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- PDB-2ymd: Crystal structure of a mutant binding protein (5HTBP-AChBP) in co... -

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Open data

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Basic information

Entry

Database: PDB / ID: 2ymd

Title

Crystal structure of a mutant binding protein (5HTBP-AChBP) in complex with serotonin (5-hydroxytryptamine)

Components

SOLUBLE ACETYLCHOLINE RECEPTOR

Keywords

RECEPTOR / PENTAMERIC LIGAND-GATED ION CHANNEL

Function / homology

Function and homology information

extracellular ligand-gated monoatomic ion channel activity / transmembrane signaling receptor activity / metal ion binding / identical protein binding / membrane
Similarity search - Function

Biological species

APLYSIA CALIFORNICA (California sea hare)

Method

X-RAY DIFFRACTION /

SYNCHROTRON /

MOLECULAR REPLACEMENT / Resolution: 1.96 Å

Authors

Kesters, D. / Thompson, A.J. / Brams, M. / Elk, R.v. / Spurny, R. / Geitmann, M. / Villalgordo, J.M. / Guskov, A. / Danielson, U.H. / Lummis, S.C.R. ...

Citation

Journal: Embo Rep. / Year: 2013
Title: Structural Basis of Ligand Recognition in 5-Ht(3) Receptors.
Authors: Kesters, D. / Thompson, A.J. / Brams, M. / Van Elk, R. / Spurny, R. / Geitmann, M. / Villalgordo, J.M. / Guskov, A. / Helena Danielson, U. / Lummis, S.C. / Smit, A.B. / Ulens, C.

History

Deposition	Oct 9, 2012	Deposition site: PDBE / Processing site: PDBE
Revision 1.0	Dec 12, 2012	Provider: repository / Type: Initial release
Revision 1.1	Jan 30, 2013	Group: Database references
Revision 1.2	Dec 20, 2023	Group: Data collection / Database references ...Data collection / Database references / Derived calculations / Other / Refinement description Category: chem_comp_atom / chem_comp_bond ...chem_comp_atom / chem_comp_bond / database_2 / pdbx_database_status / pdbx_initial_refinement_model / struct_site Item: _database_2.pdbx_DOI / _database_2.pdbx_database_accession ..._database_2.pdbx_DOI / _database_2.pdbx_database_accession / _pdbx_database_status.status_code_sf / _struct_site.pdbx_auth_asym_id / _struct_site.pdbx_auth_comp_id / _struct_site.pdbx_auth_seq_id
Revision 1.3	Nov 13, 2024	Group: Structure summary / Category: pdbx_entry_details / pdbx_modification_feature / Item: _pdbx_entry_details.has_protein_modification

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Structure visualization

Structure viewer	Molecule: MolmilJmol/JSmol

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Downloads & links

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Download

PDBx/mmCIF format	2ymd.cif.gz	896.6 KB	Display	PDBx/mmCIF format
PDB format	pdb2ymd.ent.gz	758.7 KB	Display	PDB format
PDBx/mmJSON format	2ymd.json.gz		Tree view	PDBx/mmJSON format
Others	Other downloads

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Validation report

Summary document	2ymd_validation.pdf.gz	550.4 KB	Display	wwPDB validaton report
Full document	2ymd_full_validation.pdf.gz	568.2 KB	Display
Data in XML	2ymd_validation.xml.gz	105.6 KB	Display
Data in CIF	2ymd_validation.cif.gz	153.2 KB	Display
Arichive directory	https://data.pdbj.org/pub/pdb/validation_reports/ym/2ymd ftp://data.pdbj.org/pub/pdb/validation_reports/ym/2ymd	HTTPS FTP

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Related structure data

Related structure data	2ymeC 2xysS 2br7 2br8 2byn 2byp 2byq 2byr 2bys 2c9t 2uz6 2w8f 2w8g 2wn9 2wnc 2wnj 2wnl 2wzy 2x00 2xnt 2xnu 2xnv 2xyt 2xz5 2xz6 2y54 2y56 2y57 2y58 2y7y 4aft 4afw PDB Unreleased entry 4bqt S: Starting model for refinement C: citing same article (ref.)
Similar structure data	22390 22358 22382 6y5a-d 22391 6ur8-d 6uvr-d 5jyx-d Search similar-shape structures by Omokage search (details) Search similar-shape structures by Omokage search (details) Search similar-shape structures by Omokage search (details) Similarity search - Function & homologyF&H Search Similarity search - FunctionF&H Search Similarity search - HomologyF&H Search

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Links

PDB pages	PDBj / wwPDB / NCBI
Related items in Molecule of the Month	#191 - Nov 2015 Glutamate-gated Chloride Receptors similarity (4) #71 - Nov 2005 Acetylcholine Receptor similarity (4)

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Assembly

Deposited unit

A: SOLUBLE ACETYLCHOLINE RECEPTOR

B: SOLUBLE ACETYLCHOLINE RECEPTOR

C: SOLUBLE ACETYLCHOLINE RECEPTOR

D: SOLUBLE ACETYLCHOLINE RECEPTOR

E: SOLUBLE ACETYLCHOLINE RECEPTOR

F: SOLUBLE ACETYLCHOLINE RECEPTOR

G: SOLUBLE ACETYLCHOLINE RECEPTOR

H: SOLUBLE ACETYLCHOLINE RECEPTOR

I: SOLUBLE ACETYLCHOLINE RECEPTOR

J: SOLUBLE ACETYLCHOLINE RECEPTOR

hetero molecules

245 kDa, 10 polymers
Search similar-shape structures of this assembly by Omokage search (details)

Idetical with deposited unit
defined by software

A: SOLUBLE ACETYLCHOLINE RECEPTOR

B: SOLUBLE ACETYLCHOLINE RECEPTOR

C: SOLUBLE ACETYLCHOLINE RECEPTOR

D: SOLUBLE ACETYLCHOLINE RECEPTOR

E: SOLUBLE ACETYLCHOLINE RECEPTOR

hetero molecules

defined by software
123 kDa, 5 polymers
Search similar-shape structures of this assembly by Omokage search (details)

F: SOLUBLE ACETYLCHOLINE RECEPTOR

G: SOLUBLE ACETYLCHOLINE RECEPTOR

H: SOLUBLE ACETYLCHOLINE RECEPTOR

I: SOLUBLE ACETYLCHOLINE RECEPTOR

J: SOLUBLE ACETYLCHOLINE RECEPTOR

hetero molecules

defined by software
122 kDa, 5 polymers
Search similar-shape structures of this assembly by Omokage search (details)

Unit cell

Length a, b, c (Å)	203.565, 140.064, 126.528
Angle α, β, γ (deg.)	90.00, 99.08, 90.00
Int Tables number	5
Space group name H-M	C121

Noncrystallographic symmetry (NCS)

NCS oper: (Code: given
Matrix: (-1, -0.029, -0.004), (-0.024, 0.725, 0.689), (-0.017, 0.689, -0.725)
Vector: 52.963, 0.539, 0.403)

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Components

#1: Protein	SOLUBLE ACETYLCHOLINE RECEPTOR / ACHBP Mass: 24092.885 Da / Num. of mol.: 10 / Fragment: ACETYLCHOLINE BINDING DOMAIN, RESIDUES 20-231 / Mutation: YES Source method: isolated from a genetically manipulated source Source: (gene. exp.) APLYSIA CALIFORNICA (California sea hare) Production host: SPODOPTERA FRUGIPERDA (fall armyworm) / Strain (production host): SF21 / References: UniProt: Q8WSF8
#2: Chemical	ChemComp-SRO / SEROTONIN / 3-(2-AMINOETHYL)-1H-INDOL-5-OL Mass: 176.215 Da / Num. of mol.: 10 / Source method: obtained synthetically / Formula: C₁₀H₁₂N₂O
#3: Chemical	ChemComp-GOL / GLYCEROL / GLYCERIN / PROPANE-1,2,3-TRIOL Mass: 92.094 Da / Num. of mol.: 14 / Source method: obtained synthetically / Formula: C₃H₈O₃
#4: Chemical	ChemComp-PO4 / PHOSPHATE ION Mass: 94.971 Da / Num. of mol.: 10 / Source method: obtained synthetically / Formula: PO₄
#5: Water	ChemComp-HOH / water Mass: 18.015 Da / Num. of mol.: 2665 / Source method: isolated from a natural source / Formula: H₂O
Has protein modification	Y
Nonpolymer details	SEROTONIN (SRO): SYNONYM 5-HYDROXYTRYPTAMINE
Sequence details	THE CONFLICTS BETWEEN THE UNIPROT AND PROTEIN SEQUENCE ARE DUE TO DIFFERENCES IN THE CLONING METHOD ...THE CONFLICTS BETWEEN THE UNIPROT AND PROTEIN SEQUENCE ARE DUE TO DIFFERENCES IN THE CLONING METHOD USED TO OBTAIN THE GENE.

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Experimental details

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Experiment

Experiment	Method: X-RAY DIFFRACTION / Number of used crystals: 1

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Sample preparation

Crystal	Density Matthews: 3.21 Å³/Da / Density % sol: 61.41 % / Description: NONE
Crystal grow	Details: 400 MM (NH4)H2PO4

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Data collection

Diffraction	Mean temperature: 100 K
Diffraction source	Source: SYNCHROTRON / Site: SLS / Beamline: X06SA / Wavelength: 1
Detector	Type: DECTRIS PILATUS 6M / Detector: PIXEL / Date: Jun 2, 2011
Radiation	Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength	Wavelength: 1 Å / Relative weight: 1
Reflection	Resolution: 1.96→46.9 Å / Num. obs: 249028 / % possible obs: 99.6 % / Observed criterion σ(I): 1 / Redundancy: 3.8 % / B_iso Wilson estimate: 22.28 Å² / R_merge(I) obs: 0.01 / Net I/σ(I): 6.4
Reflection shell	Resolution: 1.96→2.19 Å / Redundancy: 3.6 % / R_merge(I) obs: 0.08 / Mean I/σ(I) obs: 1 / % possible all: 99.6

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Processing

Software

Name	Version	Classification
PHENIX	(PHENIX.REFINE)	refinement
XDS		data reduction
SCALA		data scaling
MOLREP		phasing

Refinement

Method to determine structure:

MOLECULAR REPLACEMENT
Starting model: PDB ENTRY 2XYS

2xys

Resolution: 1.96→46.903 Å / SU ML: 0.18 / σ(F): 1.42 / Phase error: 19.56 / Stereochemistry target values: ML

	R_factor	Num. reflection	% reflection
R_free	0.2011	2294	1 %
R_work	0.1591	-	-
obs	0.1595	239406	95.78 %

Solvent computation

Shrinkage radii: 1 Å / VDW probe radii: 1.2 Å / Solvent model: FLAT BULK SOLVENT MODEL / B_sol: 2 Å² / k_sol: 2 e/Å³

Displacement parameters

B_iso mean: 29.2 Å²

Refinement step

Cycle: LAST / Resolution: 1.96→46.903 Å

	Protein	Nucleic acid	Ligand	Solvent	Total
Num. atoms	16864	0	264	2665	19793

Refine LS restraints

Refine-ID	Type	Dev ideal	Number
X-RAY DIFFRACTION	f_bond_d	0.007	17569
X-RAY DIFFRACTION	f_angle_d	1.061	23927
X-RAY DIFFRACTION	f_dihedral_angle_d	14.086	6321
X-RAY DIFFRACTION	f_chiral_restr	0.073	2624
X-RAY DIFFRACTION	f_plane_restr	0.005	3067

LS refinement shell

Resolution (Å)	R_factor R_free	Num. reflection R_free	R_factor R_work	Num. reflection R_work	Refine-ID	% reflection obs (%)
1.9609-2.0036	0.2862	120	0.2593	12058	X-RAY DIFFRACTION	78
2.0036-2.0502	0.3124	138	0.2356	13761	X-RAY DIFFRACTION	89
2.0502-2.1014	0.2243	136	0.2121	14212	X-RAY DIFFRACTION	92
2.1014-2.1583	0.2371	138	0.1995	14470	X-RAY DIFFRACTION	94
2.1583-2.2218	0.2327	144	0.1968	14718	X-RAY DIFFRACTION	95
2.2218-2.2935	0.238	144	0.1888	14802	X-RAY DIFFRACTION	96
2.2935-2.3754	0.2379	143	0.1764	14981	X-RAY DIFFRACTION	97
2.3754-2.4706	0.2323	147	0.1739	15090	X-RAY DIFFRACTION	98
2.4706-2.583	0.238	146	0.173	15098	X-RAY DIFFRACTION	98
2.583-2.7191	0.2193	147	0.1661	15157	X-RAY DIFFRACTION	98
2.7191-2.8895	0.2228	146	0.1582	15304	X-RAY DIFFRACTION	99
2.8895-3.1125	0.1932	146	0.1483	15367	X-RAY DIFFRACTION	99
3.1125-3.4257	0.1762	150	0.1364	15463	X-RAY DIFFRACTION	100
3.4257-3.9212	0.1767	148	0.1301	15427	X-RAY DIFFRACTION	100
3.9212-4.9394	0.1365	149	0.1161	15559	X-RAY DIFFRACTION	100
4.9394-46.9162	0.1917	152	0.1641	15645	X-RAY DIFFRACTION	100

Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°²)	L12 (°²)	L13 (°²)	L22 (°²)	L23 (°²)	L33 (°²)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å²)	T12 (Å²)	T13 (Å²)	T22 (Å²)	T23 (Å²)	T33 (Å²)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	2.713	-3.6267	0.5889	6.3552	1.8321	6.7384	0.2181	-0.6945	0.2615	0.3426	-0.0861	-0.1764	-0.1931	0.3744	-0.1153	0.1678	-0.0873	-0.0227	0.3047	-0.0759	0.2767	44.9986	-2.0205	20.4183
2	3.1309	0.8048	1.1776	8.3432	-4.5996	3.3929	-2.1218	0.1609	2.4123	-0.2842	0.4002	-2.0308	-0.2932	-0.0667	1.7311	0.6874	-0.0692	-0.1827	0.702	-0.0403	0.8771	39.0381	8.3864	16.4779
3	8.0521	1.5827	2.9331	2.3371	2.5941	3.0851	0.1258	0.762	0.4757	-0.6869	0.1559	-0.412	-0.7848	0.6758	-0.0717	0.3123	-0.0496	0.0788	0.2913	0.1089	0.3721	28.4662	8.9097	3.6555
4	0.6417	0.6447	0.4831	2.0715	-0.5238	0.6245	0.0176	-0.0496	-0.1758	0.0166	-0.0198	-0.0512	0.053	0.0688	-0.0143	0.1623	-0.018	-0.0184	0.1784	-0.031	0.1177	10.8648	-11.948	13.6799
5	4.9308	4.69	-5.1717	4.513	-4.9361	5.4235	-0.2739	0.2416	-0.3546	-0.395	0.0916	-0.2612	0.6084	0.1589	0.3132	0.2219	-0.0308	0.0295	0.202	-0.024	0.2365	25.635	-8.669	9.9132
6	6.1625	0.3132	0.8692	7.0264	-3.9673	7.2909	0.1402	0.3306	-0.1572	-0.2794	0.1215	-0.4583	0.172	0.4654	-0.2418	0.141	-0.0352	0.0276	0.1866	-0.092	0.1985	44.3832	-4.5435	11.3326
7	3.7572	-0.3592	-0.2109	0.0606	-0.1043	0.5822	-0.08	-0.0792	-0.0191	0.0305	0.0614	-0.0393	-0.0073	0.0958	0.0101	0.1747	-0.0305	-0.0112	0.1532	-0.03	0.1808	23.7747	-4.369	15.8365
8	8.3919	6.6931	-7.4071	7.359	-6.2859	9.7684	0.1941	-0.3209	-0.5921	0.1768	-0.3719	-0.3916	-0.0899	0.4916	0.1611	0.1407	-0.0476	-0.0091	0.1947	-0.0275	0.1881	27.1871	-8.9706	13.7463
9	0.235	-0.8454	-0.0688	2.9303	-0.2754	2.4614	-0.1421	-0.0644	-0.2096	-0.1946	0.08	0.3172	-0.0522	-0.2183	0.0497	0.108	-0.0286	0.0191	0.1304	0.0216	0.1676	3.1867	-13.8356	14.3364
10	2.256	2.4723	-3.5847	3.5302	-4.8105	6.7137	-0.2989	0.366	-0.14	-0.7691	0.1887	0.5474	0.1736	-0.1403	0.0624	0.1807	-0.0178	-0.0151	0.2838	-0.0663	0.2763	0.4864	-20.2228	6.1431
11	3.6269	0.1502	-1.1689	8.0434	-0.0495	2.4657	-0.1123	0.6476	0.3289	-0.5223	0.1042	-0.1544	-0.0081	0.2263	0.0033	0.1675	-0.0415	-0.0451	0.2351	0.0433	0.0934	17.8579	1.0143	4.0525
12	2.1887	1.0923	-1.9031	4.6443	-2.1051	7.9796	-0.0242	0.1534	-0.2598	-0.1294	-0.0236	-0.0568	0.3356	0.1239	0.0581	0.1422	0.0031	-0.0178	0.1237	-0.0614	0.1527	13.2593	-20.9027	9.0219
13	3.8163	-0.239	4.6533	3.4066	-1.3042	6.0142	0.144	0.7953	-0.3282	0.3415	-0.3511	0.4603	0.5525	-0.2509	0.041	0.252	-0.0368	0.0188	0.2422	0.0089	0.1408	11.9646	-1.6584	-2.1032
14	6.1899	-6.0488	-0.5539	6.0084	0.8932	2.0361	-0.45	-1.0519	0.4495	0.3294	0.6922	-0.1435	-0.3951	-0.3164	-0.2042	0.2836	0.0013	-0.0476	0.3085	0.0111	0.2137	11.6347	6.9111	0.4859
15	8.5906	6.8027	-5.1611	5.8066	-5.0652	6.156	0.0814	-0.147	0.1404	0.1265	-0.1261	0.4615	0.2504	0.0781	0.1259	0.1894	-0.0381	-0.0034	0.2279	-0.0571	0.1827	6.6951	-17.9804	8.0986
16	2.6257	1.2071	-4.2163	8.8144	-0.9195	7.436	0.1543	-0.3989	-0.1867	0.3819	-0.3647	-0.8769	0.0847	0.4116	0.1753	0.1635	-0.0931	-0.0369	0.3088	0.0622	0.2484	31.2647	17.6037	10.0411
17	3.0665	1.9005	1.5256	2.0876	-1.5775	7.833	1.0653	-2.685	0.5376	-0.3278	-0.9352	0.4813	-0.1233	2.2197	-0.3613	0.5818	-0.0899	0.1448	0.7959	-0.09	0.5121	27.6955	24.4849	19.8763
18	5.5176	-3.5163	-0.3666	2.8324	-1.655	6.6985	-0.046	0.4784	1.0671	-0.5492	0.1846	-0.1879	-0.4886	0.7472	-0.1509	0.4338	-0.1999	0.0105	0.178	0.0075	0.354	12.6363	31.3363	21.5469
19	2.5582	2.333	-0.2857	4.0014	-0.6118	1.2814	-0.0719	0.1383	0.0643	-0.1725	0.1463	0.0737	-0.0366	-0.0044	-0.0557	0.1171	0.0042	-0.0122	0.1348	-0.0089	0.1016	1.0841	9.4049	16.5395
20	7.7563	-0.1318	-2.4905	6.1645	0.982	4.1427	0.1197	0.4421	0.232	-0.3486	-0.2195	-0.1487	-0.3891	0.199	0.0713	0.1837	-0.0746	-0.0282	0.2878	0.0332	0.1341	25.1816	22.1967	5.1127
21	2.5752	0.9986	-1.5916	1.0578	-0.6134	0.9429	-0.0589	0.0134	0.0385	-0.0121	0.0535	-0.0478	-0.0126	0.0313	0.0003	0.1791	-0.0525	-0.0165	0.2096	-0.0088	0.1289	11.1574	13.2446	18.4259
22	9.561	7.2201	-7.3913	5.649	-6.1539	7.3043	0.0439	-0.2668	0.0758	0.2732	-0.2722	0.0674	-0.2494	-0.128	0.222	0.1772	-0.0611	-0.0225	0.1716	-0.0103	0.1552	11.5218	13.3319	11.7884
23	1.5106	-2.0674	-0.524	3.268	1.1495	3.7353	0.0715	-0.1951	-0.1267	-0.0163	0.0182	0.2329	0.0645	-0.3541	-0.1183	0.1365	-0.044	0.0006	0.1443	0.0106	0.1368	-5.9149	3.8846	22.5059
24	5.8731	-2.3032	4.5263	5.6478	-3.162	4.3123	0.5998	-0.0753	-0.5638	0.0884	-0.0356	1.6852	0.1807	-1.182	-0.5027	0.2205	-0.1126	-0.0015	0.5038	-0.0466	0.3647	-20.0382	-1.0427	14.5945
25	4.0739	1.2008	1.8004	0.7477	1.4931	2.794	0.078	-0.1356	0.2447	-0.0118	-0.1447	0.1023	-0.2427	-0.0933	0.0428	0.1628	0.0129	0.002	0.1016	0.0152	0.1461	-0.5279	20.3474	21.7557
26	5.2675	2.3166	4.8633	3.4459	2.0683	4.5804	-1.1411	1.3991	0.3921	-1.7683	0.8003	0.358	-0.9554	0.2276	0.269	0.4322	-0.0756	-0.0215	0.3542	0.0173	0.27	-2.4813	18.5852	6.9682
27	2.375	0.3017	1.0536	6.865	0.3779	1.4388	0.1053	0.0928	0.0819	-0.1603	-0.0819	0.0668	0.1246	-0.0596	-0.0157	0.1293	-0.0429	0.0009	0.1539	0.0095	0.1037	-6.2972	5.9817	10.5511
28	8.4527	-3.6257	2.3516	7.0424	-6.0884	8.4975	0.7027	0.9775	-0.9661	-0.652	-1.1314	1.1151	1.9402	1.0417	0.417	0.8418	0.3274	0.0553	0.8209	-0.132	0.7052	-4.9537	25.7798	29.7472
29	5.474	1.039	1.9315	2.9842	-1.6033	2.1417	0.2365	-0.6713	0.6564	0.8155	-0.3803	0.2945	-0.1032	-0.3073	0.1495	0.2206	-0.0071	0.0614	0.2084	-0.0199	0.1987	-4.45	20.5092	20.2078
30	4.9117	-2.567	-1.6138	7.5373	4.893	3.2111	0.2334	0.2154	-0.4732	-0.0464	-0.4504	0.7234	0.6508	-0.3743	0.251	0.2331	-0.0546	-0.0466	0.2703	-0.0084	0.2621	-13.4164	-1.1702	12.5618
31	5.0283	1.4776	-0.8274	3.5563	-3.0876	3.4684	0.0402	0.4398	-0.5023	-0.429	0.3181	-1.1283	0.1078	0.5207	0.0009	0.242	-0.0866	0.0809	0.1909	-0.0176	0.3377	21.4092	31.839	29.1625
32	8.5342	0.7735	-4.4119	2.8786	1.3328	3.3772	0.4972	-2.5219	-0.2117	0.3918	-1.5709	-1.8673	-1.2216	0.7499	1.1852	0.6341	-0.0695	-0.2461	0.8545	0.0503	0.8353	26.3917	26.4978	39.3554
33	3.8306	-1.1348	-2.8973	5.5576	0.4981	4.3916	-0.1234	-0.5795	0.3471	0.4068	-0.0962	-0.4126	-0.2951	0.034	0.0933	0.392	-0.1454	-0.1648	0.2314	0.0023	0.4014	18.1931	23.1674	53.1831
34	1.3794	0.0924	0.5849	2.2817	0.3527	2.6569	-0.0326	0.0038	0.0194	-0.1399	0.0807	0.0667	-0.0312	-0.1189	-0.0653	0.1031	-0.0298	0.0345	0.1412	0.0029	0.0878	-2.3993	9.8912	41.2526
35	4.613	4.4715	-2.8712	4.4235	-2.3927	6.5316	0.2459	-0.3224	0.3315	0.2015	-0.319	-0.0853	-0.4017	-0.0687	0.1122	0.2365	-0.0109	-0.0178	0.1288	-0.0185	0.2268	10.754	27.6729	42.8004
36	5.5253	4.8101	3.9705	4.5964	4.8554	7.4335	0.0481	0.1967	1.094	-0.0656	-0.1288	0.195	-0.6481	0.0291	0.0849	0.2357	-0.0061	0.0637	0.1544	-0.0091	0.3312	17.5021	40.2988	33.1127
37	1.0604	2.3327	-0.6888	4.5856	-1.4287	0.8459	0.0332	-0.0085	0.042	0.0694	0.0164	-0.0519	-0.0207	0.0217	-0.0469	0.1189	-0.016	-0.004	0.1299	0.0124	0.1697	9.4261	18.6589	38.0099
38	7.9757	7.1701	7.6441	6.5886	7.245	8.2857	-0.178	0.2973	0.2876	-0.1408	0.0423	0.7512	0.0311	-0.074	0.1451	0.1562	-0.0414	0.0024	0.2169	-0.0165	0.1747	5.813	21.697	37.1016
39	0.6125	-0.8156	0.7311	1.362	-0.6844	0.9405	-0.1059	-0.1748	-0.1475	-0.023	0.0767	0.0987	0.2598	-0.3693	0.0507	0.2085	-0.1059	-0.0102	0.2263	0.0257	0.1348	-4.9919	2.6419	42.4247
40	5.022	-5.425	-3.3784	6.2483	3.5699	3.1854	0.3081	-0.6362	-0.8235	0.858	-0.4774	0.9322	0.2064	-1.4686	0.3015	0.308	-0.1415	-0.0035	0.5615	0.0153	0.2878	-21.6164	1.7701	43.6205
41	6.1218	-0.0241	0.596	0.4319	-0.9198	1.6776	0.1059	-0.4222	0.0326	0.2395	-0.1585	-0.0284	-0.0925	-0.0686	0.0579	0.2456	-0.0612	0.009	0.1586	-0.0134	0.1291	4.1802	13.6589	52.1154
42	6.0187	4.7178	5.7	3.7873	4.5473	5.4356	0.0499	-0.8976	1.5533	0.395	-0.6264	1.0715	-0.3812	-0.3371	0.497	0.3498	0.0199	0.0326	0.3379	-0.0683	0.3618	-5.8187	23.5532	47.6515
43	2.5337	1.5176	1.428	2.6341	2.2579	5.7167	0.1817	-0.268	0.1645	0.2292	-0.1116	0.2113	0.0238	-0.2955	-0.0315	0.1379	0.0003	0.0346	0.1746	-0.0176	0.1451	-11.0445	13.0805	40.7366
44	3.2424	-4.4809	2.3982	8.1959	-2.0909	2.5571	0.947	-0.0385	-0.2387	0.6226	-0.8743	0.4331	-0.052	-0.4565	-0.0371	0.9408	-0.0835	0.0634	0.7295	0.004	0.3851	7.0233	8.8207	61.4123
45	3.5908	2.1652	2.8071	2.9907	1.4538	2.9288	0.3348	-0.1266	-0.051	0.4477	-0.2311	0.0403	0.076	0.0147	0.3422	0.2746	-0.092	0.0145	0.3178	0.0203	0.1813	-6.7408	10.4948	48.3629
46	4.0484	2.3035	-0.2632	6.3523	0.4802	3.1832	-0.5507	0.8462	0.384	-0.6407	0.4342	-0.2594	-0.9656	0.6906	-0.0177	0.4447	-0.3205	-0.0326	0.2088	0.0707	0.2355	29.0096	21.0322	51.6613
47	4.6022	2.1511	0.8297	3.5069	4.366	8.5886	-1.3943	0.0636	-1.5827	-0.8199	0.294	-2.5267	-0.3621	0.1676	0.9599	0.6814	-0.2681	0.1784	0.849	-0.0147	0.9495	36.5386	11.8193	47.8504
48	2.7674	-4.114	3.1139	9.0851	-5.3584	4.104	-0.0505	-0.9114	0.3092	0.5249	-0.0203	-0.814	-0.1887	0.5445	0.1843	0.2281	-0.0686	-0.0684	0.5544	-0.0857	0.4033	36.8487	-3.2255	54.6027
49	1.6955	-0.9149	-0.1409	0.6569	-0.3496	0.921	-0.0534	-0.0796	0.0463	-0.0491	-0.031	0.0903	0.0607	-0.1137	0.0873	0.1851	-0.058	-0.0085	0.116	0.0312	0.0789	8.6088	-8.1793	50.5931
50	4.7298	6.2775	3.0538	8.7674	3.02	8.139	0.2	-0.5291	-0.2413	0.3998	-0.2794	-0.3679	0.0518	0.0794	0.0132	0.2046	-0.0037	-0.0363	0.1691	-0.0048	0.1788	25.5797	4.0714	57.8002
51	2.0192	-0.7726	1.2444	6.7689	-3.2031	1.9165	-0.2152	-0.4249	0.6109	1.0134	-0.0651	-0.0093	-0.4502	0.347	0.1819	0.3684	-0.155	-0.0237	0.2748	-0.025	0.2295	30.5653	21.0635	61.6785
52	0.4485	0.5349	0.3978	1.3918	0.4264	0.5163	-0.0018	0.027	0.0742	-0.031	0.019	-0.0267	-0.0818	0.0967	-0.022	0.2303	-0.0846	0.0198	0.2164	0.0053	0.1611	20.1376	3.2623	50.4401
53	6.4082	4.5635	6.3094	6.2474	1.8596	9.0756	-0.0286	-0.5041	0.6213	0.1497	-0.1533	0.1467	-0.1513	-0.0646	0.21	0.1619	-0.0659	-0.0057	0.1923	-0.0124	0.1294	17.8176	4.4394	54.4711
54	0.4769	-1.1513	-0.2476	4.7715	-0.6509	1.067	0.0297	-0.0621	-0.1344	0.3537	-0.0098	0.1977	0.3557	-0.3081	-0.0382	0.2244	-0.0846	-0.013	0.1974	-0.0172	0.1495	6.2126	-13.3926	47.0911
55	1.8385	-1.6264	-1.2626	2.3398	1.0721	0.8818	-0.3546	-0.107	-0.7504	0.6319	0.0762	0.5637	1.9643	-2.1738	0.1689	0.447	-0.1844	0.059	0.4503	-0.0221	0.3432	-6.5506	-20.2699	55.7502
56	5.5311	2.633	-3.5623	2.7308	-0.7449	2.8408	-0.0872	-0.0917	-0.1574	0.0337	0.1253	-0.1639	0.1571	0.1447	-0.0441	0.1794	-0.0101	-0.0398	0.1242	0.0069	0.1107	22.1648	-12.0597	53.7888
57	5.9094	-6.0386	-6.7459	7.0522	6.398	8.1307	0.1113	-1.1722	-0.102	0.3685	-0.0414	0.0778	0.3661	0.2018	-0.0749	0.248	-0.0023	-0.0267	0.2853	0.0474	0.1385	14.9343	-6.4908	65.4457
58	6.5161	-1.2652	0.9569	0.9821	-0.6122	1.1861	0.035	-0.0118	-0.3535	0.0719	0.0718	0.1774	0.0583	-0.1212	-0.1166	0.1805	-0.0681	-0.0031	0.1352	0.0077	0.1078	3.9063	-8.3418	57.9589
59	4.6333	-5.2655	-4.7485	6.0212	5.4224	4.8933	0.2486	0.2639	0.122	-0.1143	0.1657	-0.1854	0.1199	-0.1286	-0.4276	0.4444	0.062	0.0177	0.3839	0.0336	0.4715	28.6215	-20.5028	51.8812
60	8.4304	-0.888	-0.3413	1.1365	-0.5696	2.5054	0.1158	-0.0003	-0.4014	0.0146	0.0463	0.2179	0.1912	-0.1281	-0.1303	0.2016	-0.0585	0.0031	0.1033	0.0022	0.1431	8.8682	-13.9943	56.1749
61	3.1985	1.1347	3.484	7.6433	-0.2085	6.8846	-0.003	-0.07	1.2759	0.4023	-0.1786	-0.1097	-0.303	0.0652	0.2415	0.2463	-0.1048	-0.0618	0.2348	0.0011	0.3777	43.5891	0.0796	46.0333
62	5.4164	5.6836	5.6805	5.9893	5.9906	6.011	-1.6748	0.9728	0.0647	-0.9096	1.6521	0.0847	-0.5754	2.8248	0.0024	0.6238	-0.2058	0.0231	1.0113	0.0955	0.5876	44.5425	0.4568	33.6654
63	6.3519	-6.3072	-6.1713	6.3987	6.004	6.2262	-0.1766	-0.151	-0.1946	-0.2071	0.2459	-0.8186	0.0048	1.3201	-0.2065	0.2253	-0.0178	0.0125	0.5456	0.0347	0.3382	43.3927	-12.698	23.7859
64	2.6916	0.071	-0.3847	1.0154	-0.3827	1.5426	0.0788	-0.0949	-0.0613	0.0537	-0.0471	0.006	0.1106	-0.0547	-0.0401	0.2037	-0.0291	-0.0132	0.093	-0.0123	0.1321	18.095	-21.2225	34.0625
65	4.0012	5.7772	1.0205	8.5212	1.6103	2.1489	-0.0472	0.3004	-0.4554	-0.048	0.1605	-0.3669	0.23	0.3694	0.0194	0.2216	0.0011	-0.0544	0.2244	0.0044	0.2069	40.1137	-14.6215	36.7234
66	8.4015	1.4992	-5.8937	4.5462	2.7966	10.001	0.1325	-0.9993	-0.5386	0.5936	-0.2049	-1.0848	0.6157	0.5529	0.1334	0.3169	-0.0539	-0.1713	0.2208	0.0587	0.3649	50.2897	-7.1226	48.4642
67	3.7888	1.4184	1.6097	0.5507	1.0308	1.437	0.0803	-0.0394	0.0053	0.042	-0.0312	-0.102	-0.0098	0.0104	-0.0443	0.2165	-0.0434	-0.0224	0.1573	0.0331	0.1754	30.2869	-11.3504	36.584
68	4.9512	-0.2341	1.2337	3.3473	1.6939	1.2839	0.0437	-0.2372	-0.2302	0.1855	-0.0314	0.0054	0.3512	0.1712	0.0143	0.124	-0.0597	-0.0089	0.1785	0.0606	0.1586	31.021	-14.5867	40.0735
69	0.4473	-0.7596	-0.3663	1.868	-0.8248	3.6414	0.0279	0.0911	-0.117	-0.0416	0.0797	0.4278	0.4152	-0.3939	-0.1009	0.1803	-0.0669	-0.0052	0.2271	0.0048	0.1781	10.5812	-24.4089	30.8873
70	7.7684	1.9444	-2.9982	0.4982	-0.7292	1.1742	-0.2898	-0.1061	-0.5626	-0.2771	-0.0639	-0.1647	0.9546	-0.6505	0.306	0.4015	-0.1484	0.0196	0.263	0.0119	0.4473	9.5308	-35.9634	32.648
71	5.7122	3.1966	-2.3237	6.2095	-4.4049	5.6285	0.0024	-0.0073	-0.3967	0.0752	-0.1892	-0.2966	0.159	0.3001	0.2085	0.1817	0.0221	-0.0136	0.1624	-0.0661	0.1442	31.3865	-22.6466	27.2648
72	6.8602	-1.1156	-3.6954	3.021	1.1147	3.6869	-0.1895	-0.3135	-0.4618	0.3913	0.123	0.0271	0.2895	0.1499	0.0695	0.2479	-0.0347	-0.0264	0.1527	0.0257	0.1931	17.5181	-28.6909	39.3832
73	5.9239	-6.2698	4.4469	9.3022	-6.2522	4.2102	-2.0867	-0.4946	0.419	1.4286	-0.1811	0.4011	0.1294	-2.9581	1.9694	1.3961	-0.1536	-0.0006	1.2464	-0.2959	0.6106	28.2712	-23.9377	15.6417
74	1.9821	0.5486	0.3507	2.0702	-0.8506	0.5606	-0.2481	2.1465	0.1362	-2.0983	0.6323	1.3056	1.0338	-1.4885	-0.4006	0.9322	-0.3217	-0.222	1.2411	-0.0103	0.6767	33.3486	-21.6944	14.7417
75	4.5149	3.3724	-5.3501	4.0929	-3.5411	7.6431	-0.1606	0.3356	-0.0577	0.0952	0.2196	0.1364	0.4484	-0.2561	-0.0203	0.2389	-0.0345	-0.0206	0.169	-0.0227	0.2235	16.5503	-29.958	33.4142
76	2.9296	3.0138	3.3772	3.5441	3.5143	3.8991	-0.0674	0.1224	0.4777	-0.2627	-0.0262	1.1161	-0.249	-0.0473	0.1318	0.2194	-0.038	-0.0252	0.227	-0.0415	0.4041	-47.0328	-62.7885	17.2466
77	3.1695	5.5083	3.8469	9.7416	6.8815	4.9032	0.9456	-1.912	-0.3701	-0.0041	-1.2138	-0.2329	1.0148	-0.8126	0.2274	0.5516	-0.1072	0.1087	0.71	0.0564	0.5767	-47.841	-63.2331	29.7672
78	4.3774	-4.8393	4.2303	5.3674	-4.6859	4.1806	-0.2765	0.208	-1.0756	-0.2806	0.1332	0.3648	1.0462	-0.505	0.0374	0.5229	-0.1297	0.1049	0.3399	-0.0041	0.4519	-35.2575	-66.6936	39.7876
79	1.8282	-0.2893	-0.536	0.6333	-0.939	2.4607	0.0033	0.0899	0.0226	-0.19	0.0317	-0.1678	-0.0644	0.167	-0.0249	0.0986	-0.0165	-0.0244	0.118	0.0013	0.1698	-17.9959	-46.0011	29.3487
80	9.1228	6.1897	-0.9175	4.2897	-0.8948	3.4393	0.0047	-0.1122	-0.3689	-0.1502	-0.1927	-0.0245	0.3869	-0.1213	0.2193	0.2508	-0.0489	0.0011	0.154	-0.0328	0.2762	-31.3921	-63.4814	26.907
81	8.4475	2.3675	-0.0065	9.2248	-6.2132	4.5239	-0.3083	0.6826	-1.0549	-0.6859	0.1475	-0.3617	0.8765	0.1137	0.153	0.2206	-0.0203	-0.0057	0.1993	-0.104	0.3589	-42.7281	-71.667	15.1685
82	1.6893	2.7481	2.1297	3.5188	2.1803	2.0426	-0.0284	0.1201	-0.1664	-0.0115	0.1368	-0.0345	0.0544	0.0645	-0.0841	0.1271	-0.0291	0.0225	0.1716	-0.0315	0.2304	-31.7388	-54.2692	26.703
83	9.6163	4.0682	-2.5435	5.4538	-3.1859	4.7727	-0.0942	0.5899	-0.4563	-0.0137	0.131	-0.0962	0.0084	0.0159	-0.0451	0.1431	-0.0452	-0.0054	0.1775	-0.0361	0.2379	-28.9183	-56.1852	23.3548
84	0.6423	-0.7562	-0.3868	1.4983	0.3691	5.6804	-0.021	-0.2287	0.1868	0.0475	0.0275	-0.3013	-0.036	0.3432	-0.0209	0.2042	-0.0597	-0.0374	0.1328	-0.0114	0.2611	-14.5576	-40.867	32.9092
85	4.6521	5.4684	-5.2964	6.4688	-6.2739	6.1168	0.3359	-0.4586	-0.2781	0.3547	-0.5499	-1.5534	-0.0468	1.393	0.2599	0.2964	-0.0882	-0.0069	0.6388	-0.0043	0.4826	1.18	-40.3402	29.2673
86	8.9194	0.064	-1.4023	0.1736	0.512	1.7827	0.0087	-0.1309	0.1422	0.0496	-0.0005	0.1946	0.1596	0.0911	0.0054	0.2419	-0.0253	-0.042	0.1191	0.0223	0.2007	-22.5997	-56.7634	39.2355
87	4.7937	2.9201	-3.5091	9.0525	-7.3144	8.6386	-0.0823	0.2036	-0.4158	-0.462	-0.092	-0.4568	0.5163	0.1574	0.1512	0.1598	0.0025	0.0001	0.2065	-0.072	0.2359	-13.0996	-51.2266	21.9415
88	5.0017	3.2525	-1.4194	7.2944	-2.3613	3.5304	0.0073	0.0302	-0.6407	0.0203	-0.1434	-0.8383	0.0918	0.5222	0.1557	0.1474	0.0168	-0.0421	0.2241	-0.0417	0.2757	-10.1239	-52.2666	30.0348
89	2.4547	-3.5217	2.6464	7.4718	-0.8239	6.5822	-0.4585	-0.1473	1.4118	0.2604	-0.6234	-0.2991	-1.0852	-0.8783	1.0314	0.9775	0.1607	-0.3647	0.8051	-0.1112	0.7272	-21.4109	-57.1577	49.658
90	4.8638	3.2642	-2.3736	4.6669	-2.9592	6.7509	0.2601	-0.3119	-0.1174	0.197	-0.2824	-0.2308	-0.0678	0.5662	0.0129	0.145	0.0039	-0.0304	0.1626	-0.0214	0.3002	-11.2158	-49.2353	31.6582
91	6.4744	4.3701	-0.7994	7.5202	2.084	6.0698	-0.1196	0.6723	-0.1527	-0.3885	0.3482	0.7871	0.6534	-0.8683	-0.1379	0.2963	-0.141	-0.0928	0.2444	0.0625	0.2809	-45.891	-64.3892	43.3144
92	4.8312	4.6475	-0.0384	4.7035	1.3659	9.197	-0.6765	-1.7035	1.3609	-0.2083	-0.6195	2.2536	0.9848	0.4339	1.1431	0.5072	-0.0712	0.0291	0.8548	0.0829	0.8963	-53.4483	-55.1915	46.8848
93	3.3559	4.6252	0.6724	6.4665	0.7937	1.8539	0.1757	-0.8441	-0.4201	0.6502	-0.4457	0.5634	0.4698	-0.5049	0.2599	0.3379	-0.0347	0.1421	0.4706	0.1663	0.5038	-50.329	-45.042	59.4098
94	1.4631	-0.8036	-0.3891	0.531	0.4495	1.0718	0.0244	-0.1684	-0.1547	0.0473	-0.0193	-0.1904	0.0627	0.0626	-0.0185	0.1729	-0.0623	-0.0418	0.1652	0.0044	0.1348	-24.818	-36.8166	49.4081
95	4.8053	6.6859	-2.8508	9.65	-2.4802	8.2722	0.393	-0.7361	-0.1122	0.6345	-0.3202	0.4487	0.3897	0.0256	-0.0865	0.2776	-0.0478	0.0024	0.2288	0.0587	0.2649	-40.2212	-52.9885	55.4643
96	9.1346	-0.0201	-4.2789	7.6377	0.9372	2.1478	0.0047	-0.491	-0.578	0.6214	0.0326	-0.4522	0.2864	0.1379	-0.0381	0.3388	-0.0839	-0.1603	0.2695	0.1155	0.3163	-42.6777	-68.4027	51.3451
97	1.4556	2.7122	-0.456	6.9519	-0.6981	0.7772	0.0518	-0.113	-0.0779	-0.0297	-0.0696	0.0432	0.1024	-0.0508	0.014	0.1525	-0.0448	-0.0511	0.163	0.0254	0.1988	-36.367	-45.9843	47.3918
98	5.4664	5.3614	-5.2612	6.7953	-3.2057	7.5249	0.0398	-0.0758	-0.3649	0.0885	0.1088	-0.2952	0.1838	0.2494	-0.1734	0.1724	-0.0502	-0.022	0.1743	0.0352	0.2897	-33.0594	-50.2108	49.5871
99	1.9139	-2.3288	-0.2361	3.0272	0.6128	1.5757	0.0015	-0.2156	0.1962	0.1201	-0.1061	-0.1137	-0.2433	0.2445	0.1409	0.1753	-0.0875	0.0095	0.2047	0.0094	0.1442	-23.0174	-30.0897	48.0721
100	5.579	-3.9395	1.0213	3.4715	-0.7505	6.8989	-0.0077	-0.5761	0.4598	1.0225	-0.0931	-1.3659	-1.0577	1.6291	-0.0767	0.3539	-0.1741	-0.1524	0.3838	-0.0794	0.6277	-7.447	-27.21	54.5543
101	5.9111	-0.5027	3.1614	0.785	0.4511	2.374	0.0736	0.0993	0.0312	0.1914	0.038	0.0687	-0.0084	0.02	-0.1033	0.2392	-0.0801	0.0081	0.1802	-0.0082	0.1667	-33.3675	-33.7188	56.1683
102	2.2453	-2.2461	-2.4309	3.9926	1.1786	5.3987	-0.3787	-1.0034	-0.3251	0.5849	0.324	0.438	0.1818	-0.2819	-0.0185	0.3802	-0.0757	0.0721	0.3429	0.0122	0.2073	-40.6203	-41.5252	63.0601
103	8.6353	0.5249	-3.499	1.3709	-0.1103	5.4537	0.1364	-0.7681	-0.0965	0.3612	-0.147	-0.1101	0.1886	0.2478	0.0267	0.2393	-0.0619	-0.0673	0.2221	0.0293	0.1839	-18.9377	-40.4805	55.5658
104	7.7574	-3.3935	4.01	4.3249	-4.4285	4.6085	0.2408	0.681	-0.4105	0.3487	0.3922	-0.5596	2.3226	1.2784	-0.6095	0.9063	0.1009	-0.0372	0.6779	-0.2104	0.5967	-41.9934	-27.8455	62.449
105	8.4093	1.8508	-4.2502	2.8046	-0.7679	4.8333	0.3506	-0.4146	0.3075	0.2733	-0.2654	-0.0671	-0.1502	0.2047	-0.0614	0.2277	-0.0619	-0.051	0.187	-0.0021	0.1424	-22.5129	-34.0359	56.7925
106	6.169	3.0571	-0.6411	6.5322	-1.6768	6.266	-0.2764	0.4548	-1.0244	-0.4092	0.0265	-0.357	0.7534	-0.1258	0.209	0.3321	-0.1926	0.0748	0.2845	-0.0414	0.3809	-59.7178	-44.5956	52.9413
107	7.5963	4.9079	-3.3887	4.8137	-0.2719	3.7412	-1.5672	-0.1631	0.4253	-1.4697	1.8849	1.8623	1.6557	-0.9525	-0.4643	0.6535	-0.2279	0.0145	0.9493	0.0846	0.6908	-64.6649	-39.2735	42.822
108	6.5319	-2.7358	-1.0423	2.1479	1.6078	9.2512	-0.3694	-1.0665	0.2851	-0.0811	0.5585	0.8447	0.0836	-0.668	-0.1319	0.2272	-0.1336	-0.0132	0.592	0.0314	0.3156	-65.3762	-22.9659	40.1464
109	5.1832	-2.6482	5.4709	4.4377	-2.1848	7.0346	0.3069	-1.0722	-0.0865	0.0031	-0.2466	0.3104	0.3341	-1.4643	-0.0899	0.17	-0.0531	0.0265	0.3983	-0.0211	0.1981	-60.5076	-19.7176	46.8315
110	1.9821	-0.5248	0.3657	1.3197	-0.6731	3.5976	-0.0878	-0.0808	-0.0795	-0.0793	-0.0178	-0.0287	0.1031	0.171	0.107	0.1553	-0.0502	0.0121	0.1062	-0.032	0.1212	-33.9901	-17.9436	44.1898
111	8.4996	5.7581	-2.8221	7.6771	-1.976	7.534	-0.1217	-0.2961	0.1686	0.1124	0.0754	0.4411	0.0198	-0.4383	0.0562	0.1701	-0.0155	0.0282	0.2477	-0.01	0.1555	-58.2828	-27.0467	50.8581
112	7.3578	-1.4488	2.3893	9.316	-4.506	6.8399	-0.1019	-0.5893	-0.5359	1.0892	-0.0811	0.4254	-0.1325	-0.4493	0.1677	0.3732	-0.1244	0.0817	0.291	-0.0245	0.2224	-64.6268	-39.8133	60.3622
113	1.257	0.4778	-0.4386	0.9171	-0.3561	1.3094	0.0145	-0.0211	0.0104	0.0364	-0.0218	0.0369	0.0699	-0.0318	0.0049	0.1786	-0.0784	0.0084	0.1855	-0.0254	0.1335	-45.9311	-25.9721	45.3137
114	4.25	3.2956	3.7007	3.4361	2.5315	3.3511	-0.2497	-0.4876	1.4462	-0.3525	0.0482	-0.8125	-1.323	0.833	-0.0589	0.3974	-0.1555	-0.058	0.2358	-0.0154	0.4342	-24.1038	-3.5087	48.3702
115	6.3598	4.0958	3.7655	3.4669	2.4025	3.8698	-0.0963	0.259	0.166	0.003	0.1039	0.1208	-0.1375	-0.2159	-0.0088	0.1413	-0	0.0049	0.1647	0.0226	0.1079	-50.864	-14.3184	40.4391
116	7.2296	-2.1265	1.2371	1.9001	-0.3142	2.9544	0.007	-0.3186	-0.0297	0.1542	0.1137	-0.0197	-0.0548	-0.1282	-0.1232	0.1962	-0.0488	-0.0111	0.1262	-0.0187	0.1331	-36.4481	-15.9696	54.1785
117	3.4533	0.6034	4.1851	2.9522	0.985	5.3083	-0.2234	-0.1037	0.6709	-0.0198	-0.0187	0.1215	-0.1527	-0.1821	0.2802	0.1744	-0.0287	0.0211	0.1117	0.0347	0.1559	-41.7717	-9.157	50.0333
118	5.2766	6.5086	5.7365	9.9994	7.5079	6.4129	0.2733	1.1999	-0.4897	1.5679	1.9269	-0.8129	0.5279	2.6097	-2.1747	0.7863	0.2238	0.1119	0.8726	-0.0745	0.7079	-53.7298	-8.5932	32.3205
119	0.1541	-0.5537	0.3283	4.7286	0.4404	2.427	-0.2338	1.3257	0.0753	-0.4274	0.4208	0.3942	-0.1662	-0.4705	-0.1052	0.2153	-0.0653	-0.0349	0.5126	0.0925	0.164	-50.5432	-10.315	41.045
120	8.4897	2.0032	4.4045	7.5233	0.992	4.1048	-0.1395	0.1354	0.1216	0.5511	0.0258	-0.5376	0.2279	0.8701	-0.0264	0.2567	-0.0962	-0.0119	0.3125	0.018	0.1581	-26.1155	-9.6048	50.1564
121	3.196	-1.4407	-3.5748	8.1288	-2.207	6.1441	0.2539	-0.8091	-0.9408	0.0627	-0.4126	0.1172	0.5287	-0.2353	0.176	0.1925	-0.1096	-0.0051	0.3183	0.0517	0.4093	-69.3364	-31.8924	31.9021
122	6.0603	3.1645	-3.8965	4.6684	-4.1367	4.3777	0.0555	-0.4508	0.0972	0.525	-0.1789	0.8106	0.4134	-1.1218	0.2401	0.373	-0.1568	-0.0142	0.4366	-0.1463	0.3758	-60.7669	-33.7065	15.1896
123	7.5878	-3.0408	-2.114	6.1125	5.7856	5.6028	0.4383	0.785	-1.1935	-0.2346	-1.1333	1.32	0.5326	-1.2417	0.6449	0.3696	-0.0517	-0.1143	0.5158	-0.0732	0.345	-60.5964	-27.8557	6.1695
124	0.3035	0.2679	0.6682	0.8468	0.498	1.1629	0.0182	-0.1499	0.1468	0.0305	-0.0271	-0.0143	-0.0331	-0.047	-0.0058	0.2026	-0.0448	0.0082	0.2034	0.0223	0.1422	-37.8694	-15.4615	22.5226
125	4.1797	4.3583	-2.7308	4.6168	-3.3318	6.0679	-0.1675	0.4523	0.2256	-0.2059	0.171	0.4163	-0.0128	-0.3514	-0.0021	0.1407	0.0053	-0.0012	0.2206	-0.0406	0.2264	-61.3607	-22.5212	19.4216
126	9.0879	4.593	2.3459	3.076	-1.1968	9.3965	0.1689	0.0733	0.8712	0.1002	0.0577	0.8155	-0.2967	-0.9135	-0.2367	0.1889	0.0228	0.0419	0.2361	0.0243	0.3476	-75.6705	-24.0332	28.9372
127	6.5942	0.8115	-1.9098	-0.1786	-0.1429	0.7785	0.1203	-0.1459	0.0853	0.0222	-0.0349	0.0507	0.0247	-0.0444	-0.0821	0.1871	-0.0469	0.0151	0.1316	-0.0023	0.1861	-52.4636	-24.4207	24.3569
128	4.6261	3.4468	5.6607	5.2274	3.6886	7.0465	0.1424	-0.2256	0.0322	0.0656	-0.0179	0.0042	-0.1513	-0.2339	-0.1173	0.1506	-0.0559	0.0248	0.1701	0.0024	0.1749	-54.0441	-20.0203	25.1825
129	0.3393	-0.8572	-0.2286	2.0344	0.5031	1.748	0.2063	0.153	0.3448	-0.1152	-0.0458	-0.1956	-0.3925	0.1615	-0.087	0.1739	-0.065	0.0285	0.2043	0.0079	0.1565	-32.3696	-16.6094	20.1816
130	5.4197	-3.2543	3.2541	3.0814	-0.7754	3.2164	-0.3422	1.0759	1.0686	-0.6339	-0.1969	-1.6095	-1.2044	1.0317	0.5275	0.4222	-0.1422	0.0668	0.3601	0.0081	0.3772	-25.6856	-0.9657	18.7382
131	0.7429	0.4444	-0.8807	4.5008	-0.1119	1.1278	-0.0268	0.2536	-0.0927	-0.219	-0.0246	0.1003	-0.0548	-0.1911	0.0584	0.1718	-0.027	-0.0264	0.2316	0.0021	0.1108	-45.754	-21.4912	10.3109
132	4.2215	5.1073	4.9036	6.2172	5.9405	5.7045	-0.1532	0.7063	0.9945	-0.2447	-0.0891	1.2186	-0.6991	-0.3281	0.1824	0.3414	0.0388	0.0001	0.3568	0.0244	0.4164	-51.624	-8.6175	14.5522
133	4.5598	1.1193	2.9284	1.5909	-0.494	5.1374	-0.0435	0.085	0.2034	0.0016	0.0777	0.0378	-0.2457	0.0193	-0.0352	0.1606	-0.0162	0.0221	0.0829	0.0111	0.1494	-39.8896	-6.8778	22.3542
134	8.1878	-4.7421	0.4681	4.0071	1.6618	6.4817	-0.3916	0.2187	-0.3499	1.1645	0.9731	-0.5184	-1.3634	0.9218	-0.4645	0.7531	-0.0571	0.0838	0.7936	0.0582	0.482	-42.4618	-25.0799	1.3396
135	8.8654	6.9441	4.6011	9.0392	5.4089	5.4286	-0.0478	0.4273	-0.2892	-0.3077	0.298	-0.3053	-0.2549	-0.0965	-0.2593	0.2067	-0.0613	0.0227	0.2798	0.0431	0.1783	-39.0673	-12.2856	14.0703
136	2.0532	-0.9411	3.5006	6.36	-3.2639	6.742	0.3112	-1.0896	-0.0867	0.3179	-0.1548	0.303	0.2031	-0.8108	-0.14	0.2001	-0.1433	0.0061	0.345	-0.0073	0.2351	-61.4867	-41.9261	10.9999
137	2.6905	-3.452	3.6085	4.4276	-4.4486	5.9367	-0.5976	0.1966	-2.5347	-0.4891	-0.2952	0.1249	-1.1801	-0.4937	0.7971	0.6151	-0.1451	-0.0531	0.8137	-0.0244	0.8916	-55.5292	-52.1808	15.1278
138	5.2607	-5.0221	-4.2734	4.8563	4.1254	4.3348	-0.2677	1.0819	-1.0547	-0.3614	-0.3111	0.3585	0.4142	-1.0373	0.5849	0.467	-0.1735	-0.0804	0.3024	-0.0811	0.4483	-41.2604	-57.9796	8.4094
139	0.5199	-0.1825	-0.4575	2.0185	-0.6821	0.8069	-0.0849	0.092	-0.0084	-0.0831	0.0545	-0.0034	-0.0722	0.0517	0.0548	0.1322	-0.0459	0.046	0.1416	-0.0224	0.1219	-26.8223	-33.2633	12.2492
140	2.6458	2.7614	4.3402	3.1528	4.8383	7.4136	-0.2142	0.6956	-0.3411	-0.4878	0.1325	-0.1594	-0.2843	-0.0028	0.0004	0.2334	-0.0441	-0.0344	0.2488	-0.0087	0.2725	-40.8032	-42.4988	5.3501
141	4.6644	-5.1343	2.1181	6.4221	-1.3816	6.7565	0.4372	0.4221	-0.4817	-0.252	-0.2632	0.2071	0.2905	-0.5216	-0.1761	0.2192	-0.1031	-0.0236	0.2847	-0.0025	0.192	-58.4668	-46.3748	2.4446
142	8.4794	-4.8637	3.8666	3.9998	-3.4582	3.0325	0.0845	0.7058	0.3617	-0.6047	-0.1017	0.2805	-0.0619	0.5888	0.0287	0.2385	-0.1121	-0.0198	0.2891	0.0297	0.171	-57.2418	-38.5939	2.7993
143	2.3088	0.2829	1.574	0.4198	0.415	1.0875	0.0494	-0.1168	-0.1887	0.0011	0.0023	0.0076	0.1213	-0.185	-0.0555	0.1912	-0.0844	0.0021	0.2207	0.0206	0.1837	-39.8496	-40.2109	13.4377
144	5.4653	5.531	5.4863	5.5969	5.4923	6.9337	-0.1613	0.3865	0.2343	-0.1442	0.2218	0.5499	-0.23	-0.0752	-0.0297	0.1917	-0.0703	0.0031	0.2297	-0.0075	0.1915	-41.8323	-37.5199	8.3175
145	1.8789	1.2175	0.3588	3.694	-0.0829	0.5742	-0.0421	0.1431	-0.1857	-0.2238	-0.0113	-0.3631	0.0168	0.1408	0.0627	0.1622	-0.0365	0.0178	0.1836	-0.0192	0.1637	-22.938	-38.9602	11.0685
146	4.4087	5.344	-4.801	6.4741	-5.826	5.2513	-0.5415	1.4028	-0.365	-1.0479	0.9989	0.1074	0.5522	-0.3621	-0.374	0.4086	-0.0583	-0.008	0.3992	-0.044	0.2694	-30.4896	-39.0007	-2.6008
147	2.2531	1.6862	-0.372	8.8666	2.9556	3.1955	-0.0148	0.1633	-0.111	-0.1162	0.08	-0.2243	-0.1279	0.0166	-0.0757	0.1522	-0.037	0.0132	0.1747	0.008	0.0758	-24.8301	-29.0782	4.837
148	9.4819	-5.8269	0.482	4.0216	-1.3036	2.4063	0.407	0.2393	0.2398	0.3859	0.5787	-0.5318	-1.4187	-0.2689	-0.9145	0.7505	0.1368	-0.0369	0.6134	-0.2034	0.8836	-21.5259	-55.6546	11.9187
149	5.7727	3.2109	-1.9026	1.7878	-1.0154	4.4043	0.3207	-0.4851	-0.9087	0.252	-0.6242	-0.7236	0.4135	0.1567	0.2676	0.2108	-0.0116	-0.0487	0.2053	-0.0257	0.327	-24.682	-46.4791	6.6622
150	5.9098	2.3684	3.867	7.9958	-3.4086	9.7355	-0.0345	-0.3025	0.4435	0.6101	-0.181	-0.2246	-0.5137	-0.0699	0.1895	0.1878	-0.0541	0.0539	0.2453	-0.0325	0.2157	-16.7951	-22.8528	7.3545

Refinement TLS group

ID	Refine-ID	Refine TLS-ID	Selection details
1	X-RAY DIFFRACTION	1	(CHAIN A AND RESID 1:12)
2	X-RAY DIFFRACTION	2	(CHAIN A AND RESID 13:17)
3	X-RAY DIFFRACTION	3	(CHAIN A AND RESID 18:25)
4	X-RAY DIFFRACTION	4	(CHAIN A AND RESID 26:52)
5	X-RAY DIFFRACTION	5	(CHAIN A AND RESID 53:59)
6	X-RAY DIFFRACTION	6	(CHAIN A AND RESID 60:76)
7	X-RAY DIFFRACTION	7	(CHAIN A AND RESID 77:112)
8	X-RAY DIFFRACTION	8	(CHAIN A AND RESID 113:117)
9	X-RAY DIFFRACTION	9	(CHAIN A AND RESID 118:132)
10	X-RAY DIFFRACTION	10	(CHAIN A AND RESID 133:139)
11	X-RAY DIFFRACTION	11	(CHAIN A AND RESID 140:155)
12	X-RAY DIFFRACTION	12	(CHAIN A AND RESID 156:180)
13	X-RAY DIFFRACTION	13	(CHAIN A AND RESID 181:185)
14	X-RAY DIFFRACTION	14	(CHAIN A AND RESID 186:194)
15	X-RAY DIFFRACTION	15	(CHAIN A AND RESID 195:205)
16	X-RAY DIFFRACTION	16	(CHAIN B AND RESID 1:12)
17	X-RAY DIFFRACTION	17	(CHAIN B AND RESID 13:17)
18	X-RAY DIFFRACTION	18	(CHAIN B AND RESID 18:25)
19	X-RAY DIFFRACTION	19	(CHAIN B AND RESID 26:60)
20	X-RAY DIFFRACTION	20	(CHAIN B AND RESID 61:77)
21	X-RAY DIFFRACTION	21	(CHAIN B AND RESID 78:112)
22	X-RAY DIFFRACTION	22	(CHAIN B AND RESID 113:117)
23	X-RAY DIFFRACTION	23	(CHAIN B AND RESID 118:129)
24	X-RAY DIFFRACTION	24	(CHAIN B AND RESID 130:135)
25	X-RAY DIFFRACTION	25	(CHAIN B AND RESID 136:154)
26	X-RAY DIFFRACTION	26	(CHAIN B AND RESID 155:160)
27	X-RAY DIFFRACTION	27	(CHAIN B AND RESID 161:183)
28	X-RAY DIFFRACTION	28	(CHAIN B AND RESID 184:190)
29	X-RAY DIFFRACTION	29	(CHAIN B AND RESID 191:200)
30	X-RAY DIFFRACTION	30	(CHAIN B AND RESID 201:205)
31	X-RAY DIFFRACTION	31	(CHAIN C AND RESID 1:12)
32	X-RAY DIFFRACTION	32	(CHAIN C AND RESID 13:17)
33	X-RAY DIFFRACTION	33	(CHAIN C AND RESID 18:24)
34	X-RAY DIFFRACTION	34	(CHAIN C AND RESID 25:54)
35	X-RAY DIFFRACTION	35	(CHAIN C AND RESID 55:64)
36	X-RAY DIFFRACTION	36	(CHAIN C AND RESID 65:72)
37	X-RAY DIFFRACTION	37	(CHAIN C AND RESID 73:112)
38	X-RAY DIFFRACTION	38	(CHAIN C AND RESID 113:117)
39	X-RAY DIFFRACTION	39	(CHAIN C AND RESID 118:129)
40	X-RAY DIFFRACTION	40	(CHAIN C AND RESID 130:135)
41	X-RAY DIFFRACTION	41	(CHAIN C AND RESID 136:154)
42	X-RAY DIFFRACTION	42	(CHAIN C AND RESID 155:160)
43	X-RAY DIFFRACTION	43	(CHAIN C AND RESID 161:183)
44	X-RAY DIFFRACTION	44	(CHAIN C AND RESID 184:190)
45	X-RAY DIFFRACTION	45	(CHAIN C AND RESID 191:205)
46	X-RAY DIFFRACTION	46	(CHAIN D AND RESID 1:12)
47	X-RAY DIFFRACTION	47	(CHAIN D AND RESID 13:17)
48	X-RAY DIFFRACTION	48	(CHAIN D AND RESID 18:25)
49	X-RAY DIFFRACTION	49	(CHAIN D AND RESID 26:53)
50	X-RAY DIFFRACTION	50	(CHAIN D AND RESID 54:64)
51	X-RAY DIFFRACTION	51	(CHAIN D AND RESID 65:72)
52	X-RAY DIFFRACTION	52	(CHAIN D AND RESID 73:112)
53	X-RAY DIFFRACTION	53	(CHAIN D AND RESID 113:117)
54	X-RAY DIFFRACTION	54	(CHAIN D AND RESID 118:129)
55	X-RAY DIFFRACTION	55	(CHAIN D AND RESID 130:135)
56	X-RAY DIFFRACTION	56	(CHAIN D AND RESID 136:154)
57	X-RAY DIFFRACTION	57	(CHAIN D AND RESID 155:160)
58	X-RAY DIFFRACTION	58	(CHAIN D AND RESID 161:183)
59	X-RAY DIFFRACTION	59	(CHAIN D AND RESID 184:191)
60	X-RAY DIFFRACTION	60	(CHAIN D AND RESID 192:205)
61	X-RAY DIFFRACTION	61	(CHAIN E AND RESID 1:12)
62	X-RAY DIFFRACTION	62	(CHAIN E AND RESID 13:17)
63	X-RAY DIFFRACTION	63	(CHAIN E AND RESID 18:25)
64	X-RAY DIFFRACTION	64	(CHAIN E AND RESID 26:54)
65	X-RAY DIFFRACTION	65	(CHAIN E AND RESID 55:64)
66	X-RAY DIFFRACTION	66	(CHAIN E AND RESID 65:72)
67	X-RAY DIFFRACTION	67	(CHAIN E AND RESID 73:112)
68	X-RAY DIFFRACTION	68	(CHAIN E AND RESID 113:117)
69	X-RAY DIFFRACTION	69	(CHAIN E AND RESID 118:132)
70	X-RAY DIFFRACTION	70	(CHAIN E AND RESID 133:138)
71	X-RAY DIFFRACTION	71	(CHAIN E AND RESID 139:160)
72	X-RAY DIFFRACTION	72	(CHAIN E AND RESID 161:182)
73	X-RAY DIFFRACTION	73	(CHAIN E AND RESID 183:188)
74	X-RAY DIFFRACTION	74	(CHAIN E AND RESID 189:193)
75	X-RAY DIFFRACTION	75	(CHAIN E AND RESID 194:205)
76	X-RAY DIFFRACTION	76	(CHAIN F AND RESID 1:12)
77	X-RAY DIFFRACTION	77	(CHAIN F AND RESID 13:17)
78	X-RAY DIFFRACTION	78	(CHAIN F AND RESID 18:25)
79	X-RAY DIFFRACTION	79	(CHAIN F AND RESID 26:53)
80	X-RAY DIFFRACTION	80	(CHAIN F AND RESID 54:64)
81	X-RAY DIFFRACTION	81	(CHAIN F AND RESID 65:72)
82	X-RAY DIFFRACTION	82	(CHAIN F AND RESID 73:112)
83	X-RAY DIFFRACTION	83	(CHAIN F AND RESID 113:117)
84	X-RAY DIFFRACTION	84	(CHAIN F AND RESID 118:130)
85	X-RAY DIFFRACTION	85	(CHAIN F AND RESID 131:136)
86	X-RAY DIFFRACTION	86	(CHAIN F AND RESID 137:154)
87	X-RAY DIFFRACTION	87	(CHAIN F AND RESID 155:171)
88	X-RAY DIFFRACTION	88	(CHAIN F AND RESID 172:183)
89	X-RAY DIFFRACTION	89	(CHAIN F AND RESID 184:191)
90	X-RAY DIFFRACTION	90	(CHAIN F AND RESID 192:205)
91	X-RAY DIFFRACTION	91	(CHAIN G AND RESID 1:12)
92	X-RAY DIFFRACTION	92	(CHAIN G AND RESID 13:17)
93	X-RAY DIFFRACTION	93	(CHAIN G AND RESID 18:25)
94	X-RAY DIFFRACTION	94	(CHAIN G AND RESID 26:54)
95	X-RAY DIFFRACTION	95	(CHAIN G AND RESID 55:64)
96	X-RAY DIFFRACTION	96	(CHAIN G AND RESID 65:75)
97	X-RAY DIFFRACTION	97	(CHAIN G AND RESID 76:112)
98	X-RAY DIFFRACTION	98	(CHAIN G AND RESID 113:117)
99	X-RAY DIFFRACTION	99	(CHAIN G AND RESID 118:129)
100	X-RAY DIFFRACTION	100	(CHAIN G AND RESID 130:135)
101	X-RAY DIFFRACTION	101	(CHAIN G AND RESID 136:149)
102	X-RAY DIFFRACTION	102	(CHAIN G AND RESID 150:155)
103	X-RAY DIFFRACTION	103	(CHAIN G AND RESID 156:183)
104	X-RAY DIFFRACTION	104	(CHAIN G AND RESID 184:191)
105	X-RAY DIFFRACTION	105	(CHAIN G AND RESID 192:205)
106	X-RAY DIFFRACTION	106	(CHAIN H AND RESID 1:12)
107	X-RAY DIFFRACTION	107	(CHAIN H AND RESID 13:17)
108	X-RAY DIFFRACTION	108	(CHAIN H AND RESID 18:24)
109	X-RAY DIFFRACTION	109	(CHAIN H AND RESID 25:30)
110	X-RAY DIFFRACTION	110	(CHAIN H AND RESID 31:54)
111	X-RAY DIFFRACTION	111	(CHAIN H AND RESID 55:64)
112	X-RAY DIFFRACTION	112	(CHAIN H AND RESID 65:72)
113	X-RAY DIFFRACTION	113	(CHAIN H AND RESID 73:129)
114	X-RAY DIFFRACTION	114	(CHAIN H AND RESID 130:135)
115	X-RAY DIFFRACTION	115	(CHAIN H AND RESID 136:154)
116	X-RAY DIFFRACTION	116	(CHAIN H AND RESID 155:172)
117	X-RAY DIFFRACTION	117	(CHAIN H AND RESID 173:183)
118	X-RAY DIFFRACTION	118	(CHAIN H AND RESID 184:189)
119	X-RAY DIFFRACTION	119	(CHAIN H AND RESID 190:200)
120	X-RAY DIFFRACTION	120	(CHAIN H AND RESID 201:205)
121	X-RAY DIFFRACTION	121	(CHAIN I AND RESID 1:14)
122	X-RAY DIFFRACTION	122	(CHAIN I AND RESID 15:22)
123	X-RAY DIFFRACTION	123	(CHAIN I AND RESID 23:27)
124	X-RAY DIFFRACTION	124	(CHAIN I AND RESID 28:54)
125	X-RAY DIFFRACTION	125	(CHAIN I AND RESID 55:64)
126	X-RAY DIFFRACTION	126	(CHAIN I AND RESID 65:72)
127	X-RAY DIFFRACTION	127	(CHAIN I AND RESID 73:112)
128	X-RAY DIFFRACTION	128	(CHAIN I AND RESID 113:117)
129	X-RAY DIFFRACTION	129	(CHAIN I AND RESID 118:129)
130	X-RAY DIFFRACTION	130	(CHAIN I AND RESID 130:135)
131	X-RAY DIFFRACTION	131	(CHAIN I AND RESID 136:154)
132	X-RAY DIFFRACTION	132	(CHAIN I AND RESID 155:160)
133	X-RAY DIFFRACTION	133	(CHAIN I AND RESID 161:182)
134	X-RAY DIFFRACTION	134	(CHAIN I AND RESID 183:190)
135	X-RAY DIFFRACTION	135	(CHAIN I AND RESID 191:205)
136	X-RAY DIFFRACTION	136	(CHAIN J AND RESID 1:12)
137	X-RAY DIFFRACTION	137	(CHAIN J AND RESID 13:17)
138	X-RAY DIFFRACTION	138	(CHAIN J AND RESID 18:25)
139	X-RAY DIFFRACTION	139	(CHAIN J AND RESID 26:53)
140	X-RAY DIFFRACTION	140	(CHAIN J AND RESID 54:60)
141	X-RAY DIFFRACTION	141	(CHAIN J AND RESID 61:71)
142	X-RAY DIFFRACTION	142	(CHAIN J AND RESID 72:76)
143	X-RAY DIFFRACTION	143	(CHAIN J AND RESID 77:112)
144	X-RAY DIFFRACTION	144	(CHAIN J AND RESID 113:117)
145	X-RAY DIFFRACTION	145	(CHAIN J AND RESID 118:154)
146	X-RAY DIFFRACTION	146	(CHAIN J AND RESID 155:160)
147	X-RAY DIFFRACTION	147	(CHAIN J AND RESID 161:183)
148	X-RAY DIFFRACTION	148	(CHAIN J AND RESID 184:190)
149	X-RAY DIFFRACTION	149	(CHAIN J AND RESID 191:200)
150	X-RAY DIFFRACTION	150	(CHAIN J AND RESID 201:205)

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