0355 | 0.0358 | 0.0959 | 0.0553 | -0.1407 | -0.0969 | 0.0499 | -0.0047 | 0.0035 | 0.1075 | -0.0034 | 0.0819 | 9.267 | 16.3296 | -2.8153 | 12 | 3.1753 | -0.6069 | 0.6967 | 8.5563 | -2.0269 | 4.3491 | 0.1512 | 0.0181 | 0.4571 | 0.1275 | -0.1263 | -0.0027 | -0.4021 | 0.1774 | -0.0249 | 0.0784 | -0.0099 | 0.0319 | 0.0732 | 0.008 | 0.0868 | 19.5762 | 30.9876 | -2.2423 | 13 | 3.5399 | -0.739 | -3.8386 | 2.8477 | -0.6822 | 8.0724 | 0.1009 | -0.2108 | 0.69 | 0.1391 | -0.0564 | -0.0694 | -0.3283 | -0.0568 | -0.0444 | 0.1633 | 0.0127 | 0.016 | 0.0865 | -0.0414 | 0.3101 | 10.4698 | 35.5855 | -0.7121 | 14 | 5.7967 | 2.2607 | -1.4106 | 2.5301 | -0.7415 | 1.4444 | 0.0539 | 0.3549 | 0.1463 | -0.0667 | 0.0247 | -0.126 | -0.0955 | -0.0554 | -0.0786 | 0.0705 | 0.029 | -0.0066 | 0.1121 | 0.0634 | 0.063 | 13.4954 | 27.5138 | -13.4412 | 15 | 4.7372 | -2.0848 | -2.3556 | 5.0963 | 0.3121 | 3.3192 | 0.0505 | 0.1473 | -0.1776 | -0.1982 | -0.0601 | 0.1028 | 0.1215 | -0.1346 | 0.0096 | 0.0449 | -0.0226 | -0.0395 | 0.0396 | -0.0066 | 0.0306 | 0.7458 | 41.6069 | 21.1943 | 16 | 5.5003 | -3.1409 | -1.393 | 1.5632 | 0.4942 | 0.1808 | 0.1087 | 0.0141 | -0.3387 | -0.0094 | -0.0825 | 0.0916 | -0.0309 | -0.0082 | -0.0262 | 0.185 | 0.0149 | -0.0206 | 0.1263 | -0.006 | 0.1659 | 20.8737 | 30.3902 | 21.306 | 17 | 3.0158 | 1.1461 | -0.3631 | 2.7863 | -0.3124 | 2.9295 | 0.0178 | 0.0666 | -0.0339 | -0.0943 | -0.0703 | -0.1215 | 0.0443 | 0.0774 | 0.0524 | 0.0523 | 0.021 | 0.0038 | 0.0618 | 0.025 | 0.0509 | 23.4018 | 43.6871 | 20.5774 | 18 | 2.0477 | -0.1947 | 0.0051 | 1.0402 | 1.0097 | 2.4868 | 0.0249 | 0.0187 | -0.1124 | 0.072 | 0.0998 | -0.0935 | 0.1202 | 0.1096 | -0.1246 | 0.0333 | 0.0152 | -0.016 | 0.0247 | -0.0052 | 0.0524 | 27.1552 | 34.6211 | 31.7499 | 19 | 3.4648 | -0.0261 | 0.6915 | 2.5807 | 0.1592 | 2.0738 | -0.0111 | -0.1706 | 0.272 | 0.0242 | -0.0207 | -0.0602 | -0.1924 | -0.0706 | 0.0318 | 0.0413 | -0.0032 | -0.0111 | 0.0503 | -0.0025 | 0.0577 | 17.1141 | 49.605 | 32.5232 | 20 | 3.6442 | -0.1517 | -2.6132 | 3.0138 | 0.3752 | 1.849 | 0.0887 | 0.0013 | 0.3764 | 0.0046 | -0.169 | -0.0679 | -0.1817 | 0.3102 | 0.0803 | 0.1717 | -0.0315 | -0.0445 | 0.1588 | 0.0414 | 0.2294 | 26.1807 | 53.7501 | 31.7129 | 21 | 3.148 | -0.0781 | -1.526 | -0.3723 | -0.4212 | 2.6293 | 0.1572 | -0.0221 | 0.1306 | -0.0252 | -0.0421 | 0.1026 | -0.0093 | -0.0249 | -0.1151 | 0.1186 | -0.0069 | -0.0279 | 0.1271 | -0.0827 | 0.1407 | 23.0562 | 44.7508 | 43.0155 | 22 | 5.5578 | 3.1545 | -1.993 | 7.0821 | -0.5999 | 0.7517 | 0.1038 | -0.2442 | -0.0246 | 0.2813 | -0.0951 | 0.2208 | 0.1004 | 0.0417 | -0.0087 | 0.0673 | 0.0154 | -0.0458 | 0.0792 | -0.0188 | 0.0439 | 24.4177 | 41.0594 | 37.342 | 23 | 8.8628 | 2.421 | 0.2649 | 0.9595 | 0.0072 | 0.5068 | 0.1031 | -0.3219 | -0.4913 | -0.0237 | -0.0671 | -0.0038 | 0.048 | -0.0354 | -0.036 | 0.1287 | 0.0026 | -0.0017 | 0.0867 | 0.0163 | 0.1366 | 4.2915 | 30.1164 | 36.3838 | 24 | 3.3094 | -1.2935 | -0.6931 | 3.301 | 0.2958 | 2.6733 | 0.0079 | -0.0789 | 0.0665 | 0.2577 | -0.0182 | -0.0496 | -0.0614 | 0.0683 | 0.0102 | 0.0662 | -0.0272 | 0.0085 | 0.0692 | -0.0074 | 0.0029 | 2.1237 | 43.193 | 38.3352 | 25 | 1.7292 | 0.0008 | 0.8341 | 1.4647 | -1.5393 | 3.3984 | 0.0939 | -0.0153 | -0.1625 | -0.1015 | 0.0181 | 0.1199 | 0.2367 | -0.1623 | -0.112 | 0.0412 | -0.0141 | -0.0066 | 0.0226 | -0.0058 | 0.0626 | -2.0604 | 35.3114 | 26.9158 | 26 | 2.7961 | -1.3901 | 0.446 | 4.5687 | 0.2183 | 2.472 | 0.0366 | 0.0517 | 0.3285 | -0.0252 | -0.0162 | -0.1638 | -0.2811 | 0.0961 | -0.0205 | 0.045 | -0.0161 | 0.0128 | 0.0467 | 0.0045 | 0.0416 | 8.3771 | 50.1875 | 27.084 | 27 | 3.3997 | -0.755 | -1.2296 | 4.1538 | -0.2591 | 4.1684 | 0.0626 | -0.0341 | 0.1898 | -0.0704 | -0.1417 | 0.0714 | -0.165 | -0.2102 | 0.0791 | 0.1026 | 0.0175 | 0.0227 | 0.0348 | -0.0116 | 0.1055 | -0.8013 | 54.6256 | 28.472 | 28 | 5.6909 | 1.3772 | -4.0008 | 4.0288 | -1.139 | 1.5378 | 0.1039 | 0.3801 | 0.225 | -0.1317 | 0.0392 | 0.0101 | -0.0433 | -0.2019 | -0.143 | 0.1089 | 0.0145 | -0.0283 | 0.0942 | 0.0177 | 0.0223 | 2.3499 | 46.3922 | 15.9193 |
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精密化 TLSグループ | ID | Refine-ID | Refine TLS-ID | Auth asym-ID | Auth seq-ID |
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1 | X-RAY DIFFRACTION | 1 | A1 - 12 | 2 | X-RAY DIFFRACTION | 2 | A13 - 34 | 3 | X-RAY DIFFRACTION | 3 | A35 - 50 | 4 | X-RAY DIFFRACTION | 4 | A51 - 78 | 5 | X-RAY DIFFRACTION | 5 | A79 - 90 | 6 | X-RAY DIFFRACTION | 6 | A91 - 109 | 7 | X-RAY DIFFRACTION | 7 | A110 - 121 | 8 | X-RAY DIFFRACTION | 8 | B1 - 12 | 9 | X-RAY DIFFRACTION | 9 | B13 - 34 | 10 | X-RAY DIFFRACTION | 10 | B35 - 50 | 11 | X-RAY DIFFRACTION | 11 | B51 - 78 | 12 | X-RAY DIFFRACTION | 12 | B79 - 90 | 13 | X-RAY DIFFRACTION | 13 | B91 - 109 | 14 | X-RAY DIFFRACTION | 14 | B110 - 121 | 15 | X-RAY DIFFRACTION | 15 | C1 - 12 | 16 | X-RAY DIFFRACTION | 16 | C13 - 34 | 17 | X-RAY DIFFRACTION | 17 | C35 - 50 | 18 | X-RAY DIFFRACTION | 18 | C51 - 78 | 19 | X-RAY DIFFRACTION | 19 | C79 - 90 | 20 | X-RAY DIFFRACTION | 20 | C91 - 109 | 21 | X-RAY DIFFRACTION | 21 | C110 - 121 | 22 | X-RAY DIFFRACTION | 22 | D1 - 12 | 23 | X-RAY DIFFRACTION | 23 | D13 - 34 | 24 | X-RAY DIFFRACTION | 24 | D35 - 50 | 25 | X-RAY DIFFRACTION | 25 | D51 - 78 | 26 | X-RAY DIFFRACTION | 26 | D79 - 90 | 27 | X-RAY DIFFRACTION | 27 | D91 - 109 | 28 | X-RAY DIFFRACTION | 28 | D110 - 121 | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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