1.2 mM [U-100% 13C; U-100% 15N] homodimer protein SP_0782 (7-79) from Streptococcus pneumoniae, 20 mM ammonium acetate, 100 mM sodium chloride, 5 mM calcium chloride, 10 mM DTT, 0.02 % sodium azide, 90% H2O/10% D2O
90% H2O/10% D2O
2
1.2 mM [U-5% 13C; U-100% 15N] homodimer protein SP_0782 (7-79) from Streptococcus pneumoniae, 20 mM ammonium acetate, 100 mM sodium chloride, 5 mM calcium chloride, 10 mM DTT, 0.02 % sodium azide, 90% H2O/10% D2O
90% H2O/10% D2O
3
1.2 mM [U-100% 13C; U-100% 15N] homodimer protein SP_0782 (7-79) from Streptococcus pneumoniae, 20 mM ammonium acetate, 100 mM sodium chloride, 5 mM calcium chloride, 10 mM DTT, 0.02 % sodium azide, 100% D2O
100% D2O
4
1.2 mM (1) [U-100% 13C; U-100% 15N]; (2) natural abundance homodimer protein SP_0782 (7-79) from Streptococcus pneumoniae, 20 mM ammonium acetate, 100 mM sodium chloride, 5 mM calcium chloride, 10 mM DTT, 0.02 % sodium azide, 90% H2O/10% D2O
90% H2O/10% D2O
試料
濃度 (mg/ml)
構成要素
Isotopic labeling
Solution-ID
1.2mM
homodimer protein SP_0782 (7-79) from Streptococcus pneumoniae-1
[U-100% 13C; U-100% 15N]
1
20mM
ammonium acetate-2
1
100mM
sodium chloride-3
1
5mM
calcium chloride-4
1
10mM
DTT-5
1
0.02 %
sodium azide-6
1
1.2mM
homodimer protein SP_0782 (7-79) from Streptococcus pneumoniae-7
[U-5% 13C; U-100% 15N]
2
20mM
ammonium acetate-8
2
100mM
sodium chloride-9
2
5mM
calcium chloride-10
2
10mM
DTT-11
2
0.02 %
sodium azide-12
2
1.2mM
homodimer protein SP_0782 (7-79) from Streptococcus pneumoniae-13
[U-100% 13C; U-100% 15N]
3
20mM
ammonium acetate-14
3
100mM
sodium chloride-15
3
5mM
calcium chloride-16
3
10mM
DTT-17
3
0.02 %
sodium azide-18
3
1.2mM
homodimer protein SP_0782 (7-79) from Streptococcus pneumoniae-19