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Structure paper

TitleCrystallography and chemistry should always go together: a cautionary tale of protein complexes with cisplatin and carboplatin.
Journal, issue, pagesActa Crystallogr. ,Sect. D, Vol. 71, Page 1965-1979, Year 2015
Publish dateFeb 23, 2015 (structure data deposition date)
AuthorsShabalin, I. / Dauter, Z. / Jaskolski, M. / Minor, W. / Wlodawer, A.
External linksActa Crystallogr. ,Sect. D / PubMed:26327386
MethodsX-ray diffraction
Resolution0.98 - 2.14 Å
Structure data

PDB-4ydx:
Crystal structure of cisplatin bound to a human copper chaperone (monomer) - new refinement
Method: X-RAY DIFFRACTION / Resolution: 1.602 Å

PDB-4yea:
Crystal structure of cisplatin bound to a human copper chaperone (dimer) - new refinement
Method: X-RAY DIFFRACTION / Resolution: 2.14 Å

PDB-4yem:
Carboplatin binding to HEWL in NaBr crystallisation conditions studied at an X-ray wavelength of 0.9163A - new refinement
Method: X-RAY DIFFRACTION / Resolution: 1.47 Å

PDB-4yen:
Room temperature X-ray diffraction studies of cisplatin binding to HEWL in DMSO media after 14 months of crystal storage - new refinement
Method: X-RAY DIFFRACTION / Resolution: 2 Å

PDB-4yeo:
Triclinic HEWL co-crystallised with cisplatin, studied at a data collection temperature of 150K - new refinement
Method: X-RAY DIFFRACTION / Resolution: 0.98 Å

Chemicals

ChemComp-PT:
Unknown entry

ChemComp-SO4:
SULFATE ION

ChemComp-TCE:
3,3',3''-phosphanetriyltripropanoic acid

ChemComp-HOH:
WATER

ChemComp-CU:
COPPER (II) ION

ChemComp-BR:
BROMIDE ION

ChemComp-NA:
Unknown entry

ChemComp-DMS:
DIMETHYL SULFOXIDE / DMSO, precipitant*YM

ChemComp-ACT:
ACETATE ION

ChemComp-CL:
Unknown entry

ChemComp-CPT:
Cisplatin / medication, chemotherapy*YM

ChemComp-EDO:
1,2-ETHANEDIOL

ChemComp-NO3:
NITRATE ION

Source
  • homo sapiens (human)
  • gallus gallus (chicken)
KeywordsMETAL TRANSPORT / Re-refinement of 3iwl / cisplatin / platinum / Metal-binding / Re-refinement of 3iwx / HYDROLASE / Re-refinement of 4XAN / Carboplatin / Metal binding / lysozyme / Re-refinement of 4G4A / Re-refinement of 4mwk

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