SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AA" IN EACH CHAIN ON SHEET RECORDS BELOW ... SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AA" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 9-STRANDED BARREL THIS IS REPRESENTED BY A 10-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL. THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN THE SHEET RECORDS BELOW, TWO SHEETS ARE DEFINED.
pH: 7.5 詳細: 30 MGML-1 IN 50 MM IMIDAZOLE, 5 MM CACL2, 25 MM ACARBOSE, PH 7.5 MIXED IN 1:1 RATIO WITH THE WELL SOLUTION CONSISTING OF 0.1 M IMIDAZOLE PH 7.5 100 MM MALTOSE, 5 MM CACL2, AND WITH 18% (W/V) ...詳細: 30 MGML-1 IN 50 MM IMIDAZOLE, 5 MM CACL2, 25 MM ACARBOSE, PH 7.5 MIXED IN 1:1 RATIO WITH THE WELL SOLUTION CONSISTING OF 0.1 M IMIDAZOLE PH 7.5 100 MM MALTOSE, 5 MM CACL2, AND WITH 18% (W/V) MONOMETHYLETHER POLYETHYLENE GLYCOL 5K AS PRECIPITANT.
解像度: 2.1→15 Å / Cor.coef. Fo:Fc: 0.966 / Cor.coef. Fo:Fc free: 0.947 / SU B: 3.781 / SU ML: 0.1 / 交差検証法: THROUGHOUT / ESU R: 0.166 / ESU R Free: 0.151 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.198
699
2.1 %
RANDOM
Rwork
0.151
-
-
-
obs
0.152
33201
99.9 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK