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Yorodumi- PDB-3ana: THREE-DIMENSIONAL STRUCTURE OF D(GGGATCCC) IN THE CRYSTALLINE STATE -
+Open data
-Basic information
Entry | Database: PDB / ID: 3ana | ||||||||||||||||||
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Title | THREE-DIMENSIONAL STRUCTURE OF D(GGGATCCC) IN THE CRYSTALLINE STATE | ||||||||||||||||||
Components | DNA (5'-D(*Keywords | DNA / A-DNA / DOUBLE HELIX | Function / homology | DNA | Function and homology information Method | X-RAY DIFFRACTION / Resolution: 2.5 Å | Authors | Heinemann, U. / Lauble, H. | Citation | Journal: Nucleic Acids Res. / Year: 1988 | Title: Three-dimensional structure of d(GGGATCCC) in the crystalline state. Authors: Lauble, H. / Frank, R. / Blocker, H. / Heinemann, U. History |
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-Structure visualization
Structure viewer | Molecule: MolmilJmol/JSmol |
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-Downloads & links
-Download
PDBx/mmCIF format | 3ana.cif.gz | 17.4 KB | Display | PDBx/mmCIF format |
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PDB format | pdb3ana.ent.gz | 10.4 KB | Display | PDB format |
PDBx/mmJSON format | 3ana.json.gz | Tree view | PDBx/mmJSON format | |
Others | Other downloads |
-Validation report
Summary document | 3ana_validation.pdf.gz | 361.2 KB | Display | wwPDB validaton report |
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Full document | 3ana_full_validation.pdf.gz | 369.8 KB | Display | |
Data in XML | 3ana_validation.xml.gz | 3.6 KB | Display | |
Data in CIF | 3ana_validation.cif.gz | 4.2 KB | Display | |
Arichive directory | https://data.pdbj.org/pub/pdb/validation_reports/an/3ana ftp://data.pdbj.org/pub/pdb/validation_reports/an/3ana | HTTPS FTP |
-Related structure data
Similar structure data |
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-Links
-Assembly
Deposited unit |
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1 |
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Unit cell |
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-Components
#1: DNA chain | Mass: 2427.605 Da / Num. of mol.: 2 / Source method: obtained synthetically #2: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: X-RAY DIFFRACTION |
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-Sample preparation
Crystal | Density Matthews: 2.9 Å3/Da / Density % sol: 57.59 % | |||||||||||||||||||||||||||||||||||
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Crystal grow | Method: microdialysis / Details: MICRODIALYSIS / Temp details: ROOM TEMPERATURE | |||||||||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS pH: 7.5 | |||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Ambient temp details: ROOM TEMPERATURE |
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Detector | Type: STOE / Detector: DIFFRACTOMETER |
Radiation | Scattering type: x-ray |
Radiation wavelength | Relative weight: 1 |
Reflection | Highest resolution: 2.5 Å / Num. all: 4130 / Num. obs: 1594 / Observed criterion σ(I): 1 |
Reflection | *PLUS Num. obs: 1300 / % possible obs: 78 % / Rmerge(I) obs: 0.029 / Num. measured all: 1594 |
-Processing
Software | Name: NUCLSQ / Classification: refinement | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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Refinement | Resolution: 2.5→10 Å / σ(F): 3 /
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Refine Biso |
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Refinement step | Cycle: LAST / Resolution: 2.5→10 Å
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Refine LS restraints |
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Refinement | *PLUS σ(F): 3 / Highest resolution: 2.5 Å / Lowest resolution: 10 Å / Num. reflection obs: 1428 / Rfactor obs: 0.166 | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Solvent computation | *PLUS | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | *PLUS | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refine LS restraints | *PLUS
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