Mass: 1034.210 Da / Num. of mol.: 1 / Source method: obtained synthetically / Details: This sequence occurs naturally in humans / Source: (synth.) Homo sapiens (human) / References: UniProt: P01042
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Experimental details
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Experiment
Experiment
Method: SOLID-STATE NMR
NMR experiment
Conditions-ID
Experiment-ID
Solution-ID
Sample state
Spectrometer-ID
Type
1
1
1
isotropic
1
2D 13C-13C DQ-SQ
1
2
1
isotropic
1
2D 15N-13C TEDOR
1
3
2
isotropic
1
2D 13C-13C DQ-SQ
1
4
2
isotropic
1
2D 15N-13C TEDOR
1
5
3
isotropic
1
2D 13C-13C DQ-SQ
1
6
3
isotropic
1
2D 15N-13C TEDOR
1
7
4
isotropic
1
2D 13C-13C DQ-SQ
1
8
4
isotropic
1
2D 15N-13C TEDOR
1
9
5
isotropic
1
2D 13C-13C DQ-SQ
1
10
5
isotropic
1
2D 15N-13C TEDOR
1
11
6
isotropic
1
2D 13C-13C DQ-SQ
1
12
6
isotropic
1
2D 15N-13C TEDOR
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Sample preparation
Details
Type
Solution-ID
Contents
Details
Label
Solvent system
solid
1
300 uM [U-13C; U-15N] K1 Des-Arg10-Kallidin (DAKD), 10 mM not labeled AMUPOL, 50 mM not labeled HEPES, 150 mM not labeled NaCl, 4 % w/v not labeled DDM, 0.4 % w/v not labeled CHS, 10% H2O/ 40%D2O/ 50% d8-glycerol
frozensolutionofDAKDinDDM/CHSdetergentmicelle
UCN-K1 DAKD
10% H2O/ 40%D2O/ 50% d8-glycerol
solid
2
300 uM [U-13C; U-15N] R2S7 Des-Arg10-Kallidin (DAKD), 10 mM not labeled AMUPOL, 50 mM not labeled HEPES, 150 mM not labeled NaCl, 4 % w/v not labeled DDM, 0.4 % w/v not labeled CHS, 10% H2O/ 40%D2O/ 50% d8-glycerol
frozensolutionofDAKDinDDM/CHSdetergentmicelle
UCN-R2S7 DAKD
10% H2O/ 40%D2O/ 50% d8-glycerol
solid
3
300 uM [U-13C; U-15N] P3 Des-Arg10-Kallidin (DAKD), 10 mM not labeled AMUPOL, 50 mM not labeled HEPES, 150 mM not labeled NaCl, 4 % w/v not labeled DDM, 0.4 % w/v not labeled CHS, 10% H2O/ 40%D2O/ 50% d8-glycerol
frozensolutionofDAKDinDDM/CHSdetergentmicelle
UCN-P3 DAKD
10% H2O/ 40%D2O/ 50% d8-glycerol
solid
4
300 uM [U-13C; U-15N] P4 Des-Arg10-Kallidin (DAKD), 10 mM not labeled AMUPOL, 50 mM not labeled HEPES, 150 mM not labeled NaCl, 4 % w/v not labeled DDM, 0.4 % w/v not labeled CHS, 10% H2O/ 40%D2O/ 50% d8-glycerol
frozensolutionofDAKDinDDM/CHSdetergentmicelle
UCN-P4 DAKD
10% H2O/ 40%D2O/ 50% d8-glycerol
solid
5
300 uM [U-13C; U-15N] G5F6 Des-Arg10-Kallidin (DAKD), 10 mM not labeled AMUPOL, 50 mM not labeled HEPES, 150 mM not labeled NaCl, 4 % w/v not labeled DDM, 0.4 % w/v not labeled CHS, 10% H2O/ 40%D2O/ 50% d8-glycerol
frozensolutionofDAKDinDDM/CHSdetergentmicelle
UCN-G5F6 DAKD
10% H2O/ 40%D2O/ 50% d8-glycerol
solid
6
300 uM [U-13C; U-15N] S7P9 Des-Arg10-Kallidin (DAKD), 10 mM not labeled AMUPOL, 50 mM not labeled HEPES, 150 mM not labeled NaCl, 4 % w/v not labeled DDM, 0.4 % w/v not labeled CHS, 10% H2O/ 40%D2O/ 50% d8-glycerol