N-TERMINAL GLYCINE REMAINS FROM TEV-CLEAVAGE OF EXPRESSION TAG. RESIDUE NUMBERING IS ACCORDING TO ...N-TERMINAL GLYCINE REMAINS FROM TEV-CLEAVAGE OF EXPRESSION TAG. RESIDUE NUMBERING IS ACCORDING TO MOUSE CNPASE ISOFORM 1 (P16330-2).
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 1.9 Å3/Da / 溶媒含有率: 36.6 % / 解説: NONE
結晶化
pH: 4 詳細: 250 UM PROTEIN AND 10 MM 2, 3(RP)-CYCLIC-AMPS MIXED WITH 0.5 PLUS 0.5 DROPS WITH 30% PEG4000 AND 50 MM ACETATE (MIX OF PH 3 AND PH 5 IN 2:1 RATIO) AT RT
解像度: 2.3→19.29 Å / SU ML: 0.31 / σ(F): 1.99 / 位相誤差: 30.09 / 立体化学のターゲット値: ML 詳細: HYDROGENS WERE INCLUDED IN RIDING POSITIONS. RESIDUES 158-162 AND 208-213 WERE EXCLUDED DUE TO INSUFFICIENT ELECTRON DENSITY.
Rfactor
反射数
%反射
Rfree
0.2694
418
5 %
Rwork
0.2112
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obs
0.2142
8367
98.03 %
溶媒の処理
減衰半径: 0.9 Å / VDWプローブ半径: 1.11 Å / 溶媒モデル: FLAT BULK SOLVENT MODEL