温度: 288 K / 手法: 蒸気拡散法, シッティングドロップ法 詳細: Crystallized in plastic sitting drop trays, 30 nl of protein (concentration 10 mg/mL) combined with 30 nl precipitant: 0.10 M Ammonium acetate 10 %(w/v) PEG 3350 Solution was equilibrated ...詳細: Crystallized in plastic sitting drop trays, 30 nl of protein (concentration 10 mg/mL) combined with 30 nl precipitant: 0.10 M Ammonium acetate 10 %(w/v) PEG 3350 Solution was equilibrated against a reservoir of 60% PEG 3350.
解像度: 1.92→30 Å / Cor.coef. Fo:Fc: 0.969 / Cor.coef. Fo:Fc free: 0.946 / SU B: 11.056 / SU ML: 0.133 / 交差検証法: THROUGHOUT / ESU R Free: 0.159 / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS