+Open data
-Basic information
Entry | Database: PDB / ID: 243d | ||||||||||||||||||
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Title | STRUCTURE OF THE DNA OCTANUCLEOTIDE D(ACGTACGT)2 | ||||||||||||||||||
Components | DNA (5'-D(*Keywords | DNA / A-DNA / DOUBLE HELIX | Function / homology | DNA | Function and homology information Method | X-RAY DIFFRACTION / Resolution: 1.9 Å | Authors | Wilcock, D.J. / Adams, A. / Cardin, C.J. / Wakelin, L.P.G. | Citation | Journal: Acta Crystallogr.,Sect.D / Year: 1996 | Title: Structure of the DNA octanucleotide d(ACGTACGT)2. Authors: Wilcock, D.J. / Adams, A. / Cardin, C.J. / Wakelin, L.P. History |
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-Structure visualization
Structure viewer | Molecule: MolmilJmol/JSmol |
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-Downloads & links
-Download
PDBx/mmCIF format | 243d.cif.gz | 12.8 KB | Display | PDBx/mmCIF format |
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PDB format | pdb243d.ent.gz | 7.4 KB | Display | PDB format |
PDBx/mmJSON format | 243d.json.gz | Tree view | PDBx/mmJSON format | |
Others | Other downloads |
-Validation report
Arichive directory | https://data.pdbj.org/pub/pdb/validation_reports/43/243d ftp://data.pdbj.org/pub/pdb/validation_reports/43/243d | HTTPS FTP |
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-Related structure data
Similar structure data |
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-Links
-Assembly
Deposited unit |
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1 |
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Unit cell |
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-Components
#1: DNA chain | Mass: 2426.617 Da / Num. of mol.: 1 / Source method: obtained synthetically |
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#2: Water | ChemComp-HOH / |
-Experimental details
-Experiment
Experiment | Method: X-RAY DIFFRACTION |
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-Sample preparation
Crystal | Density Matthews: 2.35 Å3/Da / Density % sol: 47.56 % | ||||||||||||||||||||||||||||||||||||||||
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Crystal grow | Temperature: 291 K / Method: vapor diffusion, hanging drop / pH: 7 Details: pH 7.00, VAPOR DIFFUSION, HANGING DROP, temperature 291.00K | ||||||||||||||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS Temperature: 291 K / pH: 7 | ||||||||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 295 K |
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Diffraction source | Source: SEALED TUBE / Type: OTHER / Wavelength: 0.7107 |
Detector | Type: MARRESEARCH / Detector: IMAGE PLATE / Date: Oct 4, 1993 |
Radiation | Scattering type: x-ray |
Radiation wavelength | Wavelength: 0.7107 Å / Relative weight: 1 |
Reflection | Resolution: 1.5→9 Å / Num. all: 24514 / Num. obs: 3962 / % possible obs: 88.7 % / Observed criterion σ(I): 1 / Rmerge(I) obs: 0.0883 |
Reflection | *PLUS Highest resolution: 1.5 Å / Lowest resolution: 9 Å / % possible obs: 88.7 % / Observed criterion σ(I): 1 |
-Processing
Software |
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Refinement | Resolution: 1.9→5 Å / σ(F): 1
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Refine Biso |
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Refinement step | Cycle: LAST / Resolution: 1.9→5 Å
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Refine LS restraints |
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Software | *PLUS Name: X-PLOR / Classification: refinement | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refinement | *PLUS Highest resolution: 1.9 Å / Lowest resolution: 5 Å / σ(F): 1 | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Solvent computation | *PLUS | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | *PLUS Biso mean: 15 Å2 |