CATALYZES A REVERSIBLE EPIMERIZATION OF GDP-D-MANNOSE.
配列の詳細
THE FIRST TWO RESIDUES (GA) IN THE SPECIFIED SEQUENCE ARE A REMNANT FROM A CLEAVED HIS-TAG (AND ARE ...THE FIRST TWO RESIDUES (GA) IN THE SPECIFIED SEQUENCE ARE A REMNANT FROM A CLEAVED HIS-TAG (AND ARE NOT IN THE UNIPROT SEQUENCE), THE RESIDUE NUMBERING IN THE STRUCTURE USES THE THIRD RESIDUE (M) AS RESIDUE 1.
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 1.75 Å3/Da / 溶媒含有率: 29.04 %
結晶化
手法: 蒸気拡散法, シッティングドロップ法 / pH: 6 詳細: 100 MM BIS-TRIS PH 6.0, 2.2 M AMMONIUM SULPHATE, SITTING DROP VAPOUR DIFFUSION. CRYOPROTECTED WITH 6M SODIUM FORMATE.
解像度: 2→29.88 Å / Cor.coef. Fo:Fc: 0.968 / Cor.coef. Fo:Fc free: 0.929 / SU B: 4.606 / SU ML: 0.13 / 交差検証法: THROUGHOUT / ESU R: 0.202 / ESU R Free: 0.182 / 立体化学のターゲット値: RESTRAINED / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.223
2324
5.1 %
RANDOM
Rwork
0.147
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obs
0.151
43435
99.6 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK