タイプ: ADSC QUANTUM 4 / 検出器: CCD / 日付: 2006年9月15日 詳細: Variable vertical and fixed horizontal slits. KOHZU double crystal monochromator with a water-cooled flat first crystal and a sagittally focused second crystal positioned for a fixed exit ...詳細: Variable vertical and fixed horizontal slits. KOHZU double crystal monochromator with a water-cooled flat first crystal and a sagittally focused second crystal positioned for a fixed exit beam condition. Located ~18 m from source and ~6 m from sample position. Mirror system consisting of two vertically stacked, fused silica, spherical mirrors, to provide vertical focusing and harmonic rejection. One of the mirrors is rhodium coated and the other is uncoated. Located ~19.7 m from source.
放射
モノクロメーター: KOHZU double crystal monochromator with a water-cooled flat first crystal and a sagittally focused second crystal positioned for a fixed exit beam condition. Located ~18 m ...モノクロメーター: KOHZU double crystal monochromator with a water-cooled flat first crystal and a sagittally focused second crystal positioned for a fixed exit beam condition. Located ~18 m from source and ~6 m from sample position. プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 0.9797 Å / 相対比: 1
反射
解像度: 1.75→30 Å / Num. obs: 48051 / % possible obs: 97.2 % / Observed criterion σ(I): -3 / 冗長度: 1.7 % / Rmerge(I) obs: 0.056 / Net I/σ(I): 12.2
反射 シェル
解像度: 1.75→1.81 Å / 冗長度: 1.6 % / Rmerge(I) obs: 0.334 / Mean I/σ(I) obs: 2 / Num. unique all: 9414 / % possible all: 93.8