温度: 293 K / 手法: 蒸気拡散法, ハンギングドロップ法 / pH: 4 詳細: 0.1 M sodium acetate, 0.25 M ammonium sulfate, 8% PEG 3350 The Crystal was soaked in crystallizaion solution containing 2mM CaCl2 and pH adjusted to 7.0 before data collection.
解像度: 1.06→19.04 Å / Cor.coef. Fo:Fc: 0.972 / Cor.coef. Fo:Fc free: 0.962 / SU B: 0.324 / SU ML: 0.017 / 交差検証法: THROUGHOUT / ESU R: 0.027 / ESU R Free: 0.029 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.17418
2873
5.1 %
RANDOM
Rwork
0.15401
-
-
-
obs
0.15502
53860
99.65 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK