SINEFUNGIN IS REPRESENTED AS ADENOSYL-ORNITHINE (SFG). WE OBSERVE SOME POSITIVE DENSITY NEAR THE ...SINEFUNGIN IS REPRESENTED AS ADENOSYL-ORNITHINE (SFG). WE OBSERVE SOME POSITIVE DENSITY NEAR THE SINEFUNGIN MOLECULE THAT WE CANNOT BUILD INTO. WE ONLY OBSERVE IT FOR THE SINEFUNGIN DATA AND NOT FROM THE S-ADENOSYL HOMOCYSTEINE. MOST LIKELY DUE TO A CONTAMINANT FROM THE SINEFUNGIN COMPOUND. ZN ION WAS BUILT IN SOME DENSITY WE COULD NOT ACCOUNT FOR. THE FLUORESCENT SCAN AT THE BEAMLINE REVEALED ZN AND THE ANOMALOUS MAP MATCHED THAT PEAK. WE DO NOT SEE THIS PEAK FOR THE S-ADENOSYL HOMOCYSTEINE DATA (PROBABLY DUE TO A CONTAMINANT FROM THE SINEFUNGIN COMPOUND).
解像度: 1.9→40 Å / Cor.coef. Fo:Fc: 0.952 / Cor.coef. Fo:Fc free: 0.911 / SU B: 7.621 / SU ML: 0.105 / 交差検証法: THROUGHOUT / ESU R: 0.17 / ESU R Free: 0.162 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.23423
3183
5.1 %
RANDOM
Rwork
0.17456
-
-
-
obs
0.17766
59055
93.8 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK