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TitleCatalytically important damage-free structures of a copper nitrite reductase obtained by femtosecond X-ray laser and room-temperature neutron crystallography.
Journal, issue, pagesIucrj, Vol. 6, Page 761-772, Year 2019
Publish dateJun 15, 2018 (structure data deposition date)
AuthorsHalsted, T.P. / Yamashita, K. / Gopalasingam, C.C. / Shenoy, R.T. / Hirata, K. / Ago, H. / Ueno, G. / Blakeley, M.P. / Eady, R.R. / Antonyuk, S.V. ...Halsted, T.P. / Yamashita, K. / Gopalasingam, C.C. / Shenoy, R.T. / Hirata, K. / Ago, H. / Ueno, G. / Blakeley, M.P. / Eady, R.R. / Antonyuk, S.V. / Yamamoto, M. / Hasnain, S.S.
External linksIucrj / PubMed:31316819
MethodsX-ray diffraction / neutron diffraction
Resolution1.5 - 1.801 Å
Structure data

PDB-6gsq:
Oxidised copper nitrite reductase from Achromobacter cycloclastes determined by serial femtosecond rotation crystallography
Method: X-RAY DIFFRACTION / Resolution: 1.5 Å

PDB-6gt0:
Nitrite-bound copper nitrite reductase from Achromobacter cycloclastes determined by serial femtosecond rotation crystallography
Method: X-RAY DIFFRACTION / Resolution: 1.5 Å

PDB-6gt2:
Reduced copper nitrite reductase from Achromobacter cycloclastes determined by serial femtosecond rotation crystallography
Method: X-RAY DIFFRACTION / Resolution: 1.6 Å

PDB-6gti:
Achromobacter cycloclastes copper nitrite reductase at pH 5.0
Method: X-RAY DIFFRACTION / Resolution: 1.5 Å

PDB-6gtj:
Neutron crystal structure for copper nitrite reductase from Achromobacter Cycloclastes at 1.8 A resolution
Method: NEUTRON DIFFRACTION / Resolution: 1.801 Å

PDB-6gtk:
Achromobacter cycloclastes copper nitrite reductase at pH 5.5
Method: X-RAY DIFFRACTION / Resolution: 1.5 Å

PDB-6gtl:
Achromobacter cycloclastes copper nitrite reductase at pH 6.0
Method: X-RAY DIFFRACTION / Resolution: 1.5 Å

PDB-6gtn:
Achromobacter cycloclastes copper nitrite reductase at pH 6.5
Method: X-RAY DIFFRACTION / Resolution: 1.5 Å

Chemicals

ChemComp-CU:
COPPER (II) ION

ChemComp-SO4:
SULFATE ION

ChemComp-HOH:
WATER

ChemComp-NO2:
NITRITE ION

ChemComp-MLI:
MALONATE ION

Source
  • achromobacter cycloclastes (bacteria)
KeywordsOXIDOREDUCTASE / FEMTOSECOND / SF-ROX / NITRITE REDUCTASE / Perdueteration / electron transfer

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