SEQUENCE AUTHORS STATE THAT THE DIFFERENCE BETWEEN THEIR CLONED SEQUENCE AND THE DATABASE SEQUENCE ... SEQUENCE AUTHORS STATE THAT THE DIFFERENCE BETWEEN THEIR CLONED SEQUENCE AND THE DATABASE SEQUENCE AT POSITION 457 REPRESENTS VARIATION IN THE PHAGE SEQUENCE AND NOT A MUTATION INCORPORATED BY AMPLIFICATION OF THE GENE.
解像度: 2.7→30 Å / FOM work R set: 0.821 / Isotropic thermal model: Restrained / 交差検証法: THROUGHOUT / σ(F): 0 / 立体化学のターゲット値: Engh & Huber 詳細: Atoms at 0.00 occupancy have little or no electron density and were modelled stereochemically. Residues 287-295 are missing due to insufficient electron density
Rfactor
反射数
%反射
Selection details
Rfree
0.25
1292
5 %
Random
Rwork
0.217
-
-
-
obs
-
25425
97.5 %
-
溶媒の処理
Bsol: 50.771 Å2
原子変位パラメータ
Biso mean: 69.1 Å2
Baniso -1
Baniso -2
Baniso -3
1-
-14.783 Å2
0 Å2
0 Å2
2-
-
30.546 Å2
0 Å2
3-
-
-
-15.762 Å2
Refine analyze
Free
Obs
Luzzati coordinate error
0.38 Å
0.32 Å
Luzzati d res low
-
5 Å
Luzzati sigma a
0.48 Å
0.44 Å
精密化ステップ
サイクル: LAST / 解像度: 2.7→30 Å
タンパク質
核酸
リガンド
溶媒
全体
原子数
4017
0
0
106
4123
拘束条件
Refine-ID
タイプ
Dev ideal
Dev ideal target
X-RAY DIFFRACTION
c_bond_d
0.007
X-RAY DIFFRACTION
c_angle_deg
1.261
X-RAY DIFFRACTION
c_mcbond_it
1.344
1.5
X-RAY DIFFRACTION
c_scbond_it
2.018
2
X-RAY DIFFRACTION
c_mcangle_it
2.331
2
X-RAY DIFFRACTION
c_scangle_it
3.126
2.5
X-RAY DIFFRACTION
c_dihedral_angle_d
22.8
X-RAY DIFFRACTION
c_improper_angle_d
0.68
LS精密化 シェル
Refine-ID: X-RAY DIFFRACTION / Total num. of bins used: 25