温度: 298 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 6.7 詳細: Crystals are formed by mixing in a 1:1 ratio endonuclease (5 mg/ml) with crystallization buffer containing 200 mM MES, 27% PEG8000, 200 mM ammonium sulfate, 1 mM manganese chloride, 10 mM ...詳細: Crystals are formed by mixing in a 1:1 ratio endonuclease (5 mg/ml) with crystallization buffer containing 200 mM MES, 27% PEG8000, 200 mM ammonium sulfate, 1 mM manganese chloride, 10 mM magnesium acetate, 10 mM taurine, and 50 mM sodium fluoride. Crystals form within a few hours and grow to maximum size in one to two weeks
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データ収集
回折
平均測定温度: 100 K Ambient temp details: . X-ray diffraction data collection was performed at the Cornell High Energy Synchrotron Source (CHESS) F1 beamline. The diffraction data were indexed, processed, scaled and ...Ambient temp details: . X-ray diffraction data collection was performed at the Cornell High Energy Synchrotron Source (CHESS) F1 beamline. The diffraction data were indexed, processed, scaled and merged using HKL2000.29 The structure was solved and refined using the software PHENIX.30
放射光源
由来: シンクロトロン / サイト: CHESS / ビームライン: F1 / 波長: 0.917 Å
検出器
タイプ: ADSC QUANTUM 270 / 検出器: CCD / 日付: 2013年12月9日
放射
プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 0.917 Å / 相対比: 1
反射
解像度: 1.8→22.9 Å / Num. all: 27807 / Num. obs: 27807 / % possible obs: 99.31 % / 冗長度: 3.5 % / Net I/σ(I): 22.39
反射 シェル
解像度: 1.8→1.83 Å / 冗長度: 3 % / Rmerge(I) obs: 0.592 / Mean I/σ(I) obs: 1.83 / % possible all: 99.2