Mass: 18.015 Da / Num. of mol.: 447 / Source method: isolated from a natural source / Formula: H2O
Sequence details
AUTHORS SEQUENCE NOT YET DEPOSITED IN SEQUENCE DATABASE. RESIDUE THR 3 HAS BEEN MUTATED TO VAL 3. ...AUTHORS SEQUENCE NOT YET DEPOSITED IN SEQUENCE DATABASE. RESIDUE THR 3 HAS BEEN MUTATED TO VAL 3. THE GENBANK REFERENCE CODE FOR THIS ENTRY IS GQ232759.
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 2.3 Å3/Da / Density % sol: 45.7 %
Crystal grow
pH: 6.5 / Details: 2.2M (NH4)2SO4, 0.1M MES PH 6.5
Resolution: 1.8→72.17 Å / Cor.coef. Fo:Fc: 0.955 / Cor.coef. Fo:Fc free: 0.932 / SU B: 3.309 / SU ML: 0.103 / Cross valid method: THROUGHOUT / ESU R: 0.138 / ESU R Free: 0.133 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.231
3575
5 %
RANDOM
Rwork
0.186
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obs
0.189
67358
99.7 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK