#1: Journal: Acta Crystallogr.,Sect.F / Year: 2010 Title: Purification, Crystallization and Preliminary X- Ray Analysis of Human Gimap2. Authors: Schwefel, D. / Frohlich, C. / Daumke, O.
Type: MARMOSAIC 225 mm CCD / Detector: CCD / Date: Jun 19, 2008
Radiation
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.9184 Å / Relative weight: 1
Reflection
Resolution: 1.9→50 Å / Num. obs: 18848 / % possible obs: 99.7 % / Observed criterion σ(I): 1 / Redundancy: 5.1 % / Biso Wilson estimate: 32.9 Å2 / Rmerge(I) obs: 0.07 / Net I/σ(I): 18.1
Reflection shell
Resolution: 1.9→2 Å / Redundancy: 4.1 % / Rmerge(I) obs: 0.53 / Mean I/σ(I) obs: 3 / % possible all: 98.8
-
Processing
Software
Name
Version
Classification
REFMAC
5.2.0019
refinement
XDS
datareduction
XDS
datascaling
MOLREP
phasing
Refinement
Method to determine structure: MOLECULAR REPLACEMENT / Resolution: 1.9→19.44 Å / Cor.coef. Fo:Fc: 0.954 / Cor.coef. Fo:Fc free: 0.935 / SU B: 5.517 / SU ML: 0.089 / Cross valid method: THROUGHOUT / ESU R: 0.143 / ESU R Free: 0.133 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. ATOM RECORD CONTAINS SUM OF TLS AND RESIDUAL B FACTORS. ANISOU RECORD CONTAINS SUM OF TLS AND RESIDUAL U FACTORS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.22109
958
5.1 %
RANDOM
Rwork
0.18456
-
-
-
obs
0.18637
17886
99.89 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK