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TitleRapid and efficient room-temperature serial synchrotron crystallography using the CFEL TapeDrive.
Journal, issue, pagesIucrj, Vol. 9, Page 778-791, Year 2022
Publish dateNov 17, 2021 (structure data deposition date)
AuthorsZielinski, K.A. / Prester, A. / Andaleeb, H. / Bui, S. / Yefanov, O. / Catapano, L. / Henkel, A. / Wiedorn, M.O. / Lorbeer, O. / Crosas, E. ...Zielinski, K.A. / Prester, A. / Andaleeb, H. / Bui, S. / Yefanov, O. / Catapano, L. / Henkel, A. / Wiedorn, M.O. / Lorbeer, O. / Crosas, E. / Meyer, J. / Mariani, V. / Domaracky, M. / White, T.A. / Fleckenstein, H. / Sarrou, I. / Werner, N. / Betzel, C. / Rohde, H. / Aepfelbacher, M. / Chapman, H.N. / Perbandt, M. / Steiner, R.A. / Oberthuer, D.
External linksIucrj / PubMed:36381150
MethodsX-ray diffraction
Resolution1.4 - 2.3 Å
Structure data

PDB-7qar:
Serial crystallography structure of cofactor-free urate oxidase in complex with the 5-peroxo derivative of 9-methyl uric acid at room temperature
Method: X-RAY DIFFRACTION / Resolution: 2.3 Å

PDB-7zpv:
Room temperature SSX crystal structure of CTX-M-14
Method: X-RAY DIFFRACTION / Resolution: 1.4 Å

PDB-7zq0:
Room temperature SSX structure of GH11 xylanase from Nectria haematococca (1000 frames)
Method: X-RAY DIFFRACTION / Resolution: 1.9 Å

PDB-8af4:
Room temperature SSX structure of GH11 xylanase from Nectria haematococca (40000 frames)
Method: X-RAY DIFFRACTION / Resolution: 1.51 Å

PDB-8af5:
Room temperature SSX structure of GH11 xylanase from Nectria haematococca (10000 frames)
Method: X-RAY DIFFRACTION / Resolution: 1.63 Å

PDB-8af6:
Room temperature SSX structure of GH11 xylanase from Nectria haematococca (4000 frames)
Method: X-RAY DIFFRACTION / Resolution: 1.7 Å

PDB-8af7:
Room temperature SSX crystal structure of CTX-M-14 (10K dataset)
Method: X-RAY DIFFRACTION / Resolution: 1.55 Å

PDB-8af8:
Room temperature SSX crystal structure of CTX-M-14 (5K dataset)
Method: X-RAY DIFFRACTION / Resolution: 1.55 Å

Chemicals

ChemComp-XDS:
(5S)-5-(dioxidanyl)-9-methyl-7H-purine-2,6,8-trione

ChemComp-HOH:
WATER

ChemComp-SO4:
SULFATE ION

Source
  • aspergillus flavus (mold)
  • klebsiella pneumoniae (bacteria)
  • fusarium haematococcum (fungus)
KeywordsOXIDOREDUCTASE / COFACTOR-FREE OXIDASE / REACTION INTERMEDIATE / SERIAL CRYSTALLOGRAPHY / DIOXYGEN / HYDROLASE / beta-lactamase / SSX / TapeDrive / Xylanase / room temperature

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