M: DNA (5'-D(*CP*CP*TP*AP*TP*CP*AP*AP*TP*GP*AP*TP*AP*GP*A)-3') N: DNA (5'-D(*TP*CP*TP*AP*TP*CP*AP*TP*TP*GP*AP*TP*AP*GP*G)-3') A: PROTEIN (TETRACYCLINE REPRESSOR) ヘテロ分子
M: DNA (5'-D(*CP*CP*TP*AP*TP*CP*AP*AP*TP*GP*AP*TP*AP*GP*A)-3') N: DNA (5'-D(*TP*CP*TP*AP*TP*CP*AP*TP*TP*GP*AP*TP*AP*GP*G)-3') A: PROTEIN (TETRACYCLINE REPRESSOR) ヘテロ分子
M: DNA (5'-D(*CP*CP*TP*AP*TP*CP*AP*AP*TP*GP*AP*TP*AP*GP*A)-3') N: DNA (5'-D(*TP*CP*TP*AP*TP*CP*AP*TP*TP*GP*AP*TP*AP*GP*G)-3') A: PROTEIN (TETRACYCLINE REPRESSOR) ヘテロ分子
タイプ: MARRESEARCH / 検出器: AREA DETECTOR / 日付: 1997年7月28日
放射
プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 1.5418 Å / 相対比: 1
反射
解像度: 2.45→34.5 Å / Num. obs: 12437 / % possible obs: 97.2 % / Observed criterion σ(I): 0 / 冗長度: 3.4 % / Biso Wilson estimate: 58 Å2 / Rmerge(I) obs: 0.09 / Net I/σ(I): 12.1
反射 シェル
解像度: 2.45→2.55 Å / 冗長度: 3 % / Rmerge(I) obs: 0.287 / % possible all: 93.3
反射
*PLUS
最低解像度: 24.5 Å / Num. obs: 11520 / Num. measured all: 42624 / Biso Wilson estimate: 57.9 Å2
反射 シェル
*PLUS
% possible obs: 94.4 % / Mean I/σ(I) obs: 3.3
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解析
ソフトウェア
名称
バージョン
分類
AMoRE
位相決定
X-PLOR
3.851
精密化
DENZO
データ削減
SCALEPACK
データスケーリング
精密化
解像度: 2.5→34.5 Å / 交差検証法: THROUGHOUT / σ(F): 2 詳細: USED WEIGHTED FULL MATRIX LEAST SQUARE PROCEDURE. THE DNA BASE PAIRS 1, 8 AND 15 ARE NOT PALINDROMIC. IN REFINEMENT THE CENTRAL BASE M 8 WAS MODELED USING ADENINE AND THYMINE WITH 50 % ...詳細: USED WEIGHTED FULL MATRIX LEAST SQUARE PROCEDURE. THE DNA BASE PAIRS 1, 8 AND 15 ARE NOT PALINDROMIC. IN REFINEMENT THE CENTRAL BASE M 8 WAS MODELED USING ADENINE AND THYMINE WITH 50 % OCCUPANCY EACH, RESPECTIVELY. BASE M 1 WAS EITHER CYTOSINE OR THYMINE AND BASE M 15 WAS EITHER GUANINE OR ADENINE. DUE TO CLOSE CRYSTAL PACKING CONTACTS THESE TERMINAL BASES WERE FOUND DISORDERED AND WERE MODELED AS CYTOSINE (BASE M 1) AND ADENINE (BASE M 15), RESPECTIVELY.