pH: 5 詳細: PROTEIN (10MM HEPES PH 7.5, 150 MM NACL, 10% GLYCEROL, 5 MM DTT, 5 MM MGCL);RESERVOUR (2.5 M NA/K PHOSPHATE, 150 MM NACITRATE, PH 5.0;CRYOPROTECTION (1.8 M NA/K PHOSPHATE, 100 MM NACITRATE, ...詳細: PROTEIN (10MM HEPES PH 7.5, 150 MM NACL, 10% GLYCEROL, 5 MM DTT, 5 MM MGCL);RESERVOUR (2.5 M NA/K PHOSPHATE, 150 MM NACITRATE, PH 5.0;CRYOPROTECTION (1.8 M NA/K PHOSPHATE, 100 MM NACITRATE, 18.5% GLYCEROL, 185 MM MGSO4) TWO MINUTE SOAK.
解像度: 2.001→32.989 Å / SU ML: 0.22 / σ(F): 0 / 位相誤差: 17.96 / 立体化学のターゲット値: ML 詳細: MAGNESIUM IN ACTIVE SITE CHOSEN OVER WATER DUE TO COORDINATION NUMBER AND GEOMETRY. MOST LIKELY DOES NOT REPRESENT THE TYPICAL COORDINATION DURING CHEMISTRY. PHOSPHATE IS ASSUMED TO BE BOUND ...詳細: MAGNESIUM IN ACTIVE SITE CHOSEN OVER WATER DUE TO COORDINATION NUMBER AND GEOMETRY. MOST LIKELY DOES NOT REPRESENT THE TYPICAL COORDINATION DURING CHEMISTRY. PHOSPHATE IS ASSUMED TO BE BOUND BY THE ACTIVE SITE POSITION THAT COORDINATES THE PHOSPHATE OF SUBSTRATE.
Rfactor
反射数
%反射
Rfree
0.2177
1106
5.1 %
Rwork
0.1707
-
-
obs
0.173
21908
95.89 %
溶媒の処理
減衰半径: 0.83 Å / VDWプローブ半径: 1.1 Å / 溶媒モデル: FLAT BULK SOLVENT MODEL / Bsol: 37.422 Å2 / ksol: 0.376 e/Å3