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TitleStructural Insights into Catalysis and Inhibition of O-Acetylserine Sulfhydrylase from Mycobacterium tuberculosis: CRYSTAL STRUCTURES OF THE ENZYME {alpha}-AMINOACRYLATE INTERMEDIATE AND AN ENZYME-INHIBITOR COMPLEX.
Journal, issue, pagesJ. Biol. Chem., Vol. 282, Page 23473-23481, Year 2007
Publish dateMay 30, 2007 (structure data deposition date)
AuthorsSchnell, R. / Oehlmann, W. / Singh, M. / Schneider, G.
External linksJ. Biol. Chem. / PubMed:17567578
MethodsX-ray diffraction
Resolution1.8 - 2.2 Å
Structure data

PDB-2q3b:
1.8 A Resolution Crystal Structure of O-Acetylserine Sulfhydrylase (OASS) Holoenzyme From MYCOBACTERIUM TUBERCULOSIS
Method: X-RAY DIFFRACTION / Resolution: 1.8 Å

PDB-2q3c:
2.1 A Resolution Crystal Structure of O-Acetylserine Sulfhydrylase (OASS) Holoenzyme From MYCOBACTERIUM TUBERCULOSIS in Complex with the Inhibitory Peptide DFSI
Method: X-RAY DIFFRACTION / Resolution: 2.1 Å

PDB-2q3d:
2.2 A Resolution Crystal Structure of O-Acetylserine Sulfhydrylase (OASS) From MYCOBACTERIUM TUBERCULOSIS in Complex with the Reaction Intermediate ALPHA-AMINOACRYLATE
Method: X-RAY DIFFRACTION / Resolution: 2.2 Å

Chemicals

ChemComp-CL:
Unknown entry

ChemComp-MPD:
(4S)-2-METHYL-2,4-PENTANEDIOL / precipitant*YM

ChemComp-HOH:
WATER

ChemComp-PDA:
2-[(3-HYDROXY-2-METHYL-5-PHOSPHONOOXYMETHYL-PYRIDIN-4-YLMETHYL)-AMINO]-PROPIONIC ACID

Source
  • mycobacterium tuberculosis (bacteria)
KeywordsTRANSFERASE / Mycobacterium tuberculosis / Pyridoxal-5'-phosphate / sulphur metabolism / cysteine biosynthesis / SAT / peptide-inhibitor / alpha-aminoacrylate intermediate

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