Mass: 18.015 Da / Num. of mol.: 208 / Source method: isolated from a natural source / Formula: H2O
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 2.87 Å3/Da / Density % sol: 57.19 % / Description: NONE
Crystal grow
Temperature: 291 K / Method: vapor diffusion, hanging drop / pH: 8.5 Details: 1 MICROLITER DROPS OF A 6.5 MG/ML PROTEIN SOLUTION WITH A SOLUTION CONTAINING 0.1M TRIS-HCL, 1.4 M SODIUM CITRATE, PH 8.5 AT 291K.
Resolution: 1.7→15 Å / Cor.coef. Fo:Fc: 0.956 / Cor.coef. Fo:Fc free: 0.941 / SU B: 2.848 / SU ML: 0.088 / Cross valid method: THROUGHOUT / ESU R: 0.1 / ESU R Free: 0.102 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.239
1984
3.6 %
RANDOM
Rwork
0.205
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obs
0.207
52997
99.8 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.4 Å / Solvent model: MASK