Mass: 5350.189 Da / Num. of mol.: 1 / Fragment: ANTICODON (RESIDUES 27-43) / Source method: obtained synthetically
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Experimental details
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Experiment
Experiment
Method: SOLUTION NMR
NMR experiment
Conditions-ID
Experiment-ID
Solution-ID
Type
1
1
1
NOESY
1
2
1
ROESY
1
3
1
TOCSY
1
4
1
HMQC
1
5
1
1H-31P COSY
1
6
1
1H-31P HETERO-TOCSY-TOCSY
1
7
1
DQCOSY
NMR details
Text: LOWEST RMSD DIFFERENCE FROM AVERAGE STRUCTURE. STRUCTURE WAS DETERMINED USING RESTRAINTS FROM HOMONUCLEAR ROESY, DQCOSY AND NOESY DATA. ASSIGNMENTS WERE MADE WITH A COMBINATION OF ROESY, NOESY, ...Text: LOWEST RMSD DIFFERENCE FROM AVERAGE STRUCTURE. STRUCTURE WAS DETERMINED USING RESTRAINTS FROM HOMONUCLEAR ROESY, DQCOSY AND NOESY DATA. ASSIGNMENTS WERE MADE WITH A COMBINATION OF ROESY, NOESY, TOCSY, 1H-13C HMQC AND 1H-31P.
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Sample preparation
Details
Contents: H2O/D2O
Sample conditions
Ionic strength: 100 mM NACL / pH: 7 / Temperature: 303 K
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