SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "EC" IN EACH CHAIN ON SHEET RECORDS BELOW ... SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "EC" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 8-STRANDED BARREL THIS IS REPRESENTED BY A 9-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL. THE SHEETS PRESENTED AS "HC" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 8-STRANDED BARREL THIS IS REPRESENTED BY A 9-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL.
THE CONFLICTS REPRESENTED IN THE DBREF RECORDS ARE SEQUENCE VARIATIONS AND THE TWO LOX SEQUENCES ...THE CONFLICTS REPRESENTED IN THE DBREF RECORDS ARE SEQUENCE VARIATIONS AND THE TWO LOX SEQUENCES CORRESPOND TO THE PUBMED ID BAA09172 AND AAB361001
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2.2 Å3/Da / 溶媒含有率: 44.6 %
結晶化
pH: 7.5 詳細: 20% PEG 4000, 10% ISOPROPANOL, 0.1M HEPES AT PH 7.5, AND 0.1M NA-L-LACTATE
解像度: 2.1→12 Å / Cor.coef. Fo:Fc: 0.923 / Cor.coef. Fo:Fc free: 0.866 / SU B: 6.192 / SU ML: 0.162 / 交差検証法: THROUGHOUT / ESU R: 0.242 / ESU R Free: 0.205 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.257
2543
1.5 %
RANDOM
Rwork
0.2
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obs
0.201
167801
100 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK